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Valved Cracker for Sulfur

Valved Cracker for Sulfur

Valved Cracker for Sulfur

Product catalog summary
Overview: The Veeco MBE Valved Cracker for Sulfur is designed to provide superior control and convenience compared to standard sources. It features a large capacity crucible made of refractory metal, which is heated to produce a sulfur beam flux. The system includes a refractory metal needle valve for gas flow regulation and a quartz cracking zone to handle sulfur's corrosive nature.
Key Features and Enhancements:
  • The Mark V Valved Cracker includes a nozzle for improved flux uniformity and reduced material waste, leading to cost savings, longer campaigns, and less hazardous waste.
  • It supports both cracked and uncracked sulfur flux generation, with flux modulation and on/off control.
  • The system is compatible with the Veeco SMC-II Automated Valve Positioner for reliable control.
Principle of Operation: The source material is loaded into the crucible and heated. A needle valve regulates the evaporant entering the growth chamber, with valve position controlled manually or automatically. The conductance zone temperature is adjusted to produce either cracked or uncracked material, and an integrated nozzle optimizes flux uniformity.
Performance and Benefits: The Valved Cracker is widely used by II-VI research groups for its excellent flux stability and responsiveness. It allows for longer growth campaigns, charge preservation, thorough outgassing, reduced cross-contamination, and lower background levels. It has been successfully used in the growth of light-emitting diodes and laser diodes.
Product Specifications:
  • Available in 500cc and 2000cc capacities.
  • Typical operating temperatures: Bulk Zone 150-250°C, Cracking Zone 800-1000°C.
  • Valve response time is less than 3 seconds with the SMC-II Automated Valve Positioner.
  • Dynamic flux range spans two to three orders of magnitude.
Compatibility and Availability: The Valved Cracker is compatible with various systems from Veeco, Riber, VG Semicon, Perkin-Elmer, and others. Custom chamber solutions are also available.
Contact Information: For more details, contact Veeco Instruments Inc. at their St. Paul, MN location or visit their website.
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Catalog excerpts

Valved Cracker for Sulfur-1

Valved Cracker for Sulfur 500cc Valved Cracker for Sulfur • Generates either cracked or uncracked S flux • Provides flux modulation and on/off control • Large source capacity • Utilizes a nozzle for excellent flux uniformity and reduced material waste • Prevents loss of source material during system bakeout • Used by leading II-VI research groups worldwide with more than 30 in the field Description The Veeco MBE Valved Cracker for Sulfur offers convenience and control unrivaled by any standard source. The large capacity refractory metal crucible is heated to generate a sulfur beam flux (consisting of Sn where n=8,7,6,5,3,2). Gas flow is regulated through a refractory metal needle valve into an independently heated cracking zone. The temperature of the cracking zone may be adjusted to generate either uncracked sulfur flux or a beam of smaller sulfur species. The cracking zone is constructed of quartz rather than a refractory metal due to sulfur’s corrosive nature. With recent enhancements, the Mark V Valved Cracker for Sulfur incorporates a nozzle that provides excellent flux uniformity and reduced material waste. This improvement in material utilization results in: • Material cost savings • Longer campaigns • Shorter system cleaning time • Less hazardous waste generation • Reduced memory effects • Lower particulate levels and flaking • Reduced system window coating A Veeco SMC-II Automated Valve Positioner is recommended for use with this source for reliable, automated control of the needle valve. Principle of operation for the Valved Cracker for Sulfur. Source material is loaded into the large capacity crucible and heated. A needle valve in the conductance tube regulates the amount of evaporant which enters the growth chamber. Valve position is controlled with either a manual micrometer or an Automated Valve Positioner. The conductance zone temperature is controlled so as to produce beams of either cracked or uncracked material and an integrated nozzle optimizes the flux uniformity across the substrate while minimizing material waste.

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Valved Cracker for Sulfur-2

Performance and Benefits The Valved Cracker for Sulfur is used by leading II-VI research groups worldwide. Control over the growth process is optimized using a needle valve for nearly instantaneous flux modulations and complete flux shut-off. The source may be idled continuously at operating temperature without depleting the charge material. With mechanical flux control, rather than the thermal control used for conventional open sources, the charge capacity may be arbitrarily large without limiting the responsiveness of the source. Flux response to valve opening and closing for the Valved Cracker...

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Valved Cracker for Sulfur-3

Product Specifications Source Characteristics Maximum Charge Capacity Minimum Mounting Flange Size Standard 2.75”/70mm With Water-Cooling 4.5”/114mm Standard 4.5”/114mm With Water-Cooling 6”/152mm Cracking Head Length Standard 1.41”/36mm With Water-Cooling 2.2”/56mm External Dimensions Contact Veeco Crucible Dimensions/Interior Fill Port Diameter Standard 2.2”/56mm With Water-Cooling 2.7”/69mm Typical Operating Temperatures Bulk Zone Cracking Zone Maximum Outgassing Temperature (Power Requirements) Bulk Zone Cracking Zone Standard for bulk zone. Optional cooling coil or jacket for cracking zone...

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Valved Cracker for Sulfur-4

Valved Cracker for Sulfur Selection Guide Typical Source Commonly Used Indicated By “X” System 500cc X Veeco sources are also available for use on systems from Eiko, Anelva, Ulvac, SVTA, and DCA, as well as custom chambers. Contact Veeco for details. Solutions for a nanoscale world.™ Compound Semiconductor • MBE Operations 4900 Constellation Drive, St. Paul, MN 55127 USA Phone: (651) 482-0800, Fax: (651) 482-0600 www.veeco.com/mbe © 2009 Veeco Instruments Inc. All rights reserved. (3-09) GEN200 and GEN2000 are registered trademarks and GEN II, GEN III, GEN930, GEN 10, GEN20 and Solutions for...

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*Prices are pre-tax. They exclude delivery charges and customs duties and do not include additional charges for installation or activation options. Prices are indicative only and may vary by country, with changes to the cost of raw materials and exchange rates.