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Corrosive Series Valved Cracker

Corrosive Series Valved Cracker

Corrosive Series Valved Cracker

Product catalog summary
Overview
The Veeco Corrosive Series Valved Cracker is a patented technology designed for handling reactive high-vapor pressure materials like antimony and tellurium. It features an all-PBN (pyrolytic boron nitride) construction to prevent corrosion, offering valved flux control that is not possible with traditional metal crucibles and valves.

Design and Operation
The system includes a removable valve assembly and a large capacity crucible, both made of PBN. The crucible is heated to generate a beam flux, and the PBN valve regulates gas flow, ensuring rapid flux stabilization and reproducibility. The source can operate in both cracked and uncracked modes, with a nozzle optimizing flux uniformity and minimizing waste.

Key Features
  • Patented all-PBN construction with over 175 units in use.
  • Proven results as the only valved antimony source.
  • Excellent flux uniformity and reduced material waste.
  • Highly reproducible mechanical flux control.
  • Large charge capacity and compatibility with materials like Sb, Te, Cd, CdTe, Zn, and Mg.

Performance and Benefits
The Corrosive Series Valved Cracker allows for the growth of complex structures not achievable with conventional sources. It provides superior flux control, enabling the growth of mixed Group V layers without frequent recalibration. SIMS analysis shows excellent flux control and reproducibility.

Specifications
  • Available in 200cc and 2000cc capacities.
  • Compatible with various MBE systems, with customized exit nozzles for optimal flux uniformity.
  • Operates at temperatures ranging from 200°C to 1200°C, depending on the zone.
  • Requires a Veeco SMC-II Automated Valve Positioner for operation.

Applications and Compatibility
The system is compatible with a wide range of MBE systems from manufacturers like Veeco, Riber, VG Semicon, and others. It is suitable for use in systems handling corrosive materials and offers options for oxygen and ammonia compatibility.

Contact Information
For more information, contact Veeco Instruments Inc. at their St. Paul, MN location or visit their website.
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Catalog excerpts

Corrosive Series Valved Cracker-1

Corrosive Series Valved Cracker 200cc Mark V Corrosive Series Valved Cracker • Patented all-PBN crucible and valve mechanism with more than 175 in the field • Only valved antimony source with proven results The patented Veeco Corrosive Series Valved Cracker is the only proven all-PBN valved source available on the market today. This innovative technology offers valved flux control for reactive high-vapor pressure materials (such as antimony and tellurium) not compatible with the metal crucibles and valves of traditional valved sources. The source design utilizes an entire valve assembly, crucible, and conductance tube constructed exclusively of pyrolytic boron nitride (PBN) to protect them from corrosion. • Utilizes a nozzle for excellent flux uniformity and reduced material waste The valve assembly is removable, allowing easy loading of the large capacity crucible through the conductance tube. The crucible is heated to generate a beam flux. Gas flow is regulated through the PBN valve, providing rapid flux stabilization, quick shut-off, and excellent reproducibility. In the cracking zone, a molecular flux may be thermally cracked to smaller molecular or atomic species. The source can also be operated in uncracked mode, if desired. • Highly reproducible mechanical flux control • Large charge capacity • Permits operation in cracked or uncracked mode • Compatible with Sb, Te, Cd, CdTe, Zn and Mg Principle of operation for the Corrosive Series Valved Cracker. Source material is loaded into the PBN crucible through the conductance tube and heated. An all-PBN valve regulates the gas flow into the growth chamber. The valve must be controlled with a Veeco SMC-II Automated Valve Positioner. Heating of the conductance zone keeps the valve clear and provides thermal cracking of polyatomic species. An integrated nozzle optimizes the flux uniformity across the substrate while minimizing material waste.

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Corrosive Series Valved Cracker-2

A near linear flux response is observed over a wide range of valve positions. Data courtesy of UC Santa Barbara. Flux reproducibility is demonstrated in two separate runs through the same valve position sequence. Data courtesy of UC Santa Barbara. SIMS analysis of composition variation in linearity graded GaAs1-xSbx. Data courtesy of UC Santa Barbara. With recent enhancements, the Mark V Corrosive Series Valved Cracker incorporates a nozzle that provides excellent flux uniformity and reduced material waste. This improvement in material utilization results in: • • • • • • • SIMS step profile for...

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Corrosive Series Valved Cracker-3

Product Specifications Source Characteristics Charge Material Sb, Te, Cd, CdTe, Zn, Mg, along with other corrosive materials Maximum Charge Capacity Minimum Mounting Flange Size Standard 4.5”/114mm With Water-Cooling 6”/152mm Standard 6”/152mm With Water-Cooling 6”/152mm In-Vacuum Length Standard 2.2”/56mm With Water-Cooling 2.7”/69m3 Standard 3.4”/36mm With Water-Cooling 4.1”/104mm External Dimensions Contact Veeco Crucible Dimensions/Interior Maximum Charge Diameter Cracking Zone Conductance Zone Bulk Zone Cracking Zone Conductance Zone Bulk Zone Typical Operating Temperature Maximum Outgassing...

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Corrosive Series Valved Cracker-4

Corrosive Series Valved Cracker Selection Guide Typical Source Commonly Used Indicated By “X” Veeco sources are also available for use on systems from Eiko, Anelva, Ulvac, SVTA, and DCA, as well as custom chambers. Contact Veeco for details. * Available only in Mark IV design. For More Information Please contact the Veeco Sales Department and request a copy of the following application notes: • The Corrosive Series Valved Cracker for Antimony • Effects of Antimonide Growth in a III-V MBE System Solutions for a nanoscale world.™ Compound Semiconductor • MBE Operations 4900 Constellation Drive,...

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*Prices are pre-tax. They exclude delivery charges and customs duties and do not include additional charges for installation or activation options. Prices are indicative only and may vary by country, with changes to the cost of raw materials and exchange rates.