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µRC micro Reaction Calorimeter

µRC micro Reaction Calorimeter

µRC micro Reaction Calorimeter

Product catalog summary
Introduction
Calorimetry is a non-destructive technique used to study various materials through heat changes during chemical, physical, and biological reactions. The micro Reaction Calorimeter (µRC) by Thermal Hazard Technology (THT) is a versatile instrument applicable in chemical and pharmaceutical fields.

Specifications and Features
The µRC is a multi-function calorimeter capable of isothermal, step-isothermal, temperature scanning, and titration studies. It can handle small samples (up to 1.5ml) and achieve rapid temperature changes due to its efficient thermal equilibrium. The temperature range is from -20°C to 170°C, controlled by Peltier modules without external cooling.

Operation and Measurement
The µRC operates on a power compensation principle, providing fast signal response. It uses disposable HPLC glass vials for sample handling, with a baseline noise of 5µW at 25°C and a maximum detectable heat of 600mW. In titration mode, it can deliver liquid samples in volumes from 1-250µL.

Applications
  • Heat Capacity Determination: Measures heat capacity of solids, liquids, and mixtures accurately.
  • Process Hazard Analysis: Provides rapid hazard analysis with reduced costs and waste.
  • Process Development: Allows investigation of reaction parameters, reactant conversion, and catalysis.
  • Catalyst Screening: Enables selection of optimal catalysts by measuring kinetics and thermodynamics.
  • Dissolution Experiments: Measures enthalpy of solution reliably using the Solid Addition System.
  • Hydrogenation: Enhances hydrogenation processes by increasing hydrogen pressure.
  • Gas Flow Option: Studies carbon capture through CO2 absorption by amine solutions.


Technical Specifications
  • Dynamic Range: 5µW to 600mW
  • Temperature Range: -20°C to 170°C
  • Cell Volume: 1.5ml
  • Injection Volume: 1 to 250µL
  • Stirring Speed: 0 to 400rpm
  • Measurement Principle: Power compensation
  • Connection: USB cable
  • Footprint: 18.3 x 18.4 x 31.1cm


Contact Information
For more information, contact the head office in the UK or regional offices in the USA, India, and China.
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Catalog excerpts

µRC micro Reaction Calorimeter-1

µRC® micro Reaction Calorimeter Compact Multi-function Calorimeter Titration Calorimetry Isothermal Calorimetry Scanning Calorimetry Pressure Measurement ALL IN ONE INSTRUMENT

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µRC micro Reaction Calorimeter-2

µRC / micro Reaction Calorimeter Introduction Calorimetry is a versatile non-destructive technique allowing the study of a wide range range of materials in a variety of physical forms. All chemical, physical and biological reactions are accompanied by heat change. These reactions, though sometimes subtle, can be measured using calorimetry. This brochure demonstrates the use of micro-calorimetry as a powerful analysis method with applications in the chemical, pharmaceutical and related fields. • Heat capacity determination • Process development • Thermal stability • Enthalpy of solution by sold...

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µRC micro Reaction Calorimeter-3

Heat Capacity The µRC can be used to rapidly and accurately measure the heat capacity of solids, liquids and mixtures. Applying small temperature steps to the material in question allows the heat required to be measured. Heat capacity can be determined at multiple temperatures within the same experiment. Using these data can significantly improve the data measured using larger reaction calorimeters. Heat capacity of acetone Process Hazard Analysis Hydrolysis reaction The Micro Reaction Calorimeter provides hazard analysis with both speed and flexibility. Working with less than 2ml total volume...

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µRC micro Reaction Calorimeter-4

Kinetic controlled reaction Process Development The µRC is easy to use which allows any chemist or engineer the ability to rapidly investigate whatever reaction parameters they desire. Calorimetry tests can provide users with information on reactant conversion, material accumulation, competitive reactions, inhibition and catalysis. Automated addition of materials allows unattended, walk-away operation and the options of disposable vials and syringes keeps costs to the minimum when conducting many reactions. Additional options such as a pressure handling option and high pressure cells will allow...

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µRC micro Reaction Calorimeter-5

Hydrogenation The process of hydrogenation is much faster and effective when the pressure of the hydrogen atmosphere is increased. As the pressure increases the ability of the hydrogen molecules to permeate the sample is improved. The hydrogenation option simultaneously delivers Hydrogen to sample and reference vials. The power signal from the instrument is used to establish when the reaction is complete. Once the power level returns to the baseline and remains constant, the reaction is considered complete. Gas Flow Option The gas flow option has been used to good effect to study Carbon Capture...

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µRC micro Reaction Calorimeter-6

Titration & Pressure Measurement Specification Baseline noise From 5pW The pRC is supplied with a standard titration tower for automatic addition and utilises a fixed needle reusable syringe. The syringes are available in lOOpL and 250pL volumes. An optional syringe tower is now available that incorporates a second 22 gauge needle, this needle is fixed in place next to the standard titration syringe and connects via a 1/16” Swagelok connector to the pressure transducer. This arrangement is ideally suited to users requiring simultaneous titration and pressure measurement. Dynamic Rage Temperature...

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*Prices are pre-tax. They exclude delivery charges and customs duties and do not include additional charges for installation or activation options. Prices are indicative only and may vary by country, with changes to the cost of raw materials and exchange rates.