XPREP - 3

XPREP - 3

XPREP - 3

Product catalog summary
Overview: The TE Instruments XPREP-3 is a filtration unit designed for preparing samples for both batch (AOX) and column (TOX) methods. It is used in conjunction with an automated halogen analyzer and features three independent operating channels.
Batch Method: This method involves the adsorption of organic halogens onto activated carbon. A mixture of 50 mg activated carbon and 100 mL water sample is shaken for at least one hour. The water is then forced through a quartz frit, leaving the activated carbon behind. Inorganic chlorides are removed with a nitrate wash solution. The quartz frit with activated carbon is then transferred to the AOX analyzer.
Column Method: Similar to the batch method, halogens are adsorbed onto activated carbon inside pre-packed columns. Two columns are used, and a 100 mL sample is filtered through them at a flow rate of 3 mL/min. Inorganic chlorides are washed out, and the carbon content is transferred to the analyzer. The second column acts as a "break-through" check, ensuring the sample is properly adsorbed.
Key Features: The XPREP-3 is easy to use, with a closed filtration system that minimizes contamination risk. It is cost-effective due to its reusable and self-cleaning design. The system ensures no pressure loss over columns or frits, and each channel's pressure is controllable to prevent blockages.
Specifications: The unit measures 50 x 52 x 29 cm and weighs 5 kg. It supports manual filtration with a speed of 0 - 50 mL/min and requires an external gas connection. The operating pressure is adjustable between 0.3 - 3 bar per channel, and it accommodates sample and wash volumes of 10 - 150 mL. Waste is collected centrally with drain capability.
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Catalog excerpts

XPREP - 3-1

// X PREP -3 Effective Batch & Column method pre-treatment for AOX & TOX samples TE Instruments XPREP-3 is a filtration unit into the combustion zone automatically by the designed to prepare samples for both batch NEWTON or by manual introduction. (AOX) and column (TOX) method. After the filtration stage, the samples are introduced in an automated halogen analyzer. The • For the column method, 2 pre-filled columns are connected, using luer-lock fittings for rapid column change or column holder for non independent operating channels, which can be configured to run either batch- or column method: luer-lock columns. After filtration the columns are placed in the T USCAN , or the halogen loaded carbon is cleared from the columns into reusable quartz • For the batch method, a quartz frit is used sample cups, ready for introduction into the to separate the water from the activated combustion zone. carbon after the adsorption stage. Next, the reusable quartz frit is ready for introductio

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XPREP - 3-2

due to closed filtration system No blockage columns Per channel pressure controllable No pressure loss over columns or frit How Does the Batch Method Work? The AOX batch method is based on the Method Work? adsorption of the organic halogens onto Similar to the batch method, halogens are activated carbon. adsorbed onto activated carbon inside a A mixture of 50 mg activated carbon and 100 pre-packed column. 2 columns are joined mL water sample is shaken for at least one together and connected to the filtration unit. Next, 100 mL sample is poured into the regulations. During this treatment stage,...

 Open the catalog to page 2

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*Prices are pre-tax. They exclude delivery charges and customs duties and do not include additional charges for installation or activation options. Prices are indicative only and may vary by country, with changes to the cost of raw materials and exchange rates.