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Dynamic Mechanical Analyzer - DMA 850

Dynamic Mechanical Analyzer - DMA 850
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Dynamic Mechanical Analyzer - DMA 850

Product catalog summary
Introduction
The document introduces the Discovery DMA 850, a dynamic mechanical analyzer known for its high sensitivity, performance, and versatility. It is capable of measuring minimal forces and displacements with precision and ease of use.
Features and Benefits
The DMA 850 includes a non-contact, low mass motor delivering forces from 0.1 mN to 18 N, ensuring high force sensitivity and accuracy. It features an optical encoder with 0.1 nm resolution over a 25 mm range, enhancing versatility. The system includes two environmental systems for precise control and an Air Chiller System for cooling without liquid nitrogen. It is user-friendly with a touch screen and TRIOS software.
Technology and Mechanical Design
The analyzer uses a direct drive motor and frictionless air bearing for control and sensitivity. High-stiffness casting and temperature-controlled transducer eliminate external influences, improving measurement accuracy.
Environmental Control Systems
The DMA 850 offers a Standard Furnace for temperature control from -160°C to 600°C and a DMA-RH Accessory for humidity and temperature control, preventing condensation.
Cooling Systems
The Gas Cooling Accessory extends the range to -150°C using nitrogen gas. Air Chiller Systems provide subambient testing without liquid nitrogen, and the Nitrogen Purge Cooler offers economical cooling and heating.
Clamp Designs
The DMA 850 includes various clamps for different deformation types and sample conditions, enhancing measurement precision and user convenience.
Specifications
The DMA 850 supports various deformation modes and sample sizes, including dual/single cantilever, 3-point bend, tension, shear, and compression. It includes a dual cantilever clamp for powdered materials and shear sandwich mode for soft materials.
Technology Features
The DMA 850 features an app-style touchscreen for usability, allowing experiment control and real-time monitoring. TRIOS software offers advanced data analysis, including onset and endset analysis and modulus crossover.
Advanced Analysis Capabilities
The software supports Time-Temperature Superposition (TTS), activation energy calculation, and custom analysis, with options for calibration, data export, and report generation.
Experimental Design
The DMA 850 allows unlimited test sequencing for complex experimental designs, supporting oscillation, stress control, strain control, and rate control modes.
Applications
DMA evaluates mechanical properties like stiffness and viscoelastic behavior, useful for characterizing thermal events such as glass transition and melting. It also performs creep and stress relaxation tests.
Key Features
The DMA 850 includes Auto-Ranging for parameter selection and DirectStrain for real-time strain control, ensuring accurate measurements.
Key Sections
1. Isostress and Isostrain Experiments
These experiments measure shrinkage or relaxation during thermal transitions by maintaining constant deformation.
2. Properties Measured by DMA
Includes Modulus of Elasticity, Complex Moduli, Damping Properties, Glass Transition, and Secondary Transitions.
3. Applications of DMA
Used to measure glass transition temperature, frequency effects on modulus, and secondary transitions in materials.
4. Specific Material Analyses
Analyzes materials like printed circuit boards and pharmaceutical capsules to understand mechanical properties.
5. Environmental Effects
Discusses the impact of humidity on materials like Nylon 6, affecting mechanical properties and glass transition.
6. Time/Temperature Superposition (TTS)
TTS predicts material performance at different frequencies or time scales.
7. Specifications and Features of DMA Equipment
Outlines specifications including force, frequency range, temperature range, and available features.
Conclusion
The document emphasizes DMA's versatility and sensitivity in analyzing material properties, making it essential in material science and engineering.
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Catalog excerpts

Dynamic Mechanical Analyzer - DMA 850-1

DISCOVER the WORLD'S FINEST DYNAMIC MECHANICAL ANALYZER

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Dynamic Mechanical Analyzer - DMA 850-2

Discover a new DMA that provides Unmatched Sensitivity Superior Performance Maximum Versatility

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Dynamic Mechanical Analyzer - DMA 850-3

The World’s Most SENSITIVE DMA to Measure the Lowest Forces... 5 nm Oscillation Displacements 105 Storage Modulus (MPa) Loss Modulus (MPa) Storage Modulus (MPa) Loss Modulus (MPa)

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Dynamic Mechanical Analyzer - DMA 850-4

with Reliable, Efficient Environmental Systems ...and clamps optimized for ACCURACY and EASE-OF-USE

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Dynamic Mechanical Analyzer - DMA 850-5

Dynamic Mechanical Analyzer TA Instruments invites you to experience the ultimate in Dynamic Mechanical Analyzers, the Discovery DMA 850. Building on superior technologies of the world’s best-selling DMA, improvements in every aspect of DMA performance deliver the most accurate and reproducible measurement of mechanical properties over a wide temperature range. It’s never been easier to get great DMA data! Features and Benefits: • Non-contact, low mass motor delivers continuous forces from 0.1 mN to 18 N to measure everything from soft to stiff materials • Frictionless, low-compliance air bearing...

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Dynamic Mechanical Analyzer - DMA 850-6

Drive System Low Mass, High Stiffness Sample Clamps Responsive Direct Drive Motor The DMA 850’s non-contact motor applies both dynamic and static deformation over the full 25 mm range of motion, providing exceptional control in all modes and clamp positions. The motor is constructed of high-performance lightweight composites that maximize axial and torsional stiffness while minimizing system inertia. Sophisticated control electronics enable the fastest motor control over the widest continuous range of force, from 0.1 mN to 18 N. This enables the system to capture a broad spectrum of material...

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Dynamic Mechanical Analyzer - DMA 850-7

Mechanical Design An accurate mechanical measurement is built on a foundation that completely transfers all motor deformation to the sample, while also eliminating any influence from external Temperature-Controlled Transducer factors such as system resonance, thermal drift or frame deformation. Optimized Mechanics Temperature-Controlled Transducer The critical drive components of the DMA 850 are The transducer is temperature-controlled to eliminate drift mounted within a high-stiffness aluminum casting that associated with temperature changes from the sample or is rigidly mounted to an FEA-optimized...

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Dynamic Mechanical Analyzer - DMA 850-8

Environmental Control Systems Industry-leading ENVIRONMENTAL CONTROL SYSTEMS The DMA 850 offers you a choice of two dedicated environmental systems: the Standard Furnace and the DMA-RH Accessory for humidity and temperature control. Installation is simple, making it convenient to switch between systems as required. All environmental systems and accessories are designed specifically for high performance DMA measurements and seamless integration and are manufactured by TA Instruments. Standard Furnace The Standard Furnace for the DMA 850 is a wide-range bifilar wound furnace that provides uniform...

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Dynamic Mechanical Analyzer - DMA 850-9

The DMA-RH Accessory is a fully integrated unit and includes the following This precision environmental system provides accurate control of sample temperature and relative humidity for DMA experiments. A custom-designed humidity and temperature chamber optimized for mechanical measurements provides stable, reliable control of temperature and humidity over a wide range of operating conditions. The system successfully prevents condensation, a common occurrence in controlled-humidity environments which makes accurate control of relative humidity impossible. Stable, responsive peltier elements precisely...

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Dynamic Mechanical Analyzer - DMA 850-10

Nitrogen Purge Cooler (NPC) Gas Cooling Accessory (GCA) The GCA extends the operating range of the DMA 850 to -150°C. It uses cold nitrogen gas generated from controlled evaporation of liquid nitrogen. Automated filling of the tank can be programmed to occur after the scan is complete. The GCA will provide ballistic or controlled cooling rates over the entire operating range of the DMA 850 (-150 to 600°C). In general, the maximum cooling rate is a function of the installed clamp and the thermal characteristics of the sample. The figure below shows the typical range* of controlled cooling rates...

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Dynamic Mechanical Analyzer - DMA 850-11

Clamp Designs The DMA 850 features clamps in a complete set of deformation types, so a broad range of samples can be accurately analyzed and closely resemble real world process or application conditions. Each clamp is individually optimized for accuracy and ease-of-use. Clamp features and benefits: • High stiffness, low mass designs provide maximum modulus accuracy thermal mass reduces temperature equilibration time and optimizes transition temperature accuracy and precision clamp stiffness calibrations ensure modulus accuracy and repeatability, especially between operators • Simple dovetail...

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Dynamic Mechanical Analyzer - DMA 850-12

Clamp Designs Shear Sandwich Powder Clamp 3-point bending, or free bending, is often considered a Two equal-size pieces of the same material are sheared Parallel plate compression measurements are most suitable for low to The transition temperatures of loose powders can be difficult “pure” mode of deformation because clamping effects are between a fixed and moving plate for the measurement of moderate modulus materials such as foams and elastomers. It can also to measure by mechanical techniques.The powder accessory eliminated. Sample spans of 5 mm, 10 mm, 15 mm, 20 mm, shear modulus, G. This...

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Dynamic Mechanical Analyzer - DMA 850-13

Submersion Clamps 3-Point Bend Compression Submersion Clamps Submersion clamps for the DMA 850 are designed specifically to provide the ideal test conditions for measuring mechanical properties in a fluid environment up to 150°C. Accurate sample temperature is obtained by a thermocouple placed within the fluid reservoir and close to the sample Inert stainless steel construction and a seal-free design ensure compatibility with a wide range of fluids Temperature control provided by the Standard Furnace without additional circulators or environmental systems Deformation Modes and Sample Size * Lengths...

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Dynamic Mechanical Analyzer - DMA 850-14

“APP” Style Touch Screen Revolutionary DMA performance at your fingertips The DMA 850 boasts a brand-new One-Touch-Away™ app-style touchscreen that greatly enhances usability by placing key instrument features at your fingertips. • Ergonomic design for easy viewing and operation • Packed with functionality to simplify operation and enhance user experience The app-style touch screen includes: • Start/stop experiments • Set temperature • Set clamp position • Toggle motor modes • Measure sample • Real-time signals • Test and instrument status at a glance The app-style touchscreen, powerful new TRIOS...

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*Prices are pre-tax. They exclude delivery charges and customs duties and do not include additional charges for installation or activation options. Prices are indicative only and may vary by country, with changes to the cost of raw materials and exchange rates.