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DILATOMETRY PUSH-ROD AND OPTICAL

DILATOMETRY PUSH-ROD AND OPTICAL
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DILATOMETRY PUSH-ROD AND OPTICAL

Product catalog summary
Introduction to Dilatometry
A dilatometer is a precision instrument used to measure dimensional changes in materials as a function of temperature. It is applicable to a wide range of materials including ceramics, glasses, metals, and polymers, providing measurements of properties such as linear thermal expansion, coefficient of thermal expansion (CTE), and sintering temperature.
Dilatometry Measurement Techniques
There are two primary types of dilatometry: push-rod and optical. Push-rod dilatometers use a mechanical contact system, while optical dilatometers use CCD sensors for non-contact measurement. The linear thermal expansion is calculated as the change in length divided by the initial length, and the CTE is the fractional linear change per degree change in temperature.
Push-Rod vs. Optical Dilatometers
Push-rod systems can measure samples from 0.1 to 50 mm and operate from -150°C to 2800°C, whereas optical systems can measure samples from 0.3 to 80 mm and operate up to 1650°C.
True Differential™ Technology
TA Instruments offers True Differential™ technology for enhanced precision and accuracy in thermal expansion measurements, reducing reliance on system calibration and increasing temperature program flexibility.
High-Resolution Horizontal Dilatometer - DIL 830 Series
The DIL 830 Series features True Differential™ technology, optical encoder displacement sensors, and dynamic fast-cool furnaces, offering industry-leading CTE accuracy.
Advanced Vertical Dilatometer - DIL 820 Series
The DIL 820 Series operates in a vertical orientation, allowing for large displacement measurements and high-temperature applications up to 2800°C.
Performance and Technology
The DIL 820 and 830 Series incorporate optical encoders with a displacement resolution of 1 nm, enabling accurate measurement of small dimensional changes.
Specifications
The DIL 820 and 830 Series feature dynamic furnaces with high-tech insulation and active cooling, supporting a wide temperature range and various atmospheres, with a maximum heating and cooling rate of 100°C/min.
Procedures
The document highlights the rapid cooling capabilities of the furnaces, allowing for quick test turnaround.
Norms and Standards
The instruments conform to major standard test methods, including ASTM and DIN standards.
Recommendations
The use of the same furnace for consecutive tests improves reproducibility and reduces errors.
Key Features
The document emphasizes the True Differential™ design for high CTE accuracy, dual-sample operation for increased throughput, and the flexibility of interchangeable furnaces.
Overview of DIL 806 and 860 Series
The document provides a detailed description of the DIL 806 and 860 Series optical dilatometers, highlighting their advanced features, performance data, and applications in material characterization.
Specifications of DIL 806 and 860 Series
The DIL 806 features a rapid heating capability of up to 100 °C/min and can cool from 1400 °C to 50 °C in under 10 minutes. The 860 Series offers a maximum temperature of 1650 °C with heating rates up to 200 °C/sec.
Technology
Both series utilize a non-contact optical system, allowing for the testing of irregularly shaped and soft samples.
Performance Data
The document includes performance graphs showing temperature uniformity and dimensional changes.
Software
The Misura 4™ software suite offers comprehensive control and analysis capabilities.
Applications
The instruments are suitable for characterizing raw materials, semi-finished products, and optimizing manufacturing processes.
Specifications Overview
The document provides detailed specifications for the DIL 806 & 860 series, focusing on resolution, measuring range, CTE accuracy, temperature range, heating rate, atmosphere, and contact force.
Dilatometry Applications
The applications section highlights the use of dilatometry in measuring glass transition and softening temperatures, simulating fast firing cycles, and studying sintering processes.
Fast Firing and Sintering
Fast firing technology is discussed as a cost-effective method for processing ceramics.
Pyroplasticity and Fleximetry
The study of pyroplastic deformation using the Absolute Fleximeter mode is detailed.
Heating Microscopy and Material Characterization
Heating microscopy is used to identify characteristic shapes and temperatures of materials.
Solid Oxide Fuel Cell (SOFC) Compatibility
The document discusses the importance of understanding layer behavior during co-sintering of SOFCs.
Mold Powder and Ash Fusibility
Characterization of mold powders for continuous casting and ash flow temperature analysis for solid fuels are covered.
Industry-Leading Sales & Support
TA Instruments highlights its commitment to customer support, with a global team providing exceptional service across 23 countries and 5 continents.
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Catalog excerpts

DILATOMETRY PUSH-ROD AND OPTICAL-1

DILATOMETRY PUSH-ROD AND OPTICAL

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DILATOMETRY PUSH-ROD AND OPTICAL-2

HIGH-PERFORMANCE DILATOMETERS A dilatometer is a precision instrument for the measurement of dimensional changes in material as a function of temperature. Dilatometry can be used to test a wide range of material including traditional and advanced ceramics, glasses, metals, and polymers. It provides measurements of a wide variety of properties including linear thermal expansion, coefficient of thermal expansion, sintering temperature, shrinkage steps, phase transitions, density change, softening point and decomposition temperature, anisotropic behavior, and glass transition temperature. No single...

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DILATOMETRY PUSH-ROD AND OPTICAL-3

DILATOMETRY and the Measurement of DIMENSIONAL CHANGES Understanding DILATOMETRY MEASUREMENT TECHNOLOGIES: PUSH-ROD vs. OPTICAL In a dilatometry experiment, a sample is placed into a holder with one end brought into contact with a push-rod. Alternatively, for a non-contact measurement, the sample is framed by optical CCD sensors. The sample and holder are then enclosed within a furnace where the sample is subjected to a prescribed temperature program of heating, cooling, or isothermal conditions. During the experiment, the linear dimensional change (expansion or contraction) of the sample is...

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DILATOMETRY PUSH-ROD AND OPTICAL-4

Push-rod Dilatometry True DifferentialTM Technology Sapphire Certified Reference CTE: True DifferentialTM vs. Quasi-Differential Unique True Differential™ Technology Provides UNMATCHED PRECISION and ACCURACY for THERMAL EXPANSION MEASUREMENTS The main components of a push-rod dilatometer are a measuring head consisting of a displacement sensor True Differential™ vs. Quasi-Differential and force controller to apply load to the sample, a measuring system consisting of a sample holding tube and a movable furnace. The sample is sandwiched As the temperature changes during an records a signal that...

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DILATOMETRY PUSH-ROD AND OPTICAL-5

HIGH-RESOLUTION HORIZONTAL DILATOMETER DIL 830 Series The DIL 830 Series features an impressive array of unique technologies and capabilities that make it the ideal choice for any R&D laboratory in need of the most accurate measurements of dimensional properties of materials. The instruments include exclusive True Differential™ technology, optical encoder displacement sensor, new fast-cool dynamic and motorized furnaces, measuring head housing with active thermal stabilization, touch screen display, and the new linear sample load motor. The result is the highest performing horizontal push-rod...

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DILATOMETRY PUSH-ROD AND OPTICAL-6

ADVANCED VERTICAL DILATOMETER DIL 820 Series VERTICAL DESIGN for the Most CHALLENGING APPLICATIONS Features and Benefits: • Exclusive True Differential™ technology reduces reliance on system calibrations and provides industry-leading CTE accuracy of 0.01 x 10-6 K-1 DIL 820 Series dilatometers operate in a vertical orientation making them uniquely capable of conducting experiments simply not possible on a horizontal design. Some examples include applications where displacement from expansion or shrinkage is large such as Rate Controlled Sintering (RCS), higher temperature applications up to 2800°C,...

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DILATOMETRY PUSH-ROD AND OPTICAL-7

DIL 820 & 830 SERIES PERFORMANCE DATA Measurement of Nanoscale Expansion on 650 Micron Thick Sample True Differential™ technology, available on DIL 822 and DIL 832 models, delivers unparalleled performance right where it is most needed in dilatometry: CTE accuracy. With the industry-leading value of 0.01 x 10-6 K-1, it provides the confidence in analysis scientists and engineers require for testing and evaluating today’s high-value and high-performance materials. Note: Refer to page 5 for a detailed explanation of the True Differential TM approach. Optical Encoder Measures Nanoscale Dimensional...

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DILATOMETRY PUSH-ROD AND OPTICAL-8

SPECIFICATIONS DIL 820 & 830 SERIES FURNACE OPTIONS Depending on furnace option. See furnace specifica

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DILATOMETRY PUSH-ROD AND OPTICAL-9

HORIZONTAL DILATOMETER DIL 800 SERIES All TA Instruments 800 Series horizontal dilatometers are precision instruments employing state-of-the-art Linear Variable Differential Transducer (LVDT) and digital amplifier technology. They are available in single-sample, dual-sample, and True Differential™ configurations. Version “L” models perform tests in air only, making them ideally suited for characterizing ceramics or other materials processed in air. Standard models can be run in air, inert, reducing, or vacuum atmospheres. These Traditional HORIZONTAL DESIGN, INDUSTRY-TESTED, RUGGED and RELIABLE...

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DILATOMETRY PUSH-ROD AND OPTICAL-10

DIL 800 SERIES PERFORMANCE DATA Sapphire Standard: CTE Measurements from -150 °C to 1500 °C Rugged and Reliable Transducer Technology Accurate and Consistent Over Broad Temperature Range Differential Transducer (LVDT) and digital amplifier technology. These transducers are thermally-stabilized and designed to be shock-proof for the ultimate in sensitivity, accuracy, precision and ruggedness. Every changes that these materials experience. The 802 True Differential™ Dilatometer provides that efficient contact is maintained even during processes that may involve contraction of the sample. superior...

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DILATOMETRY PUSH-ROD AND OPTICAL-11

FURNACE OPTIONS DIL 800 SERIES SPECIFICATIONS All DIL 800 Series horizontal dilatometers can be configured with a wide range of furnace options depending on the temperature range requirements. Furnaces are easily interchangeable, providing the utmost in configuration flexibility. Multiple furnaces of the same type can also be used to increase throughput on a single instrument. (*) Depending on furnace option. See furnace specifications for full details.

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DILATOMETRY PUSH-ROD AND OPTICAL-12

CONTACTLESS MEASUREMENTS make Unconventional Dilatometry POSSIBLE TA Instruments’ patented Shadow-Meter technology(1) allows contactless measurements of thermal expansion and contraction of thin or irregularly shaped samples of soft materials. Unaffected by system thermal expansion that can be caused by changes in temperature, the DIL 806 offers an intrinsically absolute measurement and does not need the test-specific calibrations that are required with traditional push-rod dilatometers. Features and Benefits: • Patented design requires no contact with sample allowing for maximum flexibility...

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