Glass Reaction System
49Pages

GLASS REACTION SYSTEM – PROCESS DIVISION Steroglass St l GLASS REACTION O SYSTEM

2013 PRODUCT OVERVIEW – PROCESS DIVISION MAIN TARGETS: Chemical reactions and Ch i l ti d study/production of molecules, polymers, etc.

2013 PRODUCT OVERVIEW – PROCESS DIVISION MAIN TARGETS Steroglass Glass Reaction Systems are y suitable for chemical process d development, l t scale up and process simulation

2013 PRODUCT OVERVIEW – PROCESS DIVISION SYNTESIS PROMO STRIKE 300 LABORATORIES Organic Chemistry Pharmaceutical Chemistry Industrial Chemistry Food

2013 PRODUCT OVERVIEW – PROCESS DIVISION -SMART -MULTI MULTI -CONTROL

2013 PRODUCT OVERVIEW – PROCESS DIVISION

2013 PRODUCT OVERVIEW – PROCESS DIVISION SMART PROMO STRIKE 300 This is the configuration for a fi ti f smart basic reaction package. Manual valves and operations, local analogic instruments, mainly intended to b used with a thermocirculator with be d i h h i l i h a special fluid in the vessel jacket.

2013 PRODUCT OVERVIEW – PROCESS DIVISION

2013 PRODUCT OVERVIEW – PROCESS DIVISION The classical multipurpose configuration. The number and the type of the co po e ts a o components allow a wide range of de a ge o operations. The package comes with a PLC to record and visualize the critical parameters of the process process.

2013 PRODUCT OVERVIEW – PROCESS DIVISION

2013 PRODUCT OVERVIEW – PROCESS DIVISION CONTROL PROMO STRIKE 300 This is the ultimate version in terms of performance. Triple Walled Glass Reactor or Glass Lined Reactor for the most demanding operations, from –90°C up to 200°C. The package comes with a PLC to record and visualize the critical d d i li th iti l parameters of the process.

2013 PRODUCT OVERVIEW – PROCESS DIVISION 3 MAIN CONFIGURATIONS ALREADY AVAILABLE SMART Glassware Multiple choice Glass lined Special Steel Temperature p Product and reading vapour analogic Product, vapour Product, vapour and and receiver with receiver with remote remote temperature temperature probes probes Visualization and Vi li ti d Visualization and management of the management of the parameters with a parameter with a PLC PLC based software based software

2013 PRODUCT OVERVIEW – PROCESS DIVISION 3 MAIN CONFIGURATIONS ALREADY AVAILABLE PROMO STRIKE 300GMP directives as option Phase separator Depending Depending on the on the vessel vessel -80°/+200°C -80°/+200°C

2013 PRODUCT OVERVIEW – PROCESS DIVISION STANDARD PACKAGES:

2013 PRODUCT OVERVIEW – PROCESS DIVISION SOME PACKAGE EXAMPLES -5 & 10 lt DOUBLE JACKETED GLASS MULTI PURPOSE REACTION UNITS UNDER VACUUM -20 lt DOUBLE JACKETED GLASS MULTI PURPOSE REACTION UNIT UNDER VACUUM -25 lt & 50lt EX-PROOF DOUBLE JACKETED GLASS MULTI PURPOSE REACTION UNITS UNDER VACUUM - 25 lt & 50lt EX-PROOF DOUBLE JACKETED HASTELLOY MULTI PURPOSE REACTION UNITS UNDER VACUUM -50lt GLASS ROUND VESSEL WITH OIL BATH MULTIPURPOSE REACTION UNIT -100 & 200 lt ARE AVAILABLE UPON REQUEST

2013 PRODUCT OVERVIEW – PROCESS DIVISION 5 & 10 lt DOUBLE JACKETED GLASS MULTI PURPOSE REACTION UNITS UNDER VACUUM

2013 PRODUCT OVERVIEW – PROCESS DIVISION 20 lt DOUBLE JACKETED GLASS MULTI PURPOSE REACTION UNIT UNDER VACUUM Vacuum pump

2013 PRODUCT OVERVIEW – PROCESS DIVISION 25 lt & 50lt EX-PROOF DOUBLE JACKETED GLASS MULTI PURPOSE REACTION UNITS UNDER VACUUM

2013 PRODUCT OVERVIEW – PROCESS DIVISION 25 lt & 50lt EX-PROOF DOUBLE JACKETED HASTELLOY MULTI PURPOSE REACTION UNITS UNDER VACUUM

2013 PRODUCT OVERVIEW – PROCESS DIVISION 50lt GLASS ROUND VESSEL WITH OIL BATH MULTI-PURPOSE REACTION UNIT Vacuum Rupture disk Nitrogen Vacuum Feed load Solid load

2013 PRODUCT OVERVIEW – PROCESS DIVISION MAIN FEATURES -5, 10, 25, 50 liter 3.3 borosilicate glass reactors, interchangeable, graduated, jacketed for thermal fluid recirculation - Other vessel construction material: glass lined, Hastelloy C, round type borosilicate glass with oil b th b ili t l ith il bath - -1.0 to + 0.5 bar / - 45 (-90) to + 200°C (extra low temperature achievable with triple wall jacketed vessels) - 10 280 rpm continuous adjustable stirrer with a 0.22 kW 400Vac 10...280 0 22 induction motor -Dry running mechanical seal, option magnetically coupled seal -Ex-proof version...

2013 PRODUCT OVERVIEW – PROCESS DIVISION Frame - Stainless steel tubing, to suit available space - Laboratory fume hood for contained operations as optional Cover plate -Material of construction: borosilicate glass, PTFE coated steel, glass li d steel l lined t l - DN80 fast-action closure for solids addition - Standard version with flat flange connections - Various options of connections available Glass overhead Distillation overhead consisting of: - f d vessel feed l - Vapor duct with reflux splitter, automatic or simple - coil heat exchanger - graduated glass receiver vessel - Vacuum...

2013 PRODUCT OVERVIEW – PROCESS DIVISION Stirrer - Interchangeable stirrers made of PTFE - Blade stirrer made of solid PTFE -Wide range of stirrer style: anchor, impeller, turbine, rushton type Sensor and controls -Vacuum -Product temperature, temperature -Vapor temperature, -pH Safety -Rupture disk: 0.49Barg For a correct configuration please ask for Pilot Plant Questionnaire

2013 PRODUCT OVERVIEW – PROCESS DIVISION Reactor Components: -Glass reactor single wall with direct heating with oil bath/electric heating. h ti ith il b th/ l t i h ti -Glass reactor double wall with jacket recirculation -Glass reactor triple walled with jacket recirculation -Full Glass lined/bottom glass lined -Glass Cover or low profile Glass Lined Glass Cover

2013 PRODUCT OVERVIEW – PROCESS DIVISION Stirring & Coupling: Basic d B i dry seal with PTFE stirring shaft l ith ti i h ft Different design available (anchor,impeller,turbine ) (anchor impeller turbine ...) Magnetic coupling as option ATEX version always available as option Baffles ,made of glass of PTFE Optional Glass Lined