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SERVOPRO NanoTrace DF-760E/760E Ultra

SERVOPRO NanoTrace DF-760E/760E Ultra
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SERVOPRO NanoTrace DF-760E/760E Ultra

Product catalog summary
Safety Summary
This section stresses the importance of following installation, operation, and maintenance procedures as outlined in the manual. It highlights user responsibility for safety, particularly regarding flammable and toxic gases, and notes that unauthorized modifications void warranties.
Introduction
The document introduces the DF-745/DF-749 Analyzer, detailing its dimensions, internal components, and specifications related to moisture detection, electrical requirements, laser specifications, and environmental conditions.
Installation, Startup, and Shut Down
Procedures for unpacking, installing, starting up, and shutting down the analyzer are outlined, including gas flow and pressure regulation and the use of isolation valves.
Options
Various options for the analyzer are discussed, such as key lock, operating voltage, serial communications, analog voltage output, isolation valves, hydrogen safety system, and vacuum pump.
Connecting to External Devices
Instructions for connecting the analyzer to external devices via serial communication ports, analog signal outputs, and relay ports are provided.
User Interface
This section describes the data display screen, keypad, and menu structure, including main menu functions, calibration, data history, and diagnostics.
Sample Gas Preparation and Delivery
Guidelines for preparing and delivering sample gas are given, focusing on sample pressure, flow rate effects, and handling flammable gases.
Service
Information on maintenance, including fuse replacement, moisture cell maintenance, and troubleshooting, is provided. It also covers shipping and disposal procedures.
Theory of Operation
The principles of moisture measurement and absorption spectroscopy are explained.
Specifications
Detailed specifications for moisture measurement, output signals, status indicators, and power requirements are listed.
Appendix A – Hydrogen Safety System
This appendix provides additional information on the hydrogen safety system, including installation instructions.
Specifications Summary
  • Moisture Detection: LDL is 1 ppb, resolution of 100 ppt, accuracy of ±3% of reading or ±1 ppb.
  • Electrical Requirements: 100 to 120 VAC, 50/60 Hz, 5 Amps, optional 200 to 240 VAC, 50/60 Hz, 2.5 Amps.
  • Laser Specifications: Max Power 50mW/30mW, beam divergence 436 mrad.
  • Environmental Conditions: Indoor use, operating temperature 10°C to 40°C, humidity up to 80% at 31°C.
Installation, Start-up, and Shutdown
Installation involves mounting the analyzer, connecting gas supplies, and making power connections. Proper handling and lifting techniques are necessary due to the analyzer's weight. The start-up process includes turning on the power and allowing the system to warm up.
Warm-Up Process: The analyzer requires a warm-up period of 6 to 15 minutes, potentially extending to 90 minutes depending on environmental conditions.
Gas Flow and Pressure Regulation: The system delivers a gas flow rate of 1 liter per minute to the moisture sensor. Pressure settings vary by gas type.
Back Flow Prevention System: Available only with isolation valves, it prevents contamination by engaging isolation valves when flow drops below 0.1 lpm.
Download System Data: After installation, system data should be downloaded and optionally sent to Servomex for verification.
Options: Various options are available, including key locks, operating voltage settings, serial communications, analog voltage output, isolation valves, hydrogen safety systems, and vacuum pumps.
Connecting to External Devices: The analyzer supports connections to external devices via rear panel ports, with options for serial communication and analog signal outputs.
Relay Specifications and Wiring:
Relay contacts are rated at 30 VDC, 1A, and are not designed for AC power switching. They are wired for Fail Safe operation.
User Interface Overview:
The user interface includes a Data Display Screen that shows alarm status, concentration measurements, and gas pressure. The keypad allows control over the analyzer's features.
Calibration Procedures:
The Calibrate Menu includes options for checking and adjusting zero levels, emphasizing the importance of ensuring moisture-free gas during manual zero calibration.
Data History and Download:
The Data History Screen displays data in strip chart form, with options to adjust the time scale. Data can be downloaded to a USB stick.
Diagnostics Menu
Includes submenus for Active Zero On/Off, Test Relays, Test Analog Voltage Output, Signal Monitor, Vacuum Source Capacity Test, Cell Pressure Calibration, and Manual Cell Pressure Override.
Power Up Default
Sets the default state of isolation valves after power up.
Communications
Sets parameters for serial PC communications, including baud rate selection.
Download System Data
Enables downloading of internal system data files to a USB stick for evaluation by Servomex.
Firmware Upgrade
Instructions for firmware upgrades involve inserting a memory stick with necessary files and following on-screen prompts.
Sample Gas Preparation and Delivery
Proper operation depends on maintaining specified sample gas pressure ranges, with special precautions for flammable gases like hydrogen.
Service and Maintenance
Guidelines for returning analyzers include obtaining a Return Material Authorization number. Maintenance cautions emphasize safety.
Troubleshooting and Disposal
Outlines troubleshooting steps for moisture-related issues and provides shipping instructions to prevent damage.
Theory of Operation
The NanoTrace Moisture Analyzer uses infrared absorption spectroscopy to measure moisture.
Moisture Detection Specifications:
- LDL: 1 ppb under constant conditions.
- Accuracy: Greater of ±3% of reading or ±1 ppb.
- Speed of Response: Less than 3 minutes to reach 90% of an upward step change.
- Upset Recovery Time: Less than 5 minutes to stabilize within 10 ppb after a high ppb upset.
- Range: 0-20 ppm.
- Background Gas Compatibility: N2, H2, He, Ar, O2, and CO2.
- Cell Pressure: Variable from 180 – 760 Torr based on background gas.
General Specifications:
- Construction: NEMA 1 (IP10), 19-inch rack mount.
- Dimensions: 19 inch wide x 10.5 inch high x 22.5 inch deep.
- Display: 10.1-inch LCD Color 1024X600.
- Weight: 73 pounds.
- Environmental: Altitude up to 2000 meters, operating temperature 10° C to 40° C, humidity 95% non-condensing.
- Storage Temperature: Not to exceed 50° C.
- Required Sample Conditions: Oil free, non-corrosive, non-condensing, filtered for particulates to 2μm.
Gas Routing:
- Gas Inlet, Sample: Flow Rate 1.3 slpm total, Inlet Pressure 18 to 150 psig.
- Vent: Vent to atmosphere, pressure limits -2 to 2 psig.
- Gas Inlet, Pneumatic: Gas N2 or air, Inlet Pressure 70 to 100 psig.
- Gas Inlet, Aspirator: Flow Rate 15 slpm, Gas N2 or air, Inlet Pressure 80 psig.
- Gas Path Construction Materials: Various metals and plastics including Stainless Steel and Hastelloy C22.
Output Signals & Status Indicators:
- Alarm Relays: Four non-latching, independently assignable to moisture alarms.
- Analog Output: User scalable 0-2 ppb to 0-20 ppm Moisture.
- Visual Alarm Status Indicators: Moisture levels, Temperature, Cell Pressure Range, System Error, etc.
- Digital Communications: RS-232 or RS-485.
Laser Specifications:
- Max Power: 50mW/30mW.
- Beam Divergence: 436 mrad.
- Pulse Pattern: Continuous Wave.
- Analyzer Classification: Class 1.
Power and Compliance:
- Power: 100 to 120 VAC, 50/60 Hz, standard, 5 Amps; 200 to 240 VAC, optional, 2.5 Amps.
- Compliance: EMC Directive 2014/30/EU, EU Low Voltage Directive.
Warranty:
- Warranty covers defects in material and workmanship for one year from delivery.
- Limitations include no liability for consequential damages and no warranty of fitness for a particular purpose.
Appendix A – Hydrogen Safety System:
- Designed to safeguard against explosion hazards when operating on hydrogen sample gas.
- Includes air circulation fans, sample delivery interlock valve, and analyzer case purge valve.
- Installation requires specific connections and adjustments for safe operation.
- Operation involves automatic safety checks and purging with nitrogen gas to maintain safe conditions.
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Catalog excerpts

SERVOPRO NanoTrace DF-760E/760E Ultra-1

SERVOPRO NANO Trace DF-745/DF-749 Analyzer Installation and Operator Manual Part Number: Revision: Language:

 Open the catalog to page 1
SERVOPRO NanoTrace DF-760E/760E Ultra-2

IMPORTANT INFORMATION Continued safe and reliable operation of this equipment is conditional on all installation, operation and maintenance procedures being carried out in accordance with the appropriate manuals, by personnel having appropriate qualifications, experience, and training. Failure to observe the requirements of the manual may result in the user being held responsible for the consequences and may invalidate any warranty. Servomex will accept no liability for unauthorized modifications to Servomex supplied equipment. Servomex has paid particular attention to Health and Safety throughout...

 Open the catalog to page 2
SERVOPRO NanoTrace DF-760E/760E Ultra-7

About this manual About this manual Safety information The following icons are used throughout this manual to iden�fy any poten�al hazards that could cause serious injury to people or damage to the equipment: This symbol warns of specific hazards which, if not considered, may result in personal injury or death. This symbol warns of specific hazards from laser radia�on. This symbol warns of specific hazards from the presence of electrical voltage and current. . Other information provided by the manual This symbol highlights where you must take special care to ensure the Analyser or other equipment,...

 Open the catalog to page 7
SERVOPRO NanoTrace DF-760E/760E Ultra-8

About this manual Getting Started Thank you for selecting the NanoTrace DF-745/749Analyzer. Servomex designs, manufactures, exhaustively tests, and supports every analyzer under the tightest quality controls. You can expect every Servomex analyzer to arrive in perfect condition and provide years of trouble-free service if maintained properly. Please call your nearest Servomex Business Center if you need assistance. Quality The NanoTrace DF-745/749 Analyzer has been designed and manufactured under ISO-9001 controls, thus helping to ensure the highest possible standards of quality. Every analyzer...

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SERVOPRO NanoTrace DF-760E/760E Ultra-9

Safety Summary Safety Summary General Warnings and Cautions Hazardous AC voltages are present within this instrument. Do not remove the top or left side covers — no user-serviceable parts are located under the covers. Do not connect this analyzer to AC power until all signal cables and plumbing have been connected. Disconnect the analyzer from AC power before installing or removing external connections, the sensor, the electronics, or when charging or draining electrolyte. Disconnect the analyzer from AC power before moving the analyzer. WARNING: AC POWER GROUND REQUIRED Ensure that power cord...

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SERVOPRO NanoTrace DF-760E/760E Ultra-10

Safety Summary DANGER Potentially hazardous AC voltages are present within this instrument. Leave all servicing to qualified personnel. Disconnect the AC power source when installing or removing external connections, the sensor, or electronic components. CAUTION Do not set up or operate the analyzer without a complete understanding of the instructions in this manual. Do not connect this analyzer to a power source until all signal and plumbing connections are made. CAUTION This analyzer must be operated in a manner consistent with its intended use and as specified in this manual. WARNING: ENSURE...

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SERVOPRO NanoTrace DF-760E/760E Ultra-11

Safety Summary The DF-745 analyzer is a Class 1 laser device (per BS EN 60825-1:2014 and 21CFR 1040.10 and 1040.11 except for deviations pursuant to Laser Notice No. 56, 5 May 2019). It contains a laser emitter inside the moisture sensor, which is sealed and not user serviceable. Do not disassemble or modify the moisture sensor. Exposure to laser emissions may result in injury, including damage to the eyes. © Servomex Group Limited. 2021

 Open the catalog to page 11
SERVOPRO NanoTrace DF-760E/760E Ultra-12

Safety Summary Safety Labelling and General Marking Loca�on of Informa�onal product marking and safety labelling on the DF-745/749 is shown in Figure 1, Figure 2, and Figure 3. Figure 1: Analyzer Markings Shown in Rear Area View Figure 2: Sensor Markings – Side © Servomex Group Limited. 2021

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SERVOPRO NanoTrace DF-760E/760E Ultra-13

Safety Summary Figure 3: Sensor Marking – Front © Servomex Group Limited. 2021

 Open the catalog to page 13
SERVOPRO NanoTrace DF-760E/760E Ultra-14

Product Description The NanoTrace DF-745 and DF-749 moisture analyzers are designed for con�nuous UHP (Ultra High Purity) analysis of moisture content in process gases. These instruments have a similar design that includes the following external features: a steel chassis enclosure that accommodates rack moun�ng, 6 x 9-inch LCD screen, push-buton keys for user-interface, gas panel containing ports for input and output of gasses (process and pneuma�c), flowmeter (op�onal), connectors for digital and analog data output, and an IEC 60320 C-13 receptacle for connec�on to electrical power. Internal...

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SERVOPRO NanoTrace DF-760E/760E Ultra-15

Figure 5: DF-745/749 Analyzer (rear) © Servomex Group Limited. 2021

 Open the catalog to page 15
SERVOPRO NanoTrace DF-760E/760E Ultra-16

Internal Components The DF-745/749 Analyzer’s major internal components are depicted in Figure 7, below. Figure 7: Major Internal Components Specifications Summary A summary of DF-745/749 characteris�cs is provided in the paragraphs below. Complete specifica�ons are provided in Chapter Error! Reference source not found. Specifica�ons. Moisture Detection Lowest Detection Level (LDL): 1 ppb @ Constant Conditions Resolution: Analytical (Smallest Detectable Change): 100 ppt Display: .01 ppb Accuracy: Greater of ±3% of reading or ±1 ppb @ Constant Conditions Background Gas Compatibility: N2, H2, He,...

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SERVOPRO NanoTrace DF-760E/760E Ultra-17

Laser Specifications Max Power: 50mW/30mW Beam Divergence: 436 mrad Pulse Pattern: Continuous Wave Classifica�on: Laser Device- Class 3, Analyzer-Class 1 (per BS EN 60825-1:2014 and 21CFR 1040.10 and 1040.11 except for devia�ons pursuant to Laser No�ce No. 56, 5 May 2019) Environmental Operating Conditions Altitude: 2000 meters (6500 feet), max Ambient Operating Temperature: 10° C to 40° C (50° F to 105° F) Humidity: 80% humidity for temperatures up to 31°C, decreasing linearly to 50% relative humidity at 40°C Exposure to Weather: Indoor use only in a clean and dry, non-hazardous area of pollution...

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SERVOPRO NanoTrace DF-760E/760E Ultra-18

Installa�on, Start-up, and Shutdown 3 Installation, start-up, and Shut Down 3.1 Unpacking Procedure Follow the procedure below to unpack your DF-745/749 NanoTrace Analyzer: 1. Examine the condition of the packaging and its contents. If any damage is apparent, immediately notify the carrier and Servomex. Do not proceed with the installation. 2. Check the contents against the packing slip to make sure the shipment is complete. Unattached equipment may be shipped with the analyzer in supplemental packaging. Shortages should be reported to Servomex immediately. 3. All standard NanoTrace analyzers...

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