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DF550E Operator Manual 082616

DF550E Operator Manual 082616
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DF550E Operator Manual 082616

Product catalog summary
Introduction
The DF-550E Oxygen Analyzer, manufactured by Servomex Corporation, adheres to ISO-9001 standards for quality and reliability. It is calibrated with gases traceable to NIST standards and requires regular maintenance for accuracy.
Unpacking and Initial Setup
Inspect the packaging for damage and verify contents against the packing slip. Ensure the voltage setting matches your requirements before installation.
Installation and Maintenance
Proper installation is crucial for optimal performance. The manual provides detailed instructions on adding electrolyte, making gas and electrical connections, and powering up the device. Regular maintenance, including calibration and sensor upkeep, is necessary for sustained operation.
Specifications
The manual outlines the technical specifications of the DF-550E, including operational parameters and environmental requirements.
Calibration and Operation
The analyzer supports both manual and automatic calibration systems. It includes procedures for setting up gas connections and controlling calibration components. The device features standard outputs and alarms for monitoring performance.
Options and Accessories
Various options are available, such as stainless steel tubing, battery packs, and communication ports, to enhance functionality and integration with other systems.
Sample Gas Handling
Guidelines are provided for preparing and delivering sample gases, including considerations for flow rate, pressure, and compatibility with the analyzer's components.
User Interface
The analyzer features a data display screen and keypad for user interaction. The main menu and controls menu allow for configuration and monitoring of system parameters.
Service and Troubleshooting
Maintenance procedures, including calibration and sensor maintenance, are detailed. A troubleshooting section helps diagnose and resolve common issues. A list of replaceable spare parts is also provided.
Conclusion
The DF-550E Oxygen Analyzer is a robust and reliable instrument for measuring oxygen levels in various industrial applications. Proper installation, operation, and maintenance are essential for ensuring its long-term performance.
Shipment Procedure
The document outlines the shipment procedure for the DF-550E analyzer, emphasizing the importance of draining and rinsing the sensor before shipping to prevent damage.
Theory of Operation
This section explains the functioning of the sensor and the electrolyte conditioning system, detailing how these components work together to ensure accurate measurements.
Safety
The safety section includes symbols and explanations, terms and definitions, and Material Safety Data Sheets (MSDS) for various solutions used in the analyzer. It highlights the importance of handling the electrolyte solution with care due to its caustic nature.
Warranty
The analyzer comes with a 5-year sensor warranty, with specific terms outlined in the warranty section.
Cautions
This section provides warnings and cautions to prevent damage to the analyzer and ensure user safety. It stresses the importance of operating the analyzer as specified in the manual and highlights potential hazards such as AC voltages and caustic liquids.
Specifications
The specifications section details the operational range, detection levels, accuracy, response time, and environmental conditions for the analyzer. It also describes the construction materials, power requirements, and output signals.
Figures and Tables
The document includes numerous figures and tables that provide visual aids and detailed data, such as calibration system logic, battery operation time, and gas scale factors.
Audible/Visual Alarm Status Indicators
Includes four oxygen, one temperature, and one electrolyte condition alarm (standard), and one low flow alarm (optional).
Alarm Relays
Up to 4, non-latching, independently assignable to alarms or calibration-in-process indicators.
Construction
NEMA 1.
Specifications
Dimensions: 12.2-inch wide x 8.9-inch high x 10.0-inch deep. Weight: 18 pounds (approximate).
Installation and Setup
Procedure for installation without options, voltage output set to 0-10 VDC.
Adding Electrolyte
Electrolyte is caustic; review MSDS before handling. Use only Hummingbird Brand E-Lectrolyte Gold.
Sample Gas Connections
Stainless steel bulkhead fittings for inlet and outlet. Supply with N2 sample low in O2.
Electrical Connections
Ensure power switch is OFF before connecting. Verify operating voltage.
Powering Up
Turn on power, unit undergoes diagnostic procedures. TEMP CAL message appears for 1.5 minutes.
Calibration Systems
Zero baseline establishment is crucial. Manual or Automatic Calibration options available.
Manual Calibration System Setup
Portable system with optional sample gas pressure regulator.
Automatic Calibration System Setup
Separate fittings for sample and span gas connections.
Overview
This document provides detailed instructions for the installation, setup, and operation of the DF-550E NanoTrace Oxygen Analyzer.
1. Specifications and Setup
Ensure the sample gas regulator is gradually opened to achieve the required flow rate.
2. Calibration and Purging
Automated calibration involves switching between process gas and zero gas to stabilize readings.
3. Calibration System Design
Users can design their own calibration systems using provided internal components and firmware.
4. Outputs and Alarms
Oxygen concentration outputs are available via non-isolated 4-20 mA or 0-10 VDC outputs.
5. Pressure Regulator and Purge
Optional gas pressure regulators can be installed, with specific mounting instructions provided.
6. Flow Control and Isolation Valves
Ultra High Purity (UHP) flow control valves can be used for flow control and isolation.
7. Nitrogen Case Purge System
An optional nitrogen purge system is available to reduce explosion hazards by purging the enclosure.
8. Portable Operation
Procedures for portable operation include isolating the sensor and managing power and gas connections.
9. Options
Stainless steel outlet tubing and NiMH battery packs are available for enhanced functionality and portability.
Battery Charging and Operation
The analyzer's battery charges only when connected to AC power with the power switch on.
NiMH Battery and Case Purge Option
If the NiMH Battery Option is installed alongside the Case Purge Option, the battery system must be disabled.
Battery Operation Time
The battery can power the analyzer for different durations depending on the configuration.
Key Lock and Security
An optional key lock can be installed to prevent access to internal components.
4-20 mA Output
The analyzer can be equipped with a fully-isolated 4-20 mA output.
Relays
Up to four optional relays can be assigned to alarms.
Mounting Options
The analyzer can be mounted using a panel or a 19-inch rack mount.
Communication Ports
RS232C or RS485 ports are available for interfacing with other systems.
Sample Gas Preparation and Delivery
The STAB-EL Acid Gas System reduces sensitivity to low levels of acids in the sample gas.
Sample Gas Compatibility
The analyzer should be installed with preconditioned sample gas to avoid condensation.
Solubility and Reactivity with KOH Electrolyte
Gases rated as "Soluble" to "Infinitely-Soluble" can threaten the sensor.
Flammable Sample Gas
The analyzer system cannot ignite flammable gases, but precautions should be taken.
Trace Acids in Sample Gas
The STAB-EL Acid Gas system allows oxygen measurements in gases with trace acids.
Sample Gas Temperature
Gas temperature should remain between 0°C and 50°C.
Protecting the Analyzer
Protect the analyzer from high oxygen concentrations and hostile gases.
Calibration Gas Considerations
Calibration standards should be in aluminum cylinders for stability.
Connecting to External Devices
The analyzer supports connections to external devices via rear panel ports.
Relay and Option Ports
The analyzer includes relay ports for alarms and option ports for analog outputs.
Calibration and Analog Output
The document begins with instructions for calibrating the analog output of the DF-550E Oxygen Analyzer.
User Interface Overview
The user interface section describes the Data Display Screen.
System Flags and Messages
Various system flags alert users to maintenance needs.
Keypad Functionality
The keypad allows navigation through menus and data entry.
Main Menu Navigation
The Main Menu provides access to all other menus.
Controls Menu
This menu allows users to set default conditions and activate optional features.
Setup Analyzer Menu
The Setup Analyzer Menu is used to configure various parameters.
Alarm Configuration
The document details the setup of alarms.
Flow Switch Trip Points
Table 10 lists the flow switch trip points for various gases.
Electrolyte Condition Alarm
This section describes the electrolyte condition alarm.
Analog Output
The analog output section explains how to scale voltage and current outputs.
Expanded Range Relay
This feature allows relays to be assigned to indicate when the analyzer auto-ranges.
Cal Freeze
Cal Freeze holds the oxygen analog output at the last reading before calibration.
IN CAL Relay Assign
This function assigns relays to signal when the analyzer is in calibration mode.
Communications Port
The communications port setup allows configuration of RS-232C or RS-485 formats.
Sample Gas Scale Factor (GSF)
The GSF corrects for changes in oxygen diffusion rates in non-nitrogen gases.
Disclaimer
The document notes that the theoretical method for correcting calibration in non-nitrogen gases may have accuracy limitations.
Oxygen Calibration Menu
This menu allows users to check or recalibrate the analyzer.
Gas Flow Regulation
The document outlines the procedure for regulating the flow rate of calibration gas.
Gas Scale Factor (GSF)
The Gas Scale Factor function is referenced.
Oxygen Calibration
Includes Zero Check, AutoZero, and Manual Zero procedures.
Span Calibration
Includes Check/Adjust Span, Auto Span, and Manual Span procedures.
Additional Notes
The document emphasizes the importance of stable output before performing calibrations.
Manual Calibration Procedure
A manual calibration can be initiated once the span gas is connected and the analyzer is stable.
New Sensor Installation
The New Sensor Data Screen displays factory calibration values.
Averaging Filter
The analyzer uses electronic digital filtering to smooth out noise.
Filter Settings
Three parameters adjust noise and response time: Filter Weight, Response Type, and Threshold.
Backlight and Password Protection
The backlight can be set to ON, OFF, or timed to minimize power consumption.
Diagnostics Menu
The Diagnostics Menu tests analyzer functions.
Memory and Screen Tests
The document outlines procedures for conducting memory and screen tests on the analyzer.
Service and Maintenance
Includes Return Material Authorization, Calibration, Storage Conditions, Sensor Maintenance, and Gas Purifier Maintenance.
Spare Parts and Troubleshooting
Includes a Spare Parts List and Troubleshooting Guide.
Specifications and Procedures
The document outlines various procedures for maintaining and troubleshooting the NanoTrace Analyzer.
Shipping Instructions
Before shipping the analyzer, it is crucial to drain and rinse the sensor to remove electrolyte.
Theory of Operation
The NanoTrace Analyzer operates on a Coulometric principle.
Safety Information
The document includes safety warnings about hazardous conditions.
Key Recommendations
Ensure proper electrolyte levels and secure sensor caps.
1. Specifications and Composition
The document provides detailed information on the composition and properties of various chemical substances.
2. Handling and Storage
For Potassium Hydroxide, it is crucial to use protective clothing, gloves, and eye protection.
3. Safety Measures
In case of accidental release of Potassium Hydroxide, absorb the spill with inert material.
4. Exposure Controls and Personal Protection
Potassium Hydroxide requires protective goggles, gloves, and clothing.
5. Physical and Chemical Properties
Potassium Hydroxide has a boiling point of 104.5°C and a melting point of -3.5°C.
6. Stability and Reactivity
Potassium Hydroxide is stable but reacts with incompatible materials.
7. Toxicological Information
Potassium Hydroxide is a severe irritant to eyes, skin, and mucous membranes.
8. Ecological Information
Potassium Hydroxide is completely soluble in water and degrades by reacting with atmospheric carbon dioxide.
9. Disposal Considerations
Dispose of Potassium Hydroxide in accordance with federal, state, and local regulations.
10. Regulatory Information
Potassium Hydroxide is listed on various regulatory inventories.
11. Other Information
The document includes MSDS creation and revision dates.
Health Hazards
Exposure to nickel and titanium can cause respiratory issues, skin irritation, and gastrointestinal problems.
First Aid Measures
In case of eye contact, flush with water and seek medical attention.
Fire-Fighting Measures
Nickel can become pyrophoric at high temperatures.
Accidental Release Measures
Allow materials to cool before handling.
Handling and Storage
Store in a cool, dry place away from incompatible materials.
Exposure Controls/Personal Protection
Use respirators and ventilation to control dust exposure.
Physical and Chemical Properties
The product is odorless with a specific gravity of 0.9 g/cc.
Stability and Reactivity
The product is stable but can react with strong acids and oxidizing agents.
Toxicological Information
Contains nickel and nickel oxide, which are toxic and potentially carcinogenic.
Disposal Considerations
Follow federal, state, and local regulations for disposal.
Transport Information
Classified as spontaneously combustible.
Regulatory Information
Contains chemicals subject to reporting under SARA 313.
Warranty
The product is warranted against defects for one year.
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Catalog excerpts

DF550E Operator Manual 082616-2

Copyright 2011 by Servomex Corporation No part of this publication may be reproduced, stored in a retrieval system or transmitted in any form, or by any means including electronic, mechanical, photocopying, recording or otherwise without prior written permission of Servomex Corporation. Stablex, Bi-Strata and are trademarks of Servomex Corporation. VCR is a registered trademark of the Cajon Compa

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DF550E Operator Manual 082616-3

DF-550E Operator Manual Firmware v20.11 Version 100611 Your NanoTrace Oxygen Analyzer has been designed, manufactured and is supported under ISO-9001 controls, thus helping to insure the highest possible standards of quality. Every analyzer that Servomex manufactures is tested and operated on a variety of gas concentrations to insure that it functions properly when you receive it. The certificate of calibration assures your analyzer has been calibrated on gases that are traceable to NIST standards. With proper maintenance, your analyzer should remain calibrated for years. For a fast and successful...

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DF550E Operator Manual 082616-4

Read Me First… Unpacking Procedure Follow the procedure below to unpack your Process Oxygen Analyzer. 1. Examine the condition of the packaging and its contents. If any damage is apparent, immediately notify the carrier and Servomex. Do not proceed with the installation. 2. Check the contents against the packing slip to make sure the shipment is complete. Unattached equipment may be shipped with the analyzer in supplemental packaging. Shortages should be reported to Servomex immediately. 3. All analyzers are shipped with the following: Item One bottle of Hummingbird Brand Electrolyte Gold Servomex...

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DF550E Operator Manual 082616-5

Thank You Thank you for selecting the model DF-550E Process Oxygen Analyzer. Servomex designs, manufactures, exhaustively tests, and supports every analyzer under ISO-9001 control. You should expect every Servomex analyzer to arrive in good working order and, with proper maintenance, provide years of trouble-free service.

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DF550E Operator Manual 082616-13

2 Cautions There are a number of warnings and cautions that must be observed to avoid damage to the analyzer as well to insure the safety of its users. The analyzer must be operated in a manner specified in this manual. Servomex cannot be responsible for direct or consequential damages that result from installing or operating the analyzer in a manner not described in this manual. Importantly, the analyzer has been designed for use with inert, non-toxic, non-combustible sample gases only. Servomex cannot be responsible for direct or consequential damages that result from using the analyzer with...

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DF550E Operator Manual 082616-14

CAUTION Do not setup or operate the Oxygen Analyzer without a complete understanding of the instructions in this manual. Do not connect this Analyzer to a power source until all signal and plumbing connections are made. CAUTION This analyzer must be operated in a manner consistent with its intended use and as specified in this manual. DANGER The electrolyte is a caustic solution. Review the Material Safety Data Sheet (MSDS) before handling the electrolyte solution. The sensor is shipped dry and must be charged with electrolyte before it is operated. CAUTION Over-pressurizing the sensor can result...

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DF550E Operator Manual 082616-15

EMI DISCLAIMER This Analyzer generates and uses small amounts of radio frequency energy. There is no guarantee that interference to radio or television signals will not occur in a particular installation. If interference is experienced, turn-off the analyzer. If the interference disappears, try one or more of the following methods to correct the problem:  Reorient the receiving antenna.  Move the instrument with respect to the receiver.  Place the analyzer and receiver on different AC circuits.

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DF550E Operator Manual 082616-17

3 Specifications Range of Operation: 0-10ppm Lowest Detection Level (LDL): 0.2 ppb @ Constant Conditions Resolution (Smallest Detectable Change): 0.1 ppb Calibrated Accuracy: ±3 percent of reading or ±0.5 ppb (whichever is greater) @ Constant Conditions Response Time: Typically less than 15 seconds to read 90 percent of a step change. The equilibrium time is dependent on specific conditions. Upset Recovery Time: Typically less than 15 minutes from a high ppm upset to within 10 ppb of the previous stable reading. Ambient Operating Temperature: 0° C to 45° C (32° F to 110° F) Analog Output Range:...

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DF550E Operator Manual 082616-18

Calibration System Components: (Optional) Pneumatically or manually actuated springless diaphragm valve calibration system to provide zero and span calibrations. Orbital butt- welded assembly with one quarter inch VCR-type connections. Sensor Warranty: 5 years, See Warranty section on page 117. Power Requirements: 100 to 120 VAC, 50/60 Hz, standard, 35 Watts 200 to 240 VAC, 50/60 Hz (optional), 35 Watts NiCad battery supplemental power (optional) Display: 2.5-inch by 3.75-inch super twist LCD graphics with backlighting Output Signals: Analog Output: Menu scalable from 0-20 ppb to 0-10 ppm Non-isolated...

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DF550E Operator Manual 082616-19

Dimensions: 12.2-inch (30.9cm) wide x 8.9-inch (22.7 cm) high x 10.0-inch (25.4 cm) deep approximate (with handle and gas fittings) Weight: 18 pounds (8.2 kg) (approximate) - with optional manual calibration system add 2 pounds (.9 kg) - with optional automated calibration system add 4 pounds (1.8 kg) Figure 1: PNT Oxygen Analyzer

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DF550E Operator Manual 082616-21

4 Installation and Setup This procedure describes installation of the analyzer without options and with the voltage output set to 0-10 VDC. Options may affect the setup procedure described in this section. If your analyzer is equipped with options, refer to the appropriate section to determine changes to the setup. NOTE The screens shown in this manual have values that may not match the actual values displayed during your setup. Figure 2: Major Internal Components

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DF550E Operator Manual 082616-22

4.1 Adding Electrolyte DANGER The electrolyte is a caustic solution. Review the Material Safety Data Sheet (MSDS) before handling the electrolyte solution. NOTE The sensor is shipped dry and must be charged with electrolyte before it is operated. NOTE Use only Hummingbird Brand E-Lectrolyte Gold in the Platinum Series NanoTrace Oxygen Analyzer. (gold sensor cap) Failure to do so will void warranty. Install one bottle only. NOTE Do not apply power before adding electrolyte and thoroughly purging sample line. 4.1.1 Adding Electrolyte Procedure Follow this procedure to add electrolyte: 1. Remove...

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