LT STM_2012

LT STM_2012
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LT STM_2012

Product catalog summary
Overview
The document provides an in-depth analysis of the Low Temperature Ultra-High Vacuum Scanning Tunneling Microscope (LT UHV STM) and Atomic Force Microscope (AFM) technology, emphasizing its advanced features and capabilities. The system is designed to operate at temperatures below 5 K, ensuring high stability and minimal thermal drift, which are essential for precise scientific measurements.
Key Features
  • Low Temperature Operation: Effective operation at temperatures below 5 K for stable and sensitive measurements.
  • Thermal Drift and Stability: Minimal thermal drift and high stability for long-term experiments.
  • Ultimate Performance: Optimized STM/STS/IETS performance for atomic resolution and manipulation.
  • QPlus AFM Technology: Integrates AFM capabilities without compromising STM performance, enabling single molecule manipulation and force probing.
  • Variable Temperature Operation: Supports a range of temperatures for experimental flexibility.
  • Guided 3D Coarse Positioning: Ensures precise sample positioning.
  • Efficient Cooling and Sample Exchange: Features a 50-hour liquid helium hold time and fast cool down, with safe and quick sample/tip exchange.
Applications and Performance
  • Atom Manipulation: Demonstrated precision by arranging 42 Ag atoms on a Ag(111) surface at 4.8 K.
  • Scientific Research: Applicable in spectroscopy, atom manipulation, and studies on superconductors and semiconductors.
  • Advanced Modulation Spectroscopy: Capacitive compensation for improved signal-to-noise ratio, enabling high-resolution measurements.
Technical Specifications
  • State-of-the-art Preamplifier: IVC H3 preamplifier supports tunneling currents below 1 pA with excellent signal-to-noise ratio.
  • Offset Compensation: Allows for genuine tunneling currents below 1 pA with high precision.
  • QPlus Sensor: Enables atomic resolution non-contact AFM using a quartz tuning fork for force detection.
System Configurations
  • MULTIPROBE LT S: Basic configuration with fast entry load lock and sample carousel.
  • MULTIPROBE LT XP: Extended version with additional sample preparation and analysis capabilities.
  • MULTIPROBE LT XA: Further extended for comprehensive surface analysis techniques.
Additional Features
  • Magnetic Fields and Variable Temperatures: Supports experiments with magnetic fields and variable temperature settings.
  • Sample Contacts: Provides flexibility for experimental devices and signal measurements.
Conclusion
The LT STM and AFM technology offers unparalleled performance for low-temperature scientific research, with advanced features supporting a wide range of applications and experimental setups.
Overview of the LT STM Cryostat
The LT STM cryostat is designed for mechanical stability and acoustic sensitivity, utilizing a liquid helium bath cryostat surrounded by a liquid nitrogen bath within an ultra-high vacuum chamber. This setup ensures excellent acoustic decoupling and allows the system to reach temperatures below 3 K with additional pumping on the LHe reservoir. Key features include rapid cooldown from 300 K to 5 K in under 10 hours, quick cryostat refill, and optional automatic LN2 refill.
Performance and Capabilities
The LT STM offers extremely low thermal drift, demonstrated by a series of images taken over 19 hours at 4.7 K without software drift correction. It supports a wide range of experiments, including STM, AFM, STS, IETS, and spin-polarized STM. The system allows for safe and fast in-situ sample and sensor exchange, 3D coarse positioning, and in-situ evaporation with up to two evaporators.
Technical Specifications
The system features a patented piezo inertia drive for precise 3D positioning, a temperature-compensated spring suspension for operation from 300 K to 5 K, and a lifting mechanism for easy sample exchange. It can be equipped with a long focal length optical microscope for sensor navigation and supports simultaneous evaporation during STM operation.
Customization and Modularity
Omicron offers customized system solutions integrating the LT STM with various techniques, such as magnetism, electron spectroscopy, and molecular beam epitaxy (MBE). The modularity of the MULTIPROBE LT STM allows for integration with other Omicron solutions, ensuring true UHV operation and high performance.
Applications and Research Highlights
The document highlights various research applications, including molecular manipulation, non-Fermi-liquid behavior studies, and atomic structure imaging. It also showcases collaborations with universities and research institutions worldwide, demonstrating the LT STM's versatility in advanced scientific research.
Contact Information
Omicron NanoTechnology GmbH, part of the Oxford Instruments Group, provides global sales and service support. Contact details and further information are available on their website.
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Catalog excerpts

LT STM_2012-1

LT STM Low Temperature UHV STM and AFM Technology • Low Temperature Operation at T < 5 K • Lowest Thermal Drift & Highest Stability • Ultimate STM/STS/IETS Performance • Leading QPlus AFM Technology • Variable Temperature Operation • Guided 3D Coarse Positioning • 50 Hours LHe Hold Time & Fast Cool Down • Safe & Quick Sample/Tip Exchange

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LT STM_2012-2

Ultimate SPM Atom manipulation with the LT STM - 42 Ag atoms arranged to form the Omicron Logo on a Ag(111) surface at 4.8 K. The parameters were Ugap= -20 mV, IT= 10 nA for imaging and Ugap= -10 mV, IT= 300 nA for atom manipulation, respectively. The probability for atom manipulation was nearly 1 when using these parameters. Measurements by A. Bettac, Omicron NanoTechnology, Germany. 88 2

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LT STM_2012-3

Performance at 5 K The Omicron LT STM is the first commercial low temperature UHV STM with proven and guaranteed atomic resolution in UHV at 5 K, now with more than 150 units delivered around the world. More than 10 years after presenting the LT STM, the importance of dedicated low temperature SPM techniques in a wide range of active scientific fields is still unbroken. Spectroscopy on molecules, atom manipulation, carbon, superconductors, semiconductors, gases on metals, and magnetics are only a few examples where research takes great advantage of low temperature SPM. The state of reduced mobility...

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LT STM_2012-4

The Preamplifier Modulation spectroscopy on Au(111) using a superconducting Nb STM tip. The superconducting gap is clearly resolved and corresponds to the BCS value of approximately 2∆ = 2.5 meV at 5 K (fMOD=1967 Hz, VMOD=150 µVPP) . This fundamentally proves the STM tip is in thermal equilibrium with the sample temperature (low temperature QPlus AFM preamplifier active during the measurement). Schematic diagram of the IVC H3 preamplifier. Capacitive compensation and internally switched gain with two feedback resistors. Atomically resolved STM measurement on Si(111) 7x7 surface with a true tunnelling...

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LT STM_2012-5

QPlus Sensor 1 mm The QPlus sensor allows for atomic resolution non-contact AFM while maintaining the user-friendliness and known performance level of the LT STM. The ease of use of the QPlus sensor now makes atomic resolution AFM a routine experiment. The sensor employs a quartz tuning fork for force detection in non-contact AFM operation. One prong of the tuning fork is fixed, while the SPM probe tip is mounted to the second prong. It thus acts as a quartz lever transforming its oscillation into an electrical signal as a result of the piezoelectric effect. The feedback signal is based on the...

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LT STM_2012-6

Different System Concepts The MULTIPROBE LT UHV systems are dedicated surface science systems for the low temperature UHV STM. Three standard MULTIPROBE LT configurations are available – S, XP and XA. Each standard system can be used as a base to match the customer’s special requirements. The LT S represents the basic system configuration with the LT STM main chamber and an easy to operate fast entry chamber. Transferring samples and probe tips is made quick and reliable using a UHV wobble stick. The LT XP system is an extended version of the LT S offering a separate chamber for various sample...

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LT STM_2012-7

MULTIPROBE LT XP Pos. 4 Pos. 1 Pos. 2 Pos. 3 Pos. 2a The MULTIPROBE LT XP is equipped with a fast entry load lock to introduce samples (or tip transfer plates) into the vacuum system (position 1). A mag probe is used to transfer the sample to position 2. A second mag probe transfers it to a high precision sample manipulator (LN2 or LHe cooling and various heating options available) at position 2a. This position allows extensive sample preparation with system ports configured for sputter sources, evaporators and more. Similar to the LT S system, the second mag probe can also transfer the sample...

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LT STM_2012-8

Versatility & Ease of Use Magnetic Fields Variable Temperatures Sample Contacts Based on a magnet coil located behind the sample plate, vertical fields can be generated in the LT STM. The use of superconducting wires avoids heat generation during operation. Coil options for pulsed fields or DC fields are available. The LT STM is equipped with a built-in PBN heater element and a Si diode for temperature measurement. The heater enables quick temperature variation between 5 K to ~ 60 K (LHe operation) and 78 K to ~ 250 K (LN2 operation). The option for 4 spring-loaded electrical sample contacts...

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LT STM_2012-9

The LT STM Stage Stage Details The LT STM stage has been designed for ultimate STM and AFM performance. It employs a very efficient damping system based on the combination of spring suspension and eddy current damping. This, together with the very rigid scan head design, ensures excellent vibration isolation with a stability in the picometer range. While maintaining its unique performance level, the LT STM has been continuously improved for additional functionality and flexibility. Some examples for the experimental customization possible with the LT STM are: pre-fitted tapped holes at all optical...

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LT STM_2012-10

lens holder The LT STM stage is equipped with an easy to operate lifting mechanism. The lifted stage is in direct thermal and mechanical contact with the cryostat, guaranteeing fast cool down as well as easy and safe tip and sample exchange. Once cooled, the stage is released into the eddy current damping system for high-performance SPM experiments. Omicron’s unique design of temperaturecompensated spring suspension allows STM and AFM operation at any accessible temperature from 300 K to 5 K without opening the system for re-adjustment. The patented Omicron piezo inertia drive is based on the...

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LT STM_2012-11

Optical Access & In-situ Evaporation The LT STM has the capability for simultaneous evaporation by two evaporators during STM operation. With the sample facing down, deposition of materials from below becomes possible. In addition, the large Z-coarse range of 10 mm for tip positioning allows for removal of the tip from the evaporation zone. The easy to operate thermal shield compartment consists of two shield pairs for LHe and LN2 shielding, respectively. To minimize heat impact, the shield concept provides three wobble stick selectable configurations: (i) SPM operation with Tmln < 5 K; (ii)...

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All Scienta Omicron catalogs and technical brochures

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Archived catalogs

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  2. VT SPM_2012

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  3. LT STM_2017

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*Prices are pre-tax. They exclude delivery charges and customs duties and do not include additional charges for installation or activation options. Prices are indicative only and may vary by country, with changes to the cost of raw materials and exchange rates.