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Windows guide

Windows guide

Windows guide

Product catalog summary
Overview: This document provides detailed information on selecting appropriate windows for cryogenic environments, focusing on materials suitable for various wavelengths and temperature conditions. It highlights the importance of choosing the right window material to ensure effective radiation transmission in experiments involving cryostats.
Window Mounting: Windows at room temperature must be vacuum tight and are typically sealed with a rubber 'O' ring to minimize strain and allow easy removal. Radiation shield windows, which do not need to be vacuum tight, should be thermally anchored using a copper mount and spring clip. For sample cells, vacuum tightness at low temperatures is crucial, with indium or copper gaskets used depending on the temperature range (up to 300 K or 500 K).
Window Materials: The choice of window material depends on the radiation's wavelength and intensity, environmental temperature, and beam polarization requirements. Oxford Instruments offers a variety of materials:
  • Spectrosil B: A synthetic vitreous silica, non-birefringent, suitable for filtering near-mid IR radiation, reducing thermal load on cryostats.
  • Spectrosil WF: Similar to Spectrosil B but with extended IR transmission range.
  • Sapphire: Suitable for visible and near IR applications, usable at high temperatures (up to 500 K), and increases transmission in extreme IR below 80 K. It is birefringent.
  • Polypropylene: A polymer with a broad transmission range, porous to helium gas above 100 K, and suitable for low temperatures down to 1.5 K.
  • Crystalline Quartz: Suitable for visible and near IR, with strong temperature dependence in far IR. Birefringent and available with z-axis cut to reduce polarization effects.
  • Calcium Fluoride: Usable in near and mid IR but not suitable as a cold inner window due to mechanical and thermal properties.
  • Zinc Selenide: Reliable for mid IR, but toxic and easily scratched.
  • KRS 5: Useful for mid IR, requires careful handling due to toxicity and complex mounting requirements.
  • Polythene: Suitable for extreme IR, porous to helium gas above 100 K.
  • Mylar™: A polyester film for extreme IR, porous to helium gas above 100 K.
  • Aluminised Mylar™: Suitable for X-ray and gamma ray applications, with high transmission and some diffuse scattering at low angles.
Conclusion: The document emphasizes the importance of selecting the right window material based on specific experimental needs, considering factors like wavelength, temperature, and polarization. It provides transmission data for various materials, aiding in informed decision-making for cryogenic experiments.
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Catalog excerpts

Windows guide-1

SPECTROSCOPY Windows for cryogenic environments 2 5,00 -1 lB trosi pec rosil WF S ct Spe hire p Sap um Flouride ci Cal talline Quartz s Cry propylene Poly .3 Choosing the right windows for your experiments

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Windows guide-2

Extensive choice to suit your experimental needs Many cryostats are used in experiments where the samples must be irradiated or measurements made on emitted radiation from such samples. Appropriate windows must be fitted to your cryostat to permit radiation to pass through the sample space. Window materials The type of window material selected will be determined by the wavelength and intensity of the radiation, the environmental temperature and whether or not beam polarisation is required. Oxford Instruments offers a wide range of different window materials. Window mounting Room temperature windows...

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Windows guide-3

Spectrosil WF is a water free synthetic vitreous silica. It has the same material a transmission range which extends further into the IR. The transmission data is for a 2 mm thick window. Sapphire Sapphire is an alternative window for visible and near IR applications. It is the only window which may be used at high temperatures (up to 500 transmission of sapphire increases in the extreme IR region. This effect allows sapphire to be used as a cold inner window for IR measurements. Sapphire is birefringent. The transmission data is for a 2 mm thick window. Polypropylene is a polymer with a useful...

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Windows guide-4

SPECTROSCOPY Crystalline quartz Crystalline quartz is a window for the visible and near IR. It exhibits a strong temperature dependence in the far IR. At temperatures below 80 K the transmission is greater than 70% for wavelengths greater than 80 μm. This material may be used as a cold inner window for far IR applications. Crystalline quartz is birefringent and is available cut with the z-axis normal to the window to reduce polarisation effects. The transmission data is for a 2 Calcium fluoride Calcium fluoride may be used in the near and mid IR. It cannot be used as a cold inner window due to...

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Windows guide-5

KRS 5 KRS 5 (Thallium Bromide-Thallium Iodide) complex nature of the cold window mount and the necessity to make it vacuum tight results in the clear access diameter being reduced by 2 mm when compared with other materials. The material is toxic and should be handled with care. Zinc selenide Zinc selenide is a reliable cryogenic window for the mid IR. Care should be taken with handling as it is toxic and scratches easily. The transmission data is Windows for cryogenic environments

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Windows guide-6

Polythene is a polymer which may be used in the extreme IR. The material is porous to helium gas above 100 K. The transmission data is for a 1 mm thick window. MylarTM Mylar™ is a polyester film. Standard windows are 125 μm thick and may be used as a cryogenic window in the extreme IR. Mylar is porous to helium Aluminised MylarTM Aluminised Mylar™ is a useful window for X-ray and gamma ray applications. For X-rays its transmission is greater than 90% with some diffuse scattering at low angles. Standard windows are 125 μm thick with a 0.3 μm thick aluminium coating on one side. visit www.oxford-instruments.com...

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