TMA 402 F1/F3 Hyperion®
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TMA 402 F1/F3 Hyperion® Thermomechanical Analysis – TMA Method, Technique and Applications Analyzing & Testing

Thermomechanical Analysis (TMA) TMA Analysis Results Linear thermal expansion Coefficient of thermal expansion Phase transition temperatures Sintering temperatures Shrinkage steps Glass transition temperatures Dilatometric softening points Volumetric expansion Density changes Delamination Decomposition temperature Sintering kinetics Isostrain Creep Relaxation Stress/strain curve Thermomechanical analysis (TMA) is a technique for determining the dimensional changes in solids, liquids or pasty materials as a function of temperature and/or time under a defined mechanical force (DIN 51005, ASTM...

Thermal Expansion The linear thermal expansion is an important variable for assessing the dimensional behavior of a material in response to a change in temperature. Measurement on an epoxy resin with a sample length of 6 mm in expansion mode (fused silica sample holder); 1st and 2nd heating runs at a rate of 2 K/min This plot shows the thermal expansion (dL/L0 in %) of an epoxy resin between -70°C and 270°C. In the first heating (blue curve), the onset of the glass transition (Tg) occurs at 123°C. In the second heating (red curve), the onset of Tg is slightly shifted, to 125°C. This shift...

Thermomechanical Analysis A Fundamental Analysis Technique For Material Properties Detects Even the Slightest Dimensional Changes The LVDT constitutes the centerpiece of the NETZSCH TMA 402 F1/F3 Hyperion®. The technology behind it is tried-and-true: Even the slightest of length changes, into the nanometer range (digital resolution of 0.125 nm), can be measured and detected. A variation of furnace options for all applications To adjust the instrument for various temperature ranges and varied atmospheres, all that needs to be done is to change the furnace. This can be carried out by the...

Simultaneous Measurement of Force and Displacement Signal The force operating on the sample is generated electromagnetically. This ensures a quick response time for experiments with a changing load. A highly sensitive force sensor (digital resolution < 0.01 mN, max. force ±4 N) continuously measures the force exerted via the pushrod and readjusts it automatically. This sets the NETZSCH TMA 402 F1/F3 Hyperion® apart from other instruments which only use preset values. Displacement control Isostrain From Sensitive to Stiff Materials The electronic control system allows users to set the force...

Highest Flexibility at Maximum Precision The modular design of the TMA 402 F1/F3 Hyperion® makes it unique among the competition. You are always prepared for the future! One Instrument – Different Temperature Ranges -150°C to 1000°C Steel furnace with LN cooling IC-furnace with mechanical cooling without the need of LN21 SiC furnace Copper furnace, allows for measurements under controlled humidity environment from 0°C to 100°C Water-vapour furnace connected to a water-vapour generator LN2 liquid nitrogen cooling ng evolvi s e s a the g nt? ted in al treatme s e r e t so In therm can al ® n...

Measuring Modes and Sample Holders Sample Holders for Copper, Steel, Water Vapor and SiC Furnce Sample holders made of fused silica for the range from -150°C to 1100°C Expansion/ compression – pushrod with flat tip, Ø 4 mm Penetration – pushrod with flat tip, Ø 1 mm Tension, max. tension length 30 mm Sample holders made of alumina for the range from RT to 1550°C 3-point bending for free bending lengths 10 mm and 20 mm Sample Holders Made of Fused Silica for IC Furnace* *can be combined with other TMA furnaces Expansion/ Penetration Tension, 3-point bending, max. tension for free bending...

Measurements in Humid Atmosphere Simulation of Environmental Influences For TMA measurements in humid atmospheres, there are two furnaces available. The water-vapor furnace covers a temperature range from room temperature to 1250°C. The furnace can be connected to a humidity generator or to a water-vapor generator which produces steam by evaporating water. The copper furnace can be used for conventional TMA measurements from -150°C to 500°C. It can be conveniently connected to a humidity generator, allowing for in-situ drying up to 500°C and a controlled humidity environment between 0°C and...

Swelling Behavior of Wood Under Humid Conditions In the hygroscopic wood moisture range, the dimensions and the volume undergo change when moisture is absorbed by swelling and when moisture is released by shrinkage. For the practical use of wood, the following are particularly important: The dimensions of dry wood in the three anatomical directions when the ambient climate changes (differential swelling, swelling coefficient). The shrinkage of wood when drying from the wet (fresh) to the normal condition (drying rate). To test the swelling behavior on beech wood, three samples were cut from...

Proteus® Software Clever Features for Intelligent Analysis on of eterminati d c ti a m to ansion, Au gth in exp n le le p m es! initial sa nsion mod te d n a n o penetrati At a Glance – Highlights of the TMA Proteus® Software TMA 402 Hyperion® Automatic sample length detection Force adjustment/ segment Softening point detection Density determination Force modulation Temperature modulation Strain control Report generator  Included in standard configuration  Optional Identify – Identification and Classification of TMA Curves The Identify database offers a state-of-the-art means of verifying...

AutoEvaluation on glass transition onsets AutoEvaluation AutoEvaluation is an intelligent software functionality exclusively offered by NETZSCH. It is a selfacting evaluatin of thermoanalytical measurement curves that works without using pre-defined macros. This is an immense support and time saver. AutoEvaluation offers special functions for the evaluation of various materials. When testing Metals, “Metal Melting” will automatically evaluate the onset of melting. “Glass Transition and Softening” displays the onset of glass transition and the peak of softening with just one click. Measuring...