DMA 303 Eplexor

DMA 303 Eplexor
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DMA 303 Eplexor

Product catalog summary
Introduction to Dynamic Mechanical Analysis (DMA)
Dynamic Mechanical Analysis (DMA) is a vital tool for evaluating the mechanical properties of engineering materials, especially polymers. It assesses changes in viscoelastic behavior under dynamic conditions such as temperature, time, frequency, and stress.

Importance of DMA in Product Design
DMA is crucial for understanding the mechanical behavior of polymers, which are extensively used in industries like automotive, electronics, and medical. It aids in predicting mechanical behavior, essential for designing new products.

Key Information from DMA
DMA provides insights into viscoelastic properties, stiffness, damping properties, material reactions, phase transitions, glass transition temperature, and the influence of fillers and additives. It also predicts material behavior using Time-Temperature-Superposition (TTS).

DMA 303 Eplexor® Features
The DMA 303 Eplexor® applies precise forces up to 50 N, operates over a wide temperature range from -170°C to 800°C, and has a frequency range from 0.001 Hz to 150 Hz. It offers high sensitivity with 1-nm resolution and an amplitude range of ± 2.5 mm.

Measurement Modes and Setup
Available modes include tension, 3-point bending, compression/penetration, cantilever, and shear. It features RFID technology for auto-detection of sample holders and state-of-the-art software for quick setup and operation.

Advanced Instrument Design
The instrument has a height-adjustable design for user comfort, an immersion accessory compatible with all sample holders, and an illuminated sample holder area for easy setup.

Cooling Solutions
Cooling solutions include the AIC 80 air intracooler for low-temperature experiments without liquid nitrogen and liquid nitrogen cooling for temperatures as low as -170°C.

Sample Handling Excellence
It offers a variety of sample holders for different materials and conditions, with toolless installation and automatic calibration using RFID technology.

Applications and Measurement Examples
Applications include measurement under defined humidity conditions, with examples like PET film measured in tensile mode showing significant changes in modulus of elasticity and loss factor with humidity.

Specifications and Features
The DMA 303 Eplexor® is equipped with a furnace reaching up to 800°C, a UV light source adapter, and an in-furnace camera for real-time observation. It supports high forces up to 50 N and small forces down to 1 mN.

Proteus® Software
The Proteus® software offers extensive features for measurement and analysis, including calibration routines, manual control of loads and temperatures, and the ability to combine multiple programmable sweeps.

Advanced Tools
The DMA Calculator helps determine suitable entry values for measurements, while the Identify tool aids in material identification through database comparison. AutoEvaluation provides automated analysis of onset and peak temperatures.

Applications
Applications include the study of EPDM and PELD films in tensile mode and Inconel 625 in 3-point bending, demonstrating the equipment's versatility.

Data Management
The Proteus® Search Engine facilitates efficient data management by sorting and filtering measurement data based on various criteria.

Conclusion
The DMA 303 Eplexor® and Proteus® software provide a comprehensive solution for material analysis under diverse conditions, supporting precise and efficient research and development.

Technical Specifications
The DMA 303 Eplexor® offers a temperature range from -170°C to 800°C, a heating rate of 0.01 K/min to 40 K/min, and supports a frequency range from 0.001 Hz to 150 Hz. It handles static deformations up to 30 mm and offers various deformation modes.

Measurement Modes
It supports multiple measurement modes such as temperature sweep, time sweep, temperature-frequency sweep, frequency sweep, universal test, creep/relaxation, and load sweep.

Sample Holders
Different sample holders are available for various applications, suitable for materials like thermoplastics, elastomers, films, fibers, and adhesives.

DMA and DSC
DMA provides insights into viscoelastic properties, while DSC measures changes in heat capacity. The document highlights the importance of homogeneous temperature distribution for accurate measurements.

Universal Testing
Universal tensile testing analyzes the direction-dependent behavior of materials like PE films, showing linear and non-linear viscoelastic behavior.

Master Curve Generation
Master curve generation using time-temperature superposition predicts viscoelastic properties at frequencies beyond the measurable range.

Effect of Strain on Foam Materials
The document describes how deformation affects the stiffness and energy dissipation of foam materials, introducing a new measurement mode, load sweep.

Company Overview
NETZSCH-Gerätebau GmbH is a leading global technology company specializing in mechanical, plant, and instrument engineering, offering solutions in thermal analysis, calorimetry, rheology, and fire testing.
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Catalog excerpts

DMA 303 Eplexor-1

Dynamic Mechanical Analysis DMA 303 Eplexor® Method, Technique, Applications Analyzing & Testing

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DMA 303 Eplexor-2

Dynamic Mechanical Analysis UNLOCKING THE MECHANICAL MATERIAL PROPERTIES OF A WIDE RANGE OF MATERIALS Dynamic Mechanical Analysis (DMA/DMTA) is an indispensable tool for determining the mechanical properties of engineering materials, particularly the viscoelastic behavior that characterizes polymers. Changes in the viscoelastic behavior of a material can be measured by applying forces and deformations under dynamic conditions, for example, as a function of temperature, time, frequency, stress, atmosphere, or a combination of these parameters. How Can Dynamic Mechanical Analysis Help You Fulfill...

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DMA 303 Eplexor-4

Why the DMA 303 Eplexor® Stands Out Application of Precise Forces up to 50 N Dynamic and Static Understand the mechanical behavior of even stiff materials with an unprecedented 50 N in a desktop DMA. Wide Temperature Range from -170°C to 800°C Test a wide range of materials and a material‘s broad thermal behavior within this unrivaled temperature range. Frequency Range of 0.001 Hz to 150 Hz Better understanding of a material‘s structure and properties is obtained when a wide range of deformation rates can be applied. Highest Sensitivity with 1-nm Resolution Detect minute changes in the mechanical...

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DMA 303 Eplexor-5

Static Drive (Stepper motor) Responds to sample elongation Especially important for such investigations as tensile tests Travel range: 30 mm Contactless Optical Position Sensor No friction 1-nm resolution Custom-Designed Drive System Temperature-controlled, leight-weight electro-magnetic drive For precise application of forces up to 50 N RFID* Tag on Probe and Frame Recognition of the sample holder type Automatic selection of the correct calibration 3D-Printed Silicon Carbide Furnace Lining Thin-walled but robust Exceptional heat transfer Time-saving – fast heating and cooling Temperatures at...

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DMA 303 Eplexor-6

Specimens of clearly defined geometry, cut from sheets, plates, or molded shapes, are mounted in a suitable sample holder. The DMA‘s moving probe applies a static and/or dynamic sinusoidal force, generated by ... A non-contact sensor detects dynamic sample deformation. The system‘s additional stepper motor drive adjusts when a sample experiences a length change, such as thermal expansion. This static displacement is monitored by a second contactless sensor. The furnace of the DMA 303 Eplexor® features two independent temperature control loops to ensure homogeneous conditions at the sample. This...

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DMA 303 Eplexor-7

Storage Modulus E’, Loss Modulus E’’ and tan δ Certain materials, such as polymers, exhibit viscoelastic behavior; they have both elastic properties (like an ideal spring) and viscous ones (like an ideal damper). The measurement curve on the right shows a typical DMA measurement result for a polymeric material that is undergoing a glass transition. The green curve depicts the storage modulus, E’, the red curve shows the dynamic loss modulus, E’’, and the blue curve shows the derived phase shift and the resulting loss factor, tan δ. DMA is extremely sensitive to glass transition as E’ shows a...

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DMA 303 Eplexor-8

Advanced Instrument Design Offering Flexibility and Convenience The unique suspended and moving sample holder of the DMA 303 Eplexor® arranged below the measuring system prevents contamination from falling sample fragments and allows easy and safe sample handling. We Take Care of All Users Clear View The height-adjustable measuring head accommodates for different users' heights or preferences for standing or sitting, offering optimal comfort during use. The illuminated sample holder area makes it easy to set up samples and geometries. This, in combination with heightadjustable sample holders,...

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DMA 303 Eplexor-9

IMPROVED STATUS INFORMATION – EVEN FROM AFAR Get complete insights into your measurements with the DMA 303 Eplexor®. Our advanced instrument offers a comprehensive overview of your current measurement on the built-in display. The innovative LED status bar allows you to check the general instrument status of the instrument even from afar. The integrated color display provides real-time updates on important information, such as: Measurement progress Temperature Force Frequency No more time-consuming logging into your PC – the information is right there. Visual support when changing sample holders...

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DMA 303 Eplexor-10

EFFECTIVE CHOICE OF COOLING SYSTEMS Smart and Economical Cooling Solution for Your LowTemperature Experiments Many applications, such as low-stiffness polymers, require a measurement start below room temperature. Air Chiller System The AIC 80 cooling system is a compact air intracooler that operates entirely without liquid nitrogen. It is a compact cooling unit based on a heat exchanger system with a long insulated connection line, allowing the air intracooler to be placed under the table or on the side, whichever is most convenient in your laboratory. The valve is software-controlled and will...

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DMA 303 Eplexor-11

NETZSCH offers a wide variety of sample holders for its DMA 303 Eplexor®. This results in optimal adaptation of the test conditions to the sample size and stiffness, as well as to the application. For example, a different sample holder is needed to measure a thin polymer film versus a stiff material such as a fiber-reinforced composite. RFID* tag for automatic sample holder recognition Grooves supporting toolless installation Fixture guides supporting correct insertion of sample holder The latest generation of NETZSCH DMA sample holders feature a low-mass design. There is a choice of heat-resistant...

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DMA 303 Eplexor-12

Clamping Systems to Suit Your Every Need Tension sample holder This sample holder is perfect for solid materials. The sample doesn't suffer from clamping effects and results are therefore ideal. The three-point bending tool is equipped with self-adjusting outer sample supports. This allows for good results to be achieved even on slightly warped samples. Tensile clamps are commonly used for films and fibers. With a force up to 50 N, even strips of moderately stiff materials can be measured. Specimens are fixed with only one screw, ensuring evenly distributed clamping pressure. Laser-etched, non-slip...

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