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Dilution of H2S for detection in THz range

Dilution of H2S for detection in THz range

Dilution of H2S for detection in THz range

Product catalog summary
Project Overview: The project, in collaboration with Politecnico di Bari, focuses on the dilution of hydrogen sulfide (H2S) for detection in the terahertz (THz) range. The PolySenSe Lab, led by Vincenzo Spagnolo, is spearheading this initiative.
Project Management: Vincenzo Spagnolo, a Full Professor of Applied Physics at the Technical University of Bari, leads the project. He has extensive experience in gas sensing techniques and heads the PolySense lab, a joint research initiative with THORLABS GmbH.
Role of MCQ Instruments: MCQ Instruments is responsible for diluting a certified gas mixture of 200 ppm H2S in pure nitrogen (N2) down to 20 ppm, facilitating precise and stable micro-flows for spectrometer feeding.
Technical Specifications: The project utilizes the GB100 Series Gas Mixer, which allows control of flow rates from 0.1 ml/min to 500 ml/min without cut-off. The software automation feature enables efficient experiment management.
Benefits and Innovations: The THz spectral range is advantageous for gas spectroscopy due to its strong line strengths and fast relaxation rates. H2S detection in this range is significantly stronger than in the mid-IR range, reducing hydrocarbon interference.
Application and Results: The project employs a liquid nitrogen-cooled THz QEPAS sensor with a pulsed QCL to excite H2S transitions. The Gas Mixer 100 facilitated the creation of gas mixtures that confirmed the QEPAS sensor's linear response and established a minimum detection limit in the part-per-billion scale.
Conclusion: The project sets a foundation for advanced H2S detection in natural gas, showcasing the effectiveness of the GB100 in compact and portable gas mixing solutions.
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Catalog excerpts

Dilution of H2S for detection in THz range-1

H2S DILUTON - MICRO FLOW H2S DETECTION IN THE THZ RANGE A SOLID BUSINESS CASE IN COLLABORATION WITH THE “POLITECNICO DI BARI“ GENERAL INFORMATION ABOUT THE PROJECT Dilution of H2S for detection in THz range HEAD OF PROJECT MANAGEMENT: Vincenzo Spagnolo To dilute a certified gas mixture of 200 ppm of H2S in pure N2 down to 20 ppm MORE INFORMATION ABOUT THE HEAD OF THE PROJECT Vincenzo Spagnolo received the degree (summa cum laude) and the PhD, both in physics, from University of Bari. He works as Full Professor of Applied Physics at the Technical University of Bari. Since 2017, he is the director of the joint-research lab PolySense, created by THORLABS GmbH and Technical University of Bari, devoted to the development and implementation of novel gas sensing techniques and the realization of highly sensitive QEPAS trace-gas senso

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Dilution of H2S for detection in THz range-2

DESCRIPTION OF THE APPLICATION AND THE TARGET Gas sensing spectroscopic techniques aim to operate with isolated or well separated absorption lines characterized by large cross-sections. The application developed is based on a liquid nitrogen-cooled THz QEPAS sensor, employing a pulsed QCL to excite a H2S rotational transition at 95.63 cm-1. The THz spectral range offers many advantages for gas spectroscopy because of the comb-like distribution of the spectral features, the strongest linestrenghts in the whole infrared region and the fastest relaxation rates. Hydrogen sulfide (H2S) shows absorption...

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