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Thermo mechanical Analysis TMA PT 1000

 Thermo mechanical Analysis   TMA PT 1000

Thermo mechanical Analysis TMA PT 1000

Product catalog summary
Overview of TMA/DTMA Method: Thermo Mechanical Analysis (TMA) is a technique used to measure sample displacement as a function of temperature, time, and applied force. It is commonly used to characterize linear expansion, glass transitions, and softening points of materials. The method involves applying a constant force to a specimen while varying the temperature.
Typical Applications: TMA is used for tension studies, determining softening behavior, glass transition temperatures, phase changes, mechanical behavior under force, expansion coefficients, sintering behavior, volumetric expansion, E modulus, and friction resistance.
Key Features: The TMA Platinum Series offers high resolution for measuring nanometer changes, dynamic load TMA for weak transitions, a wide measuring range from -150°C to 1600°C, and a modular design for future expansion. It includes a gas-tight cell for controlled environments and supports hyphenated techniques like evolved gas analysis.
Sample Chamber and Furnace: The sample chamber is centrally located in the furnace, allowing controlled temperature and atmosphere. An optional mass flow controller is available for gas regulation. The furnace design enables rapid heating and cooling with excellent control over the temperature range.
Sensor and Dynamic TMA Mode: Dimensional changes are transmitted via a pushrod to a precise inductive transducer, ensuring reproducibility. The dynamic TMA mode studies visco-elastic behavior by alternating the force on the probe.
Sample Holders and Pressure Control: A variety of sample holders are available, and automatic pressure control adjusts contact pressure between 10mN and 20N.
Cooling System: The liquid nitrogen cooling system is automated, eliminating the need for manual refilling and improving reproducibility.
Software Features: The software includes modules for temperature control, data acquisition, and evaluation. It supports text editing, data security, thermocouple protection, curve comparison, data export, multi-method analysis, and statistical evaluation.
Applications and Case Studies: The document provides examples of TMA applications, including the evaluation of elastomers, polyvinylchloride, silicon rubber, and polycarbonate. It discusses the glass transition points, elastic and plastic ranges, and creep behavior of these materials.
Additional Features: Optional features include DTA evaluation and rate-controlled sintering software. The document also highlights the importance of the DTA feature for evaluating thermal expansion and phase transitions.
Contact Information: LINSEIS GmbH and LINSEIS Inc. contact details are provided for further inquiries.
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Catalog excerpts

 Thermo mechanical Analysis   TMA PT 1000 -2

Thermo mechanical analysis (TMA) easily and rapidly measures sample displacement (growth, function of temperature, time, and applied force. Traditionally, TMA is used to characterize linear expansi- on, glass transitions, and softening points of materials by applying a constant force to a specimen while varying temperature. For expansion measurements, a probe rests on a sample on a stage with minimal downward pressure. Other constant force experiments include measure- ment of penetration, bending, tensi- on, shrinkage, swelling, and creep (sample motion measured as a fun- ction of time under...

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 Thermo mechanical Analysis   TMA PT 1000 -3

Sample Chamber The easily accessible chamber is located in the center of the furnace. Both temperature and atmosphere optional mass flow controller is available for purge gas regulation. The gas tight cell can be evacuated and allows you to measure under a defined atmosphere. Only such a system can provide definitive infor- mation concerning the samples The TMA Platinum Series comes with a robust and reliable furnace. Its customized design enables rapid heat up and cool down times and an excellent heating rate control over the entire temperature range Every dimensional change of the pushrod to...

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 Thermo mechanical Analysis   TMA PT 1000 -4

Features -Software: All LINSEIS TMA models are optionally equipped with the DTA evaluation feature. This provides the user with valuable additional endo- and exothermic sample information. • Program capable of text editing • Data security in case of power failure • Thermocouple break protection • Repetition measurements with minimum parameter input • Evaluation of current measurement • Curve comparison up to 32 curves • Storage and export of evaluations • Export and import of data ASCII • Data export to MS Excel • Multi-methods analysis (DSC TG, TMA, DIL, etc.) • Zoom function • 1st and 2nd derivation...

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 Thermo mechanical Analysis   TMA PT 1000 -5

FEATURES Linear Motor TMA / DTMA Features: LVDT With low constant load • Linear thermal expansion evaluation • Change of volume • Phase transformation • Sinter process evaluation • Softening point determination • Transformation points • Swelling behavior • Tension Sample Furnace With increased constant load • Penetration • Transition and comparison tests • 3 point bending test With dynamic load • Visco-elastic behavior Additional optional features • DTA evaluation • (RCS) Rate controlled sintering software Expansion Penetration E-Modulus Side Front 3 Point Bending Volumetric Expansion Tension...

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 Thermo mechanical Analysis   TMA PT 1000 -6

APPLICATIONS 5.0 150 4.8 140 4.5 4.3 130 3.8 110 3.5 3.3 Delta-L (1) [μm] 100 3.0 Glass Point 33.0°C 90 2.8 80 2.5 70 2.3 60 2.0 1.8 50 1.5 40 1.3 30 1.0 E-Modulus (smoothed) [Log(N/mm2)] 4.0 E-Modulus [PIR2-1] 120 0.8 20 0.5 Delta-L [PIR2-1] 10 Delta-L (1)[PIR2-1] 0.3 0 0.0 -10 -0.3 -90 -80 -70 -60 -50 -40 -30 -20 -10 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Temperature [°C] Glass Point 93.3°C 0 3.8 3.4 3.2 Onset 86.0°C 3.0 -300 Offset 100.5°C -400 2.8 Delta-L [PVC-1] 2.6 2.4 -500 2.2 -600 E-Modulus [PVC-1] 2.0 1.8 -700 Delta-L (1)[PIR2-1] 1.6 -800 1.4 1.2 -900 1.0 -1000 0.8 -1100 E-Modulus...

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 Thermo mechanical Analysis   TMA PT 1000 -7

50 45 Delta-L(2)[BK-00-4] 70 40 60 35 50 30 Point of Reaction 576.1°C 25 20 20 Max/Min 577.4°C 2.207μV 15 10 0 10 -10 5 Onset 575.2°C 0 -20 DTA Signal (smoothed) [μV] 40 30 Delta-L (2) [μm] 4. DTA - Feature The thermal expansion of rock crystal ( -SiO2) can be easily evaluated with the L75 Dilatometer. The additional DTA feature enables an in depth view of the thermal behavior of the material. The DTA measurement is a mathematical routine based on the sample temperature. Exo- and endothermic effects influence the change of the sample temperature during the dynamic heating or cooling cycle. At...

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 Thermo mechanical Analysis   TMA PT 1000 -8

Sample size inert, reduced inert, reduced inert, reduced LINSEIS GmbH E-mail:info@ linseis.de E-mail: [email protected] Products: DIL, TG, STA, DSC, HDSC, DTA, TMA, MS/FTIR Services: Service Lab, Calibration Service

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