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L75 / Laser (DIL Dilatometer)

L75 / Laser (DIL Dilatometer)

L75 / Laser (DIL Dilatometer)

Product catalog summary
Introduction
The document discusses the evolution and advancements in dilatometer technology by Linseis, focusing on the transition from the traditional push rod dilatometer to the new Laser Dilatometer based on the Michelson-Interferometer principle.
Traditional Push Rod Dilatometer
The original push rod dilatometer, developed by Dr. Max Linseis in the early 1950s, uses a measuring tube and a push rod to transmit the expansion signal of a sample to an LVDT sensor. This setup allows for a maximum resolution of 10nm. However, maintaining consistent thermal conditions is crucial for reproducibility, as temperature gradients can affect results.
Dual Push Rod Dilatometer
To improve accuracy, a dual push rod dilatometer measures a sample against a known reference simultaneously, eliminating errors through subtraction. This method allows for measuring expansions as small as 10E-8.
Linseis Laser Dilatometer Pico-Series
The new Laser Dilatometer Pico-series offers a significant increase in resolution and accuracy, achieving resolutions up to 0.3nm (300 Picometers), which is 33.33 times higher than previous capabilities. The interference measurement principle and special computer calibrations enhance accuracy, reducing errors to 30nm.
Technical Specifications
  • Range: 20mm
  • Resolution: +/- 1nm, typically +/-0.3nm
  • Accuracy: +/- 50nm
  • Reproducibility: +/- 10nm
  • Wavelength: 632.8nm
  • Ambient Temperature: 10..30°C
  • Sample Holder: Fused silica
  • Push Rod: Fused silica, evacuated
  • Heating: Inductive
  • Frequency Range Generator: 150..400kHz
  • Temperature Range: RT...1000°C
  • Thermocouple: Type-K (NiCr/Ni), welded to sample
  • Heating/Cooling Rate: 0.1..99.9K/s or 0.1..99.9K/min
  • Dwell Time: 0...3000s or 0...3000min
  • Acquisition Rate: max. 1000 readings/s
  • Power Requirements: 230VAC, 16A, 50..60Hz
  • Power Consumption Generator: 3.5kVA
  • Cooling Water: 2l/min, 5 Bar
  • Sample/Cooling Gas: Inert gas, 10l/min max. at 1 Bar max.
Conclusion
The Linseis Laser Dilatometer Pico-series represents a significant advancement in dilatometer technology, offering unprecedented resolution and accuracy, making it suitable for precise measurements in various scientific and industrial applications.
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Catalog excerpts

L75 / Laser (DIL Dilatometer)-1

Laser Dilatometer Pico - series 0,3nm German Patent Nr.: DE 103 09 284 A1 2004.09.30 The push rod, which transmits expansion signal from the sample to the sensor, always covers a temperature gradient of up to 1600°C from end to end, sometimes even up to 2400°C. It is understandable that these high temperatures differences on these short dimensions makes it very important for good reproducible results, to insure very good thermal conditioning of the push rod / measuring system. If this expansion Normally available dilatometers of the series L75 which use the push rod principle of measurement are successfully available in the market since 1957. As a further total new development Linseis is now offering a Laser Dilatometer built after the MichelsonInterferometer principle. The original push rod dilatometer is based on a development made by Dr.Max Linseis in the early 1950th In those days the principle used . was the same as today, using a measu ring tube in which the sample is placed. The expansion signal of the sample is transmitted through a push rod onto a LVDT sensor (linear variable differential transformer). This sensor has theoretically an indefinite resolution. T ogether with other system components and the following evaluation electronics a maximum resolution of 10nm can be obtained. transmitting part will see a different thermal history from run to run, the reproducibility can not be best. In order to get best results, identical conditions from run to run are a must. For example the room temperature, the start temperature, the heat up speed and the used sample atmosphere etc. have all to be identical.

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L75 / Laser (DIL Dilatometer)-2

Laser Dilatometer Pico - series 0,3nm Optic Laser Detector Inductivefurnace Protectiontube Bench top with Lift for measuring system and Gas/Vacuum control A further increase of resolution, as well of the absolute accuracy is now also possible through the new development of the Linseis Laser Dilatometer of the Pico-series. As the name indicates already the resolution goes up to Picometers (0,3nm = 300 Picometer). That means resolutions can be obtained which are up to a factor 33,33 higher as the resolution that were possible up to date. On top the principle of interference measurement give the...

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L75 / Laser (DIL Dilatometer)-3

Laser Dilatometer Pico - series 0,3nm Technical specifications Laser Dilatometer Range: Reproduc ibility: Wave length: Ambient temperature: Sample holder: Fused silica Fused silica, evacuated Frequency range Generator: Temperature range: Thermoc ouple: Type-K (NiCr/Ni), welded to sample Acquisition rate: Power requirements: Power consumption Generator:

 Open the catalog to page 3

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