Differential Thermal Analysis - DTA DSC PT1600
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DIFFERENTIAL THERMAL ANALYSIS

Since 1957 LINSEIS Corporation has been delivering outstanding service, know how and leading innovative products in the field of thermal analysis and thermo physical properties. We are driven by innovation and customer satisfaction. Customer satisfaction, innovation, flexibility and high quality are what LINSEIS represents. Thanks to these fundamentals our company enjoys an exceptional reputation among the leading scientific and industrial organizations. LINSEIS has been offering highly innovative benchmark products for many years. Claus Linseis Managing Director The LINSEIS business unit...

German engineering The strive for the best due diligence and ac- We want to deliver the latest and best tech- countability is part of our DNA. Our history is af- nology for our customers. LINSEIS continues fected by German engineering and strict quality to innovate and enhance our existing thermal analyzers. Our goal is constantly develop new technologies to enable continued discovery in Science.

DIFFERENTIAL THERMAL ANALYSIS Differential Termal Analysis (DTA) is the most enthalpy and Cp (Specific Heat) determination common thermal analysis method due to its under the cleanest atmospheres and under va- wide range of information provided. The LIN- cuum of 10-5mbar. The systems can be upgraded SEIS high temperature DSC PT1600 (HDSC/DTA) with an optional sample robot and coupled to a is designed to deliver highest calorimetric sensi- tivity, short time constants and a condensation free sample chamber. These features guarantee Measuring System superior resolution and baseline stability...

DSC- True Heat Flow measurement Quantitative DSC-signal Reference signal Sample signal Time (s) Ts = sample temperature Tr = reference temperature Differential Signal “A technique in which the difference in energy input into a substance and a reference material is measured as a function of temperature, while the substance and reference material are subjected to a controlled temperature program.” The differential signal is displayed as a baseline. Effects, for example the melting of a metal, can be observed as a peak. The area of the peak gives the amount of enthalpy and the direction of the...

SENSORS Our HDSC can be equipped with an unmatched Each sensor is available with different thermo- amount of different user exchangeable DSC couples to provide the highest sensitivty for your desired temperature range. Al2O3 Platinum Aluminium others DSC Heat flux 3D-Calvet-DSC sensor custom volume Different crucibles available / broad variety Crucible DTA-sensor

Best possible sensitivity for your application Electromotive force / Temperature All sensors available with the thermocouples illustrated. LINSEIS Senosor combinations cover the broadest temeprature range in the market (-180 up to 2400°C). Sensor Type Generated EMF* change in Approx. µV working tempera(Reference junction at 0°C) ture Most suited for oxidizing atmosphere Ni-Cr Cromel Similar as type S but higher temperature

Vacuum and controlled atmosphere The balance design provide for high vacuum, inert, reducing, oxidiz ing or humidified atmosphere. Furthermore, the instrument can be pressurized up to 5 bar overpressure (option). Certain corrosive conditions can be analyzed with proper precautions. The system is capable of adapting residual gas analysis systems using an optional heated capillary. Evolved gas analysis Optional gas analysis with MS, FTIR or GCMS is possible. This provides valuable additional information. Sample robot Our HDSC can be equiped with a proven sample robot for unattended sample...

Starter kit The starter kit includes a variety of tool such as scissors, cutting tools, anti electrostatic tweezers, magnifier, crucible holder, pipette, rasps, spatula etc. Oxygen Getter Material OGM The LINSEIS oxygen getter system (OGM) can be placed in any LINSEIS system as a modification of the sample gas capillary. It is used to getter smallest traces of residual oxygen in the sample chamber by offering a stronger oxygen affinity than sample materials, combined with a high effective surface to ensure the oxygen molecules react with the getter before they have a chance to get in touch...

Sample Reference

DTA This is the most common thermal analysis me- thod due to its wide range of information pro- tems allows the use of different furnaces with a vided. The LINSEIS high temperature DTA/DSC temperature range from -150 up to 2400°C. The is designed to deliver highest calorimetric sensi- system has different measuring systems for DSC tivity, short time constants and a condensation and DTA and many different crucibles. The vacu- free sample chamber. These features guarantee um tight design enables quantitative enthalpy superior resolution and baseline stability over and Cp (Specific Heat)...

All LINSEIS thermo analytical instruments are PC controlled. The individual software modules run exclusively under Microsoft® Windows® operating systems. The complete software consists of 3 modules: temperature control, data acquisition and data evaluation. The Windows® software incorporates all essential features for measurement preparation, execution, and evaluation of a thermoanalytical measurement. Thanks to our specialists and application experts, LINSEIS was able to develop comprehensive easy to understand user friendly application driven software. Features-Software: • Program capable...

Thermal Library The LINSEIS Thermal Library software package The Thermal Library allows you the comparison comes as an option for the well-known, user of the complete curves with a data base provi- friendly LINSEIS Platinum evaluation software ding thousands of references and standard ma- that is integrated in almost all our instruments. terials within only 1-2 seconds. rial Mate tion tifica Iden ion gnit reco m urve on syste c DSC retati p inter Measured and matching reference curves (green) and reference curves with poor fit (red). Our software is available in many different etc. can be...