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Analyse thermomécanique ATM

Analyse thermomécanique ATM

Analyse thermomécanique ATM

Product catalog summary
Overview of TMA/DTMA Method:
Thermo Mechanical Analysis (TMA) is a technique used to measure sample displacement as a function of temperature, time, and applied force. It is primarily used to characterize linear expansion, glass transitions, and softening points of materials. The method involves applying a constant force to a specimen while varying the temperature.
Typical Applications:
  • Tension studies of films and fibers
  • Determination of softening behavior and glass transition temperatures
  • Phase change determination and mechanical behavior under force
  • Expansion coefficient and sintering behavior analysis
  • Volumetric expansion and E modulus measurement
Key Features:
  • High resolution for measuring nanometer changes
  • Dynamic Load TMA for weak transitions and elasticity
  • Wide measuring range from -150°C to 1600°C
  • Gas tight cell for controlled measurement environment
  • Modular design for future expansion
Concept and Components:
  • Sample Chamber: Centrally located with controlled temperature and atmosphere, optional mass flow controller for purge gas regulation.
  • Furnace: Robust design for rapid heat up and cool down, excellent heating rate control.
  • Sensor: Inductive transducer (LVDT sensor) for precise dimensional change measurement.
  • Dynamic TMA Mode: Studies visco-elastic behavior with alternating force frequency.
  • Sample Holders: Various holders available for different applications.
  • Cooling System: Automated liquid nitrogen cooling system for long-term measurements.
Software Features:
  • PC controlled with modules for temperature control, data acquisition, and evaluation
  • Data security, thermocouple break protection, and automatic axis re-scaling
  • Multi-methods analysis and statistical evaluation package
  • Export capabilities to MS Excel and ASCII
Applications and Case Studies:
  • Elastomers: Evaluated for applications above 0°C, glass point at 29.9°C.
  • Polyvinylchloride (PVC): Glass point at 93.2°C, used as electrical insulator.
  • Silicon Rubber: Developed for low temperatures, glass point at -54.9°C.
  • DTA Feature: Evaluates thermal expansion of rock crystal, phase transition at 575°C.
  • Creep Behavior of Elastomers: Recovery behavior of sealing rings analyzed.
  • Polycarbonate (PC): Softening occurs before glass transition temperature, evaluated with different loads.
Product Models:
  • TMA PT10: Temperature range -30-70°C, force 1N.
  • TMA PT1000 EM: Temperature range -150-1000°C, force 1 or 5.7N.
  • TMA PT1600: Temperature range RT-1400/-1600°C, force 1 or 5.7N.
See more

Catalog excerpts

Analyse thermomécanique ATM-2

Thermo mechanical analysis (TMA) easily and rapidly measures sample displacement (growth, shrinkage, movement, etc.) as a function of temperature, time, and applied force. Traditionally, TMA is used to characterize linear expansion, glass transitions, and softening points of materials by applying a constant force to a specimen while varying temperature. For expansion measurements, a probe rests on a sample on a stage with minimal downward pressure. Other constant force experiments include measurement of penetration, bending, tension, shrinkage, swelling, and creep (sample motion measured as a...

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Analyse thermomécanique ATM-3

Sample Holders Sample Chamber A broad range of sample holders is available for the TMA. Hence the best method for testing can be selected for every application. Furthermore LINSEIS can certainly provide aid for special customer requirements. The easily accessible chamber is located in the center of the furnace. Both temperature and atmosphere can be controlled. In addition an optional mass flow controller is available for purge gas regulation. The gas tight cell can be evacuated and allows you to measure under a defined atmosphere. Only such a system can provide definitive information concerning...

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Analyse thermomécanique ATM-4

Features -Software: All LINSEIS TMA models are optionally equipped with the DTA evaluation feature. This provides the user with valuable additional endo- and exothermic sample information. • Program capable of text editing • Data security in case of power failure • Thermocouple break protection • Repetition measurements with minimum parameter input • Evaluation of current measurement • Curve comparison up to 32 curves • Storage and export of evaluations • Export and import of data ASCII • Data export to MS Excel • Multi-methods analysis (DSC TG, TMA, DIL, etc.) • Zoom function • 1st and 2nd derivation...

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Analyse thermomécanique ATM-5

Linear Motor TMA / DTMA Features: With low constant load • Linear thermal expansion evaluation • Change of volume • Phase transformation • Sinter process evaluation • Softening point determination • Transformation points • Swelling behavior • Tension With increased constant load • Penetration • Transition and comparison tests • 3 point bending test With dynamic load • Visco-elastic behavior Additional optional features • DTA evaluation • (RCS) Rate controlled sintering software Side Front Volumetric Expansion

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Analyse thermomécanique ATM-6

1. Elastomers Because of their very special and versatile properties, polyurethanes Elastomers have found wide application in virtually every industry, varying from the automotive, electrical and electronic industry, design and textile industry, to the mining and heavy duty industry. Evaluation of Elastomers specifically developed for applications above 0°C. The glass point was detected at 29.9°C. When further increasing the temperature, additional expansion of the material in the elastic range occurs. The plastic range of the material has not been reached during this evaluation. 2. Polyvinylchloride...

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Analyse thermomécanique ATM-7

Delta-L(2)[BK-00-4] DTA Signal [BK-00-3] Base Line [BK-00-3] 4. DTA - Feature The thermal expansion of rock crystal ( -SiO2) can be easily evaluated with the L75 Dilatometer. The additional DTA feature enables an in depth view of the thermal behavior of the material. The DTA measurement is a mathematical routine based on the sample temperature. Exo- and endothermic effects influence the change of the sample temperature during the dynamic heating or cooling cycle. At app. 575°C the phase transition from - to -SiO2 takes place. The deviation of the measured temperature from the literature value...

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Analyse thermomécanique ATM-8

TMA Models Model Temerature range Force Frequency Sample size inert, reduced inert, reduced inert, reduced LINSEIS GmbH Vielitzerstr. 43 95100 Selb Germany Tel.: (+49) 9287–880 - 0 Fax: (+49) 9287–70488 E-mail:[email protected] LINSEIS Inc. 20 Washington Road P.O.Box 666 Princeton-Jct. NJ 08550 Tel.: (609) 799–6282 Fax: (609) 799–7739 E-mail: [email protected] Products: DIL, TG, STA, DSC, HDSC, DTA, TMA, MS/FTIR Services: Service Lab, Calibration Service

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