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Fundamentals of leak detection

Fundamentals of leak detection
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Fundamentals of leak detection

Product catalog summary
Preface
Leybold GmbH, part of the Atlas Copco Group, is a leader in vacuum technology. This document provides an overview of vacuum technology to enhance understanding of the field, emphasizing customer partnerships and innovation.
Introduction
The document discusses the importance of leak detection in vacuum systems and industries requiring hermetic sealing, highlighting the necessity of specific leak rates for acceptance testing.
Types of Leaks
Leaks are categorized by origin, including detachable connections, permanent connections, porosity, thermal effects, virtual leaks, indirect leaks, serial leaks, and one-way leaks. Permeation is also discussed.
Leak Rate, Leak Size, and Gas Mass Flow
The document explains that no system is completely vacuum-tight, but the leak rate must be low enough to maintain required pressure. The concept of "leak rate" is introduced, measured in mbar·l/s, with a relationship to gas mass flow explained.
Leak Detection Methods Without Leak Detector
Methods include pressure rise/drop tests, bubble immersion, and foam-spray tests, each detailed with applications and limitations.
Leak Detectors and How They Work
Different types of leak detectors, such as halogen and mass spectrometers, are covered, explaining their principles, detection limits, calibration, and connection to vacuum systems.
Limit Values and Specifications for Leak Detectors
Specifications for acceptable leak rates are provided, with guidelines for different systems based on required tightness.
Leak Detection Techniques Using Vacuum Leak Detectors
Techniques such as the vacuum method, positive pressure method, and envelope test are discussed with applications and effectiveness.
Industrial Leak Test
The document outlines industrial applications of leak testing, emphasizing precise leak detection's importance in various industries.
Formulary for Leak Detection Technique
A comprehensive formulary covers pressure units, gas quantity, gas flow, pumping speed, leak rate, and unit conversion for leak detection calculations.
Specifications and Definitions
Discusses ultimate operating pressure in vacuum systems, determined by leak rate and effective pumping speed, with practical limitations like cost and space.
Causes of Pressure Issues
Failure to reach desired pressure often results from leaks or gas liberation from vessel walls and seals, differentiated using partial-pressure analysis or pressure rise tests.
Leak Detection Fundamentals
Helium is preferred for leak detection due to higher sensitivity. The document provides rough estimates of leak rates based on hole size and discusses helium leak detectors.
Correlation Between Hole Size and Leak Rate
Figures and tables illustrate the relationship between hole diameter and leak rate for air, showing smaller holes result in lower leak rates.
Leak Detection Methods
Methods include vacuum and positive pressure methods, spray and sniffer techniques for local leak detection.
Helium Standard Leak Rate
Explains the helium standard leak rate concept for consistent measurement and comparison of leak rates.
Conversion Formulas
Provides formulas for converting pressure and gas type, distinguishing between laminar viscous and molecular flow.
Leak Detection Without Special Equipment
Methods like the pressure rise test measure pressure increase time in a vacuum system without specialized detectors.
Conclusion
Emphasizes accurate measurement and helium use for sensitivity in leak detection.
Introduction to Leak Detection
Provides an overview of methods and technologies in leak detection, particularly in vacuum systems, discussing principles, procedures, and equipment.
Pressure Rise and Leak Rate Calculation
Explains how pressure rise in a vacuum container indicates a leak, with an example calculation provided.
Pressure Drop Test
Less common for vacuum systems but applicable in tank engineering, monitoring pressure drop over time.
Leak Detection Techniques
Various techniques like vacuum gauges, bubble immersion, foam-spray tests, and krypton 85 tests are detailed.
Comparison of Leak Detection Methods
Tables compare methods, highlighting test gases, pressure ranges, and detection limits, noting helium's high sensitivity.
Leak Detectors and Their Operation
Details operation of leak detectors using halogen and mass spectrometry, explaining helium's advantages as a test gas.
Conclusion
Emphasizes selecting appropriate methods and equipment for specific requirements and conditions.
Operating Principle of a Leak Detector with Mass Spectrometer
Explains operation using a mass spectrometer, focusing on the test gas spray method, with key equations for gas flow and pressure calculations.
Detection Limit and Background Signal
Discusses detection limit influenced by test gas background level, recommending techniques to manage background levels.
Calibration of Leak Detectors
Describes calibration using known leaks, detailing internal and external calibration methods.
Leak Detectors with Quadrupole and Sector Field Mass Spectrometers
Describes quadrupole mass spectrometers for larger masses and helium leak detectors with sector field mass spectrometers for sensitivity.
Direct-Flow and Counter-Flow Leak Detectors
Distinguishes between direct-flow and counter-flow detectors based on gas supply methods to the mass spectrometer.
Introduction
Provides an overview of leak detection fundamentals, focusing on vacuum systems and techniques, detailing components and processes.
Leak Detection Fundamentals
Explains auxiliary pumps' role in pre-evacuating test objects and connection lines, distinguishing between main flow and counter-flow detectors.
Counter-Flow Leak Detector
Describes counter-flow detectors where the high-vacuum pump evacuates only the mass spectrometer, detailing the detection process.
Partial-Flow Operation
Recommended when achieving start pressure is challenging, using an auxiliary pump to handle more test gas flow.
Connection to Vacuum Systems
Outlines methods for connecting leak detectors to vacuum systems, emphasizing partial-flow method and strategic placement.
Time Constant and Response Time
Defines time constant and provides examples of signal response times, explaining partial-flow operation's efficiency.
Specifications and Limit Values
Lists key specifications for leak detectors, including smallest detectable leak rate and effective pumping speed.
Leak Detection Techniques
Discusses techniques for using vacuum leak detectors, including the spray technique for local leak testing.
Conclusion
Emphasizes understanding principles and techniques for accurate and efficient vacuum system operation.
Fundamentals of Leak Detection
Test Gas Application
Adjust test gas amount based on leak rate and object size, using a choke valve to control gas flow.
Positive Pressure Method - Sniffer Technique
Involves filling the test object with test gas, tracing potential leaks with a sniffer tip detected by a mass spectrometer.
Envelope Test (Integral Leak Test)
Uses helium as a test gas, enclosing the test object in an envelope, suitable for automated industrial testing.
Bombing Test
Used for hermetically sealed components, placing them in a helium-filled pressure vessel before testing for leaks.
Industrial Leak Testing
Helium is used in industrial settings, integrated into manufacturing lines for cost-effective, reliable results.
Formulary for Leak Detection Technique
Provides equations and units for pressure, gas quantity, gas flow, pumping speed, leak rate, and adjustments for temperature and pressure.
Overview
Provides a guide on leak detection fundamentals, focusing on techniques, gas properties, and conversion units for accurate measurement.
1. Leak Rate Formulas
Provides formulas for vacuum and positive-pressure techniques, and molecular flow.
2. Change of Gas Type
Provides formulas for laminar viscous and molecular flow.
3. Gas Properties
Lists gases with chemical symbols, molar masses, and viscosities.
4. Conversion of Liquid Leak Rate to Gas Leak Rate
Provides formula for conversion.
5. Partial-flow Ratio
Defines partial-flow ratio and provides calculation formula.
6. Response Time
Provides formulas for calculating response time based on test object volume and effective pumping speed.
7. Pump-down Time and Required Pumping Speed
Provides formulas for calculating pump-down time and required pumping speed.
8. Conversion of Units
Includes tables for converting pressure, gas flow/leak rate, and temperature units.
Temperature Comparison
Compares various temperature points, including body and room temperature, ice point, boiling point of liquid nitrogen, and absolute zero.
Gas Laws
Outlines important gas laws under continuum theory, including Boyle-Mariotte, Gay-Lussac's, Amonton's, Dalton's, Poisson's, Avogadro's, General Gas Equation, Van der Waals, and Clausius-Clapeyron equations.
Additional Information
Document printed in Germany on chlorine-free bleached paper, published by Leybold GmbH.
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Catalog excerpts

Fundamentals of leak detection-1

Fundamentals of leak detection Editor: Leybold GmbH Cat. No. 199 79_VA.02 Authors: Leybold GmbH Bonner Str. 498 · D-50968 Köln T +49 (0) 221-347-0 F +49 (0) 221-347-1250 [email protected] BICOM 13619.13810.19979_VA.02      0.2.12.16 mzs Printed in Germany on chlorine-free bleached paper     Technical alterations reserved Hans Rottländer Walter Umrath Gerhard Voss

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Fundamentals of leak detection-2

Fundamentals of Leak Detection Leybold, a member of the globally active industrial Atlas Copco Group of companies has developed into the world market leader in the area of vacuum technology. In this leading position, we recognize that our customers around the world count on Leybold to deliver technical superiority and maximum value for all our products and services. This brochure is meant to provide an easy to read overview covering the entire range of vacuum technology and is independent of the current Leybold product portfolio. The presented product diagrams and data are provided to help promote...

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Fundamentals of leak detection-3

Fundamentals of Leak Detection Leak rate, leak size, (gas) mass flow . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 Helium standard leakrate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 Leak detection methods without leak detector . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Pressure rise test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Pressure drop test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12...

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Fundamentals of leak detection-4

Fundamentals of Leak Detection Industrial leak test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30 Formulary for leak detection technique . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 Pressure of a gas and pressure units . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 9.1.1 Partial pressure - total pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 9.2 9.2.1 Equation of state for ideal gases . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ....

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Fundamentals of leak detection-5

Fundamentals of Leak Detection Fundamentals of Leak Detection Introduction In addition to the actual vacuum systems and their individual components (vacuum vessel, lines, valves, measuring devices, etc .) there are numerous other systems and products in the fields industry and research with high requirements regarding tightness or so-called "hermetic sealing" . These include, in particular, assemblies for the automotive and refrigeration industry Generalized statements often made, such as “no detectable leaks” or “leak rate zero”, do not represent an adequate basis for acceptance testing Every...

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Fundamentals of leak detection-6

Fundamentals of Leak Detection 2 Leak rate, leak size (gas) mass flow No vacuum device or system can ever be absolutely vacuum-tight and it does not actually need to be. The simple essential is that the leak rate must be low enough that the required operating pressure, gas balance and ultimate pressure in the vacuum container are not influenced. It follows that the requirements in regard to the gas-tightness of an apparatus are the more stringent the lower the required pressure level is. In order to be able to register leaks quantitatively, the concept of the "leak rate" with the symbol qL and...

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Fundamentals of leak detection-7

Fundamentals of Leak Detection In order to achieve an overview of the correlation between the geometric size of the hole and the associated leak rate it is possible to operate on the basis of the following, rough estimate: A circular hole with a diameter D = 1 cm in the wall of a vacuum vessel is closed with a valve. Atmospheric pressure (p = 1013 mbar) prevails outside, a vacuum inside. When the valve is opened, the air flows at the speed of sound (vS = 330 m/s) through the opening cross section of A = p-(D2/4) - 0.79 cm2 into the vessel. The air quantity flowing into the vessel amounts to qL(air)...

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Fundamentals of leak detection-8

Fundamentals of Leak Detection Estimates or measurements of the sizes of atoms, molecules, viruses, bacteria, etc. have often given rise to everyday terms such as “watertight” or “bacteria-tight” (see Table 1).

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Fundamentals of leak detection-9

Fundamentals of Leak Detection 2.1 Helium standard leakrate Required for unequivocal definition of a leak are the pressures prevailing on either side of the (vessel) wall and the nature of the medium passing through that wall (viscosity, molar mass). For the case where the test is carried out with helium4 at a pressure difference of 1 bar from the atmosphere pressure (external) to the vacuum (p < 1 mbar, internal), which is frequently found in practice, the designation "helium standard leak rate" has been introduced in the standard DIN EN 1330-8. In order to indicate the rejection rate for a...

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Fundamentals of leak detection-10

Fundamentals of Leak Detection 3 Terms and definitions When searching for leaks one will generally have to distinguish between two tasks: 1. locating leaks and 2. measuring the leak rate In addition, we distinguish, based on the direction of flow for the fluid, between the a. vacuum method (sometimes known as an "outside-in leak"), where the direction of flow is into the test object; the pressure inside the test object is less than ambient pressure and the b . positive pressure method (often referred to as the “inside-out leak”), where the flow takes place from inside the test object outward;...

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Fundamentals of leak detection-11

Fundamentals of Leak Detection Fig. 4: Usage options for a vacuum leak detector based on the vacuum method (a, b) and based on the positive pressure method (c, d)

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Fundamentals of leak detection-12

Fundamentals of Leak Detection 4 Leak detection methods without leak detector The most sensible differentiation between the test methods used is the differentiation as to whether or not special leak detection equipment is used. In the simplest case a leak can be determined qualitatively and, when using certain test techniques, quantitatively as well (this being the leak rate) without the assistance of a special leak detector. For example, the quantity of water dripping from a leaking water faucet over a certain period of time can be determined by collecting the water with a measuring vessel....

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