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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements

Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements
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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements

Product catalog summary
Introduction
This handbook offers detailed guidance on precision DC current, voltage, and resistance measurements, focusing on low-level signals. It is designed for use with sensitive instruments such as electrometers, picoammeters, and nanovoltmeters, which are essential for measurements beyond the capabilities of standard digital multimeters (DMMs).
Section 1: Low Level DC Measuring Instruments
This section outlines the theoretical limits of DC measurements and describes various instruments used, including electrometers, DMMs, nanovoltmeters, and picoammeters. It also covers basic circuit design for voltmeter and ammeter circuits.
Section 2: Measurements from High Resistance Sources
This section addresses voltage and low current measurements from high resistance sources, discussing issues like loading errors, noise, and leakage currents. It also covers high resistance and charge measurements, including methods to extend the range of electrometers.
Section 3: Measurements from Low Resistance Sources
Focuses on low voltage and resistance measurements, highlighting challenges such as offset voltages, noise, and lead resistance. It discusses methods like the four-wire method for accurate low resistance measurements.
Section 4: Applications
Provides practical applications for the discussed measurement techniques, including capacitor dielectric absorption, electrochemical measurements, and resistivity testing of materials. It also covers charge measurement applications like capacitance measurements and static charge detection.
Section 5: Low Level Instrument Selection Guide
Offers guidance on selecting appropriate instruments and accessories for specific measurement needs.
Appendices
Includes troubleshooting guides, cable and connector assembly instructions, a glossary, and safety considerations.
Introduction to Electrometers and Low-Level DC Measuring Instruments
Electrometers are specialized instruments for measuring extremely low currents, high resistances, and charge, surpassing conventional DMMs. They are essential for detecting currents less than 10nA, measuring resistances greater than 1GΩ, minimizing circuit loading, and measuring charge or signals near Johnson noise limitations.
Electrometer Functions
  • Voltmeter Function: High input resistance and low offset current allow voltage measurements with minimal circuit loading.
  • Ammeter Function: Measures currents as low as 1fA with low voltage burden, suitable for photomultipliers and ion chambers.
  • Ohmmeter Function: Measures resistances up to 10PΩ using constant-voltage method.
  • Coulombmeter Function: Detects charge as low as 10fC, suitable for very low current measurements.
Comparison with Other Instruments
  • Digital Multimeters (DMMs): Versatile but do not reach the theoretical limits of electrometers.
  • Nanovoltmeter: Optimized for low source resistances with high voltage sensitivity.
  • Picoammeter: Similar to electrometer ammeter but less sensitive and lower cost.
  • Source-Measure Unit (SMU): Combines measuring and sourcing capabilities, suitable for high resistance measurements and I-V curve generation.
  • SourceMeter Instrument: Designed for high-speed production tests, capable of generating curves for semiconductor studies.
  • Micro-ohmmeter: Optimized for low resistance measurements using four-wire technique.
Understanding Instrument Specifications
Key terms related to instrument accuracy include sensitivity, resolution, accuracy, and uncertainty. Accuracy is crucial and can be affected by factors like input loading and shielding. Specifications are often given in terms of percentage of reading and range, or in parts per million (ppm).
Specifications and Sensitivity
The document discusses the sensitivity of measuring instruments, highlighting that changes in input signals below a certain threshold will not be detected. Sensitivity is influenced by the instrument's resolution and measurement range.
Accuracy
Absolute accuracy is traceable to primary standards like NIST and is expressed as ±(% of reading + counts) or ±(ppm of reading + ppm of range). Relative accuracy is tied to secondary standards and follows similar expression formats.
Error Calculation
Measurement errors are calculated using accuracy specifications. For example, with an accuracy of ±(25ppm of reading + 5ppm of range), a 2V range, and a 1.5V input signal, the error is calculated as 47.5µV.
Deratings
Accuracy specifications are affected by temperature and time drift. Temperature coefficients adjust accuracy outside specified temperature ranges. Time drift affects accuracy over long periods.
Noise and Noise Rejection
Noise is critical in low-level measurements. Normal Mode Rejection Ratio (NMRR) and Common Mode Rejection Ratio (CMRR) are key specifications, indicating the instrument's ability to reject noise.
Speed
Measurement speed is crucial, often expressed as readings per second. Factors like integration period and filtering affect speed, with trade-offs between speed and accuracy.
Circuit Design Basics
Operational amplifiers are fundamental in low-level measuring instruments. Voltmeter circuits use amplifiers for voltage gain, while ammeter circuits use shunt or feedback configurations for current measurements.
Advanced Circuit Configurations
High-speed picoammeters minimize shunt capacitance for faster measurements. Logarithmic picoammeters use diodes or transistors for wide dynamic range measurements.
Coulombmeter and Ohmmeter Circuits
Coulombmeters measure electrical charge using feedback circuits. High resistance ohmmeters use a voltage source and picoammeter configuration to measure resistance.
High Resistance Measurement Using External Voltage Source
This method involves using a voltage source and a picoammeter to measure high resistance. Advantages include speed and the ability to measure extremely high resistance.
Electrometer Ohmmeter Using Built-In Current Source
This configuration uses a built-in constant-current source to force a known current through RX, with the resulting voltage drop indicating resistance.
Electrometer Ohmmeter with Guarded Ohms Mode
This modification surrounds the HI input node with a guard voltage, neutralizing input cable capacitance and speeding up measurements for resistances over 10GΩ.
Electrometer Voltmeter and External Current Source
A current source generates current through RX, and the voltage drop is measured with an electrometer voltmeter.
Low Resistance Ohmmeter Circuits
Using a nanovoltmeter and external current source, very low resistances can be measured. A four-wire method eliminates lead resistance.
Micro-ohmmeter
This device uses a four-wire ratiometric technique without internal resistors, requiring all four leads for measurement.
Complete Instruments
Digital electrometers use a preamplifier for sensitivity and input resistance, with a microprocessor controlling the A/D converter and other functions. DMMs include multiple measurement functions, converting input signals to digital information.
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Catalog excerpts

Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-1

Low Level Measurements Handbook Precision DC Current, Voltage, and Resistance Measurements Low Level Measurements Handbook Specifications are subject to change without notice. All Keithley trademarks and trade names are the property of Keithley Instruments, Inc. All other trademarks and trade names are the property of their respective companies. © Copyright 2004 Keithley Instruments, Inc. Printed in U.S.A. Keithley Instruments, Inc. Corporate Headquarters • 28775 Aurora Road • Cleveland, Ohio 44139 • 440-248-0400 • Fax: 440-248-6168 • 1-888-KEITHLEY (534-8453) • www.keithley.com

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-2

“To get a free electronic version of this book, visit Keithley’s Knowledge Center web page.” a g r e at e r m e a s u r e o f c o n f i d e n c e

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-3

Low Level Measurements Handbook Precision DC Current, Voltage, and Resistance Measurements SIXTH EDITION

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-4

SECTION 1 Low Level DC Measuring Instruments 1.1 SECTION 2 Measurements from High Resistance Sources 2.1 Low Level Measurements Handbook

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-5

SECTION 3 Measurements from Low Resistance Sources 3.1

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-6

Low Level Measurements Handbook

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-7

SECTION 5 Low Level Instrument Selection Guide 5.1 APPENDIX A Low Level Measurement Troubleshooting Guide APPENDIX B Cable and Connector Assembly APPENDIX C Glossary APPENDIX D Safety Considerations INDEX

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-8

Low Level DC Measuring Instruments

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-9

FIGURE 1-1: Standard Symbols Used in this Text Prefixes Symbol yoctozeptoattofemtopiconanomicromilli(none) kilomegagigaterapetaexazettayotta- Quantities Symbol Unit volts amperes ohms coulombs seconds watts farads cycles/s degrees EMF current resistance charge time power capacitance frequency temperature

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-10

Introduction DC voltage, DC current, and resistance are measured most often with digital multimeters (DMMs). Generally, these instruments are adequate for measurements at signal levels greater than 1µV or 1µA, or less than 1GΩ. (See Figure 1-1 for standard symbols used in this text.) However, they don’t approach the theoretical limits of sensitivity. For low level signals, more sensitive instruments such as electrometers, picoammeters, and nanovoltmeters must be used. Section 1 offers an overview of the theoretical limits of DC measurements and the instruments used to make them. It includes instrument...

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-11

FIGURE 1-2: Theoretical Limits of Voltage Measurements 103 Noise Voltage Within theoretical limits Source Resistance input offset current1 when measuring voltage and lower input resistance compared to more sensitive instruments intended for low level DC measurements. These characteristics cause errors in the measurement; refer to Sections 2 and 3 for further discussion of them. Given these DMM characteristics, it’s not possible to use a DMM to measure signals at levels close to theoretical measurement limits, as shown in Figure 1-3. However, if the source resistance is 1MΩ or less, or if the...

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-12

FIGURE 1-3: Typical Digital Multimeter (DMM), Nanovoltmeter (nVM), Nanovolt Preamplifier (nV PreAmp), and Electrometer Limits of Measurement at Various Source Resistances 100 Noise Voltage Source Resistance (input burden), which affects low level current measurements, and DMM resolution is generally no better than 1nA. Thus, an electrometer or picoammeter with its much lower input burden and better sensitivity will operate at levels much closer to the theoretical (and practical) limits of low current measurements. Instrument Definitions A number of different types of instruments are available...

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-13

2. Circuit loading must be minimized, such as when: • Measuring voltage from a source resistance of 100MΩ or higher. • Measuring current when input voltage drop (burden) of less than a few hundred millivolts is required (when measuring currents from sources of a few volts or less). 3. Charge measurement is required. 4. Measuring signals at or near Johnson noise limitations (as indicated in Figure 1-2). In addition to their versatility, electrometers are easy to operate, reliable, and rugged. Voltmeter Function The input resistance of an electrometer voltmeter is extremely high, typically greater...

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-14

Coulombmeter Function Current integration and measurement of charge are electrometer coulombmeter capabilities not found in multimeters. The electrometer coulombmeter can detect charge as low as 10fC (10–14C). It’s equivalent to an active integrator and, therefore, has low voltage burden, typically less than 100µV. The coulombmeter function can measure lower currents than the ammeter function can, because no noise is contributed by internal resistors. Currents as low as 1fA (10–15A) may be detected using this function. See Section 2.3.8 for further details. 1.3.2 The DMM Digital multimeters vary...

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-15

function instruments and are correspondingly less complex than electrometers. 1.3.4 The Picoammeter A picoammeter is an ammeter built along the lines of the ammeter function of an electrometer. When compared with an electrometer, a picoammeter has a similar low voltage burden, similar or faster speed, less sensitivity, and a lower price. It may also have special characteristics, such as high speed logarithmic response or a built-in voltage source. 1.3.5 The Source-Measure Unit As its name implies, a source-measure unit (SMU) has both measuring and sourcing capabilities. Adding current and voltage...

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-16

1.3.6 The SourceMeter® Instrument The SourceMeter instrument is very similar to the source-measure unit in many ways, including its ability to source and measure both current and voltage and to perform sweeps. In addition, a SourceMeter instrument can display the measurements directly in resistance, as well as voltage and current. The typical SourceMeter instrument doesn’t have as high an input impedance or as low a current capability as a source-measure unit. The SourceMeter instrument is designed for general-purpose, high speed production test applications. It can be used as a source for moderate...

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Low Level Measurements Handbook: Precision DC Current, Voltage, and Resistance Measurements-17

Understanding Instrument Specifications Knowing how to interpret instrument specifications properly is an important aspect of making good low level measurements. Although instrument accuracy is probably the most important of these specifications, there are several other factors to consider when reviewing specifications, including noise, deratings, and speed. 1.4.1 Definition of Accuracy Terms This section defines a number of terms related to instrument accuracy. Some of these terms are further discussed in subsequent paragraphs. Table 1-1 summarizes conversion factors for various specifications...

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