CATLAB Brochure
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CATLAB Microreactor for Catalysis Studies & Thermal Analysis

Detailed product information / introduction CATLAB Module 1 Catalyst Cartridge System A combined bench-top microreactor and mass spectrometer system for rapid and reproducible catalyst characterisation and reaction studies. XXFast response, low thermal mass furnace with integrated air-cooling XXcatalyst screening XXHiden’s unique interchangeable Catalyst Cartridge System XXpulse chemisorption XXClose-coupled hot-zone evolved species probe & direct QIC inlet for <500 ms response XXpulse calibration XXdispersion measurements XXadsorption isotherms XXreaction studies XX‘In-Bed’ thermocouple...

CATLAB Software A dedicated application specific software package for automated control of MS data acquisition fully integrated with all necessary devices including MFCs, furnace temperature, switching valves, pulse injection, etc. Key Features – CATLAB Software CATLAB software XXControl of the experiment following a user defined temperature profile XXMS data, temperature and flow all collected in one software package Control of MS data acquisition, MFCs, switching valves, temperature, etc. XXData analysis routines included in the software for determination of catalyst properties such as...

Software (continued) CATLAB Example Data (continued) Temperature Programmed Reduction (TPR) Fig. 2. Temperature Programmed Reduction Figure 2 shows the results of a TPR experiment performed on a Ni sample. TPR experiments involve linear heating of the sample under a reducing atmosphere such as H2. Key Benefits: XXHigh capacity dry pumping system provides optimum performance for applications that use light gases H2/He etc. XXExcellent H2 sensitivity – more than x2 sensitivity for H2 compared with published standard RS factors. XXNo need for removal of condensable gases before analysis....

Technical Data Front View TECHNICAL SPECIFICATIONS Sample mass: Ramp Rate: Temperature sensor: Mass flow controllers: 4 streams 3-100 ml/min standard up to 8 streams with user defined flow rates optional Minimum flow pressure: Port connection: CATLAB Software Windows 7/8/10 compatible Microreactor: 631 x 400 x 475 mm Electronics Unit: 365 x 488 x 373 mm Microreactor: 30 kg Electronics Unit: 27kg Power requirement:

Technical Data (continued) TECHNICAL SPECIFICATIONS Direct inlet high pressure source All parameters adjustable in real time Dual Faraday / Channeltron electron multiplier Detection limit: 5 x 10-11 torr with Faraday detector 2 x 10-14 torr with Channeltron detector Krypton (84Kr) in air at 0.5 ppm with Faraday detector Xenon (129Xe) in air at 25 ppb with Channeltron detector Response time: Analyser bakeout: Quartz Inlet Capillary: Typical inlet flow rate/gas consumption 20 atm ml/min Low flow rate versions to 1 atm ml/min available Power requirement: 100-240 V AC, 50-60 Hz, 1.5 kVA FURTHER...

System Configuration & Options CATLAB - PCS Module 1: The Microreactor System A Quartz Microreactor with integrated low thermal mass, air-cooled radiant furnace and close-coupled QIC sampling. This item includes the CATLAB - PCS Windows® software and computer control of temperature (ramp/set-point) and flow. Low thermal mass furnace for linear ramp control and set-point regulation to 1000°C: Includes a high temperature quartz sample reactor for operation to 1 bar with high temperature sensors and interface. CATLAB - PCS module 2: The QGA Mass Spectrometer A QGA bench-top gas analysis...

Hiden’s quadrupole mass spectrometer systems address a broad application range in: GAS ANALYSIS dynamic measurement of reaction gas streams catalysis and thermal analysis molecular beam studies dissolved species probes fermentation, environmental and ecological studies SURFACE ANALYSIS UHV TPD SIMS end point detection in ion beam etch elemental imaging – 3D mapping PLASMA DIAGNOSTICS plasma source characterisation etch and deposition process reaction kinetic studies analysis of neutral and radical species VACUUM ANALYSIS partial pressure measurement and control of process gases reactive...