1. Catalogs
  2. GERSTEL
  3. Automated Dynamic Headspace DHS

Automated Dynamic Headspace DHS

Automated Dynamic Headspace DHS

Automated Dynamic Headspace DHS

Product catalog summary
Overview of Dynamic Headspace (DHS) Technology
The Dynamic Headspace (DHS) option for the GERSTEL MPS autosampler automates the extraction and concentration of volatile organic compounds (VOCs) from samples. It combines the sensitivity of Purge and Trap with the ease of Headspace analysis, offering enhanced detection limits and eliminating carryover.

Specifications and Features
  • Adsorbents: Tenax TA is commonly used, but other adsorbents can be selected based on application needs. Multi-bed adsorbent tubes are available for a wide range of analyte boiling points and polarities.
  • Sample Handling: Samples are stored in headspace vials at ambient or controlled temperatures (4°C to 200°C). Agitation and thermostating enhance extraction efficiency.
  • Temperature Control: The adsorbent tube temperature can be controlled between 20°C and 70°C for optimal analyte trapping.
  • Automation: The GERSTEL MAESTRO software provides integrated control from extraction to GC/MS analysis, minimizing errors and optimizing productivity.

Benefits of DHS
  • High Productivity: Complete automation from extraction to introduction, with high throughput capabilities (up to 120 samples).
  • Flexibility: User-defined extraction parameters and the ability to use various adsorbents.
  • Low Detection Limits: Efficient trapping and direct transfer to GC/MS system.
  • Reliability: Inert sample path and automated standard addition for quality control.

Comparison with Other Techniques
DHS was compared with static headspace and HS-SPME using coffee samples. DHS provided the highest response and lowest relative standard deviations for analytes.

Additional Features
  • Solvent-Free Extraction: Reduces costs and improves safety by eliminating solvents.
  • Water Management: Options to limit water evaporation and trapping.
  • User-Friendly Operation: Simple control via MAESTRO software, with intuitive interface and real-time parameter display.

DHSlarge Module
The DHSlarge module allows analysis of large or inhomogeneous samples, such as consumer products and packaging, in containers up to 1L. It supports unattended analysis of up to 11 samples, enhancing productivity and system utilization.
See more

Catalog excerpts

Automated Dynamic Headspace DHS-1

Automated Dynamic Headspace Enhanced Detection Limits Carryover Eliminated Highest Productivity and Throughput Most Flexible Automated Solution Available

 Open the catalog to page 1
Automated Dynamic Headspace DHS-2

Automated Dynamic Headspace DHS The Dynamic Headspace technique combines the sensitivity and low detection limits of Purge and Trap with the ease of handling, high productivity and ruggedness of Headspace analysis. The Dynamic Headspace (DHS) option for the GERSTEL MPS autosampler, an industry standard, offers complete automation of the dynamic headspace technique. The DHS station is used to extract and concentrate VOCs from liquid or solid samples placed in standard headspace vials. The headspace above the sample is purged and analytes are concentrated on a user selectable adsorbent-filled trap....

 Open the catalog to page 2
Automated Dynamic Headspace DHS-3

DHS Benefits High productivity through high throughput design Low detection limits l Exhaustive purge of sample headspace l Efficient trapping on selectable adsorbent tube l Direct and quantitative, split or splitless transfer from trap to GC/MS system l Lower detection limits than static headspace, SPME, and other widely used techniques Solvent free extraction l Saves on costly solvents and expensive disposal fees l Improves the laboratory environment and occupational safety l Improves detection limits by eliminating solvent dilution factor l Complete automation from sample extraction to sample...

 Open the catalog to page 3
Automated Dynamic Headspace DHS-4

GERSTEL DHSlarge GERSTEL DHSlarge Autosampler The DHS can be extended with the DHSlarge module to perform analysis of large or inhomogeneous bulk samples. For example, consumer products, packaging or flooring material can be placed directly in sample containers up to 1L in volume. Sample holders are available for flooring material, eliminating interfering emissions from the edges of the cut sample. Purge periods can be introduced to simulate air exchange conditions in environmental chambers. A series of analyses can be performed on a sample to determine emission behavior over time. DHS operation...

 Open the catalog to page 4
*Prices are pre-tax. They exclude delivery charges and customs duties and do not include additional charges for installation or activation options. Prices are indicative only and may vary by country, with changes to the cost of raw materials and exchange rates.