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Automatic Mercury Analyzer Laboratory ENVEA

Automatic Mercury Analyzer Laboratory ENVEA

Automatic Mercury Analyzer Laboratory ENVEA

Product catalog summary
Main Applications
The AULA-254 Gold Automatic Mercury Analyzer is used in various fields including environmental monitoring (water, soils, sludge), food analysis (fish, innards, plants), medicine (urine, blood, saliva, hair), chemical industry (process monitoring, quality control), geochemistry, mining, petrochemistry, metallurgy, and material testing. It is applicable to several EPA methods such as 245.1, 245.7, 1631, 7470, and 7471A.
Specific Features
This system is a fully automated flow analysis system with a compact modular construction. It includes an integrated GoldTrap for high sensitivity (<1 ng/l), a wide linear measuring range, and is easy to operate with AULAWIN software. It features automatic purging after mercury concentration exceedance, minimized memory effect, a thermoelectric dehumidifier, low reagent consumption, and user safety.
Working Principle
The system operates on the continuous flow method, transforming mercury in samples to its elemental state using a reducing agent. Mercury is stripped with a gas stream in a cross-flow reactor and carried into an optical cell for quantitative determination via UV absorption at 253.7 nm. This method, known as cold vapor atomic absorption spectrometry (CVAAS), is highly sensitive and selective.
Technical Specifications
The analyzer uses UV absorption (CVAAS) with a wavelength of 253.7 nm. It employs amalgamation on gold for preconcentration and thermal desorption by rapid heating. The optical cell is made of fused silica and heated to approximately 45°C. The measuring range varies depending on the GoldTrap status, with detection limits of <50 pg Hg (GoldTrap off) and <5 pg Hg (GoldTrap on). It uses argon or nitrogen as carrier gas, with a flow rate of 4-6 l/h. The autosampler has 53 places, and the sample consumption is approximately 1 ml. The system is compatible with AULA-WIN software and operates on 110 V AC/60 Hz or 230 V AC/50 Hz power supply.
Standards Compliance
The AULA-254 Gold complies with various ISO and European standards, including ISO 6637, ISO 11212-2, ISO 16772, ISO 17733, EN 1483, EN 12497, EN 13806, and EN ISO 12846. It also adheres to EPA methods 7470A, 7471A, 245.1, 245.5, 245.6, ASTM E538, FSIS USDA, and the Ontario Hydro Method.
Optional Features
An optional Automated Sample Digestion module (ASD) is available for sample preparation. The digestion procedure involves mixing the sample with a strong oxidizing reagent and heating it to approximately 98°C. Reduction of mercury is achieved with hydroxylamine hydrochloride and tin-(II)-chloride, followed by extraction with a carrier gas.
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Catalog excerpts

Automatic Mercury Analyzer Laboratory ENVEA-1

Automatic Mercury Analyzer AULA-254 Gold LABORATORY The Automatic Mercury Analyzer AULA-254 Gold is designed for fully automatic determination of mercury traces in liquid samples and sample digests. The instrument carries out routine analysis: sample after sample following exactly the preselected procedure thus increasing efficiency and productivity of your lab. MAIN APPLICATIONS SPECIFIC FEATURES  Environmental monitoring: Water, soils, sludge ...  Fully automated flow analysis system  Analysis of foodstuffs: fish, innards, plants ...  Integrated GoldTrap for maximum of sensitivity: <1 ng/l  Medicine: urine, blood, saliva, hair ...  Chemical industry: process monitoring, quality control ...  Geochemistry, mining  Compact modular construction  Wide linear measuring range  Easy to operate with AULAWIN software  Automatic purging after exceedance of mercury concentration  Minimized memory effect  Metallurgy and material testing  Applicable to EPA Methods: 245.1, 245.7, 1631, 7470, 7471A . . . .  Low reagent consumption  Safety for the user RELIABLE AND PROVEN MEASUREMENT METHOD Photometer Thermoelectric dehumidifier Rinse pump Rinse solution Schematic flow diagram: AULA-254 Gold with Automatic Sample Digester ASD The working principle of the system is based on the continuous flow method. First the mercury contained in the sample is transformed into the elemental state by addition of a reducing agent to the sample flow. In a cross-flow reactor the mercury is stripped with a gas stream and carried into the optical cell made entirely of fused silica. There the quantitative determination of mercury is obtained by measuring UV absorption at a wavelength of 253,7 nm at room temperature. This analytical technique is commonly known as cold vapor atomic absorption spectrometry (CVAAS), a method that has proved t

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Automatic Mercury Analyzer Laboratory ENVEA-2

LABORATORY OPTION: Automated Sample Digestion module (ASD) The AULA-254 can be equipped with an optional sample preparation system for aqueous and digested samples. The digestion procedure derives from standard methods commonly used in the laboratory. The sample is automatically drawn from the auto-sampler vial and is continuously mixed with a strong oxidizing reagent (e.g. potassium permanganate, bromide-bromate). Subsequently the sample/oxidant mixture is heated to approx. 98 °C in a heated coil. After the oxidation step hydroxylamine hydrochloride and tin-(II)-chloride are added for reduction...

 Open the catalog to page 2

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