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Hydrogen Removal System AGC 70-852

Hydrogen Removal System AGC 70-852

Product catalog summary
Introduction
The document discusses the AGC Hydrogen Removal System, a solution for improving trace gas analysis by removing hydrogen from gas samples. This system is an alternative to using long columns or heartcut chromatography, which can slow down analysis times.
Specifications
  • Operating Temperature: 120°C
  • Maximum Operating Pressure: 10 BAR (150 psi)
  • Carrier Flow Rate: 30-50 ml/min
  • Fittings: 1/8” VCR face seal
  • Model: AGC 70-852
  • Air Flow: 300 ml/min
System Description
The system uses a Palladium membrane within a temperature-controlled oven to selectively diffuse hydrogen. The gas sample valve (GSV) connects to the system's inlet, and the outlet connects to the chromatograph column. The system is preset to 120°C to prevent pore clogging.
Maintenance and Operation
To remove carbon buildup, the temperature can be increased to 300°C, and hydrocarbon-free air is passed through the system. Users can purge the system with helium to prevent air injection into analytical columns. The interface allows easy temperature adjustments.
Additional Features
  • Maximum Temperature: 300°C
  • Gases Removed: H2, O2, CO
  • Separator: Palladium Membrane
Data Analysis
The document includes a chromatogram with retention times and concentrations for Argon (Ar) and Nitrogen (N2), showing their respective retention times, heights, areas, and concentrations in ppm.
Contact Information
For further information, contact AGC Instruments at their Ireland or China offices.
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Catalog excerpts

Hydrogen Removal System AGC 70-852-1

Hydrogen Removal SystemImproving Trace Gas Analysis AGC 70-852 The AGC Hydrogen Removal System solves the problem in trace analysis of Hydrogen. It is an alternative to using very long columns or heartcut chromatography which can result in slower analysis times. With Hydrogen, the best way to find the impurities is simply to remove the bulk gas, leaving only the impurities behind. The AGC 70-852 is therefore designed to remove Hydrogen from a Sample volume injected into a Gas Chromatograph column. The separator is fitted with a Palladium membrane inside a temperature controlled oven because Hydrogen will diffuse selectively through a Palladium membrane. The outlet of a gas sample valve (GSV) is connected to the INLET connection (with VCR fittings/gaskets) and the OUTLET is connected to the column. The operating temperature is set above the boiling point of water to prevent clogging of the pores (the temperature is preset to 120°C). Hydrogen breakthrough may occur when carbon builds up inside the membrane. This carbon is removed by increasing the temperature to 300°C and passing Hydrocarbon free air through the system. Simply, rotating the valve to the OFF position for one hour will burn off any deposits. To prevent air from being injected into the Analytical columns, the user can temporarily purge the system with Helium before switching the valve ON. Adjusting the temperature is a simplified with a user-friendly interface. Both Oxygen and Carbon Monoxide are also removed from the sample when it is passed through the separator. Specifications Operating Temperature To discuss the use of the Hydrogen Removal System for your application or for further information please contact: AGC Instruments Unit 2, Shannon Free Zone West, Shannon, Co. Clare, Ireland China Sales Office Daxing Industrial Development Zone, Beijing, China www.agc-instruments.com Gas Analysis Since 1965

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