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GCMS QP2010 Ultra

GCMS QP2010 Ultra
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GCMS QP2010 Ultra

Product catalog summary
Overview: The Shimadzu GC-2010 Plus is a capillary gas chromatograph system designed for high sensitivity and precision in trace analysis and fast GC applications. It features Advanced Flow Technology (AFT) for enhanced chromatographic resolution and reduced analysis times.
Advanced Flow Technology: AFT allows for multidimensional GC, capillary backflush, and other specialized flow applications. It supports high-performance separation with precise flow-switching technology, ensuring reproducibility in complex separations.
Leading Sensitivity: The system includes high-sensitivity detectors, providing quality data across a broad range of applications.
Enhanced Productivity: Features include high-speed analysis, rapid oven heating/cooling, a gas saver function, and excellent repeatability. The dual-injection system and carrier gas constant linear velocity mode further enhance productivity.
Data Management: The LabSolutions software offers easy operation, improves productivity, and is GLP/GMP and network compliant.
Applications: The GC-2010 Plus is suitable for thermal decomposition analysis, liquid injection/headspace/SPME analysis, pyrolysis, distillation GC, and PONA analysis.
Backflush System: This system reverses carrier gas flow to discharge residual components, shortening analysis time and preventing column deterioration.
Detector Splitting System: Allows compounds to be split to multiple detectors, providing abundant information in a single analysis and improving confidence in peak identity.
Reproducibility: The document includes detailed data on the reproducibility of various compounds, demonstrating the system's precision.
Specifications: The GC-2010 Plus supports up to three injection units and four detectors, with options for retrofitting. It features a design that minimizes carryover and supports high-speed gas chromatography (GC) with narrow bore capillary columns. The system includes a gas saver function and permits high-pressure injection modes.
Injection Units: The system offers various injection units, including the SPL-2010 Plus and OCI/PTV-2010, which support split/splitless and on-column/programmed temperature vaporization injection modes. The WBI-2010 Plus direct injection unit features a septum purge flow channel to prevent solvent tailing and is easily modified for packed column use.
Software - LabSolutions: LabSolutions Version 5 integrates GC and LC control, offering sophisticated functionality and ease of operation. It supports up to four GC systems and features a user-friendly interface with an Assistant Bar and Data Explorer. The software facilitates method transfer and enhances productivity through simultaneous sample processing and automatic operation control.
Data Analysis and Compliance: The software includes comprehensive functions for peak identification, quantitation, and data comparison. It supports GLP/GMP regulatory compliance with user-management functions, audit trails, and system management features. The software also offers network compatibility for remote access and centralized data management.
Customization and Validation: LabSolutions allows customization of the user interface and supports validation functions to ensure software integrity. It includes QA/QC functions for pass/fail judgments and system suitability tests, enhancing data reliability and analysis confidence.
Specifications and Compliance: LabSolutions supports GLP/GMP compliance through various validation and user-management functions. It also offers optional support for 21 CFR Part 11 compliance. The software allows for the display and comparison of up to 16 chromatograms, facilitating detailed analysis through operations like addition, subtraction, and differential calculations.
Data Comparison and Report Generation: The software provides flexible report generation capabilities, allowing users to edit chromatograms and peak tables, and save report formats as templates. It includes a PDF output function to support paperless operations. LabSolutions supports six quantitation methods and seven types of calibration curves, ensuring broad compatibility with analytical requirements.
User Management and Validation Support: User access is controlled through default user groups, with options to customize security settings. The software supports GC-2010 Plus self-diagnostic functions and includes QA/QC functions for pass/fail judgments based on component concentrations and system suitability tests.
Customization and Network Capabilities: LabSolutions allows customization of the user interface and numerical formats. It supports GC-LAN connectivity for remote control and data acquisition, enabling centralized data management and internet-based data browsing.
Software and Hardware Specifications: The software is compatible with Windows 7 Professional, XP Professional, and Vista Business. It supports control of multiple GC units and offers features like automatic data file naming, batch analysis, and OLE automation compatibility. The hardware specifications include an Intel Pentium processor, 2 GB RAM, and a 160 GB HDD.
Application Systems: The document describes various application systems integrated with the GC-2010 Plus, including thermal desorption, pyrolysis, distillation GC, and PONA analysis systems. These systems are used for analyzing volatile components, high molecular weight compounds, and petroleum fractions.
Conclusion: LabSolutions provides a robust platform for gas chromatography analysis, offering extensive data management, compliance support, and customization options to enhance laboratory productivity and data integrity.
Key Sections:
  • Analysis Applications: The GC-2010 Plus is used for various analytical needs, including the measurement of residual solvents in pharmaceuticals, flavor components in foods, and volatile components in solid or liquid samples. It supports liquid injection, headspace, and SPME analysis.
  • System Configurations: The document outlines different system configurations for specific applications, such as the Thermal Desorption System for measuring air pollutants and outgassing, and the Pyrolysis System for analyzing high molecular weight compounds.
  • Distillation GC System: This system measures the boiling point distribution of petroleum fractions and prints formatted reports after analysis.
  • PONA Analysis System: This system separates and identifies gasoline or other hydrocarbon compounds, classifying them by carbon number and type, and outputs quantitative results.
Technical Specifications: The document mentions the requirement of specific components like the OCI and high-power oven for high-boiling point component analysis and the use of autosampler and cryotrap accessories.
Disclaimer: The publication is intended for research use only and not for diagnostic procedures. It is provided "as is" without warranty, and Shimadzu disclaims any proprietary interest in third-party trademarks.
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Catalog excerpts

GCMS QP2010 Ultra-2

With Advanced Flow Technology CAPILLARY GAS CHROMATOGRAPH SYSTEM The Shimadzu GC-2010 Plus represents a new generation in top end capillary GC analysis, redefining sensitivity limits for trace analysis, fast GC applications, and easy, robust operation. Advanced Flow Technology (AFT) capability further extends the applications scope of the instrument allowing multidimensional GC, capillary backflush, and other specialized flow applications. AFT additionally enables reduced analysis times, enhanced chromatographic resolution, and application-specific configurations without compromising key performance...

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GCMS QP2010 Ultra-4

Advanced Flow Technology Advanced Flow Technology is Shimadzu´s solution to provide enhanced separation power and operational efficiency for applications with complex sample matrices. This enhanced capability is based on the high precision Advanced Flow Control (AFC) of the GC-2010 Plus. Advanced Flow Technology for high-performance separation Multi-dimensional GC/GCMS System MDGC/GCMS-2010 M u l t i -Dean s ’ Sw i t c h i n g In the past, multidimensional GC has been accomplished using a switching mechanism known as Deans’ Switch. However, this system results in such problems as a reduced recovery...

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GCMS QP2010 Ultra-5

Multi-Switching Analysis of Essential Oil Oven temp Split ratio Oven temp H2: 50 mL/min, Air: 400 mL/min, Make-up: 0 mL/min 8 compounds are switched onto the 2nd column 8 compounds are separated into 15 peaks Universita degli Studi di Messina Prof. Luigi Mondello Alessandro Casill Peter Quinto Tranchida Danilo Sciarrone Chromatogram Obtained with 1st Column Heart-cut positions

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GCMS QP2010 Ultra-6

Advanced Flow Technology for Enhanced Productivityand Confident Identification Backflush System The backflush system reverses the carrier gas flow after the target compounds have eluted, to discharge residual late eluting components in the column through the injection port split vent. Backflush shortens the analysis time and improves productivity. In addition, high-boiling point components are discharged efficiently to reduce the bakeout time (elution time), and thus prevent column deterioration, contamination, and retention time shifts. Normal Analysis Unnecessary component Analysis time shortened!...

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GCMS QP2010 Ultra-7

The Intuitive and easy-to-use Advanced Flow Technology Software is included with each AFT system. Both the backflushing and detector splitting systems are controlled with this software. Analysis of Volatile Compounds in Polystyrene Backflushing was started 12 minutes after target substances were eluted. Analysis time, including the time for discharging unwanted substances, could be reduced from 75 minutes to 18.5 minutes. * Open__j Save j Configuration. Iprfipcratyrc Cg_fcjmn Ftaw CoEumn Lenalh Film Thickness Flow Control mode Total Flii» Fur-up. Finn Spirt KathD Advanced Flow Technology software...

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GCMS QP2010 Ultra-8

Industry Leading Detector Sensitivity Responding to the ever increasing demands for trace level analysis, our new detectors boast the highest sensitivity in the industry. The new Flame Photometric Detector (FPD) and Flame Ionization Detector (FID) show significantly increased sensitivity. FID-2010 Plus Minimum Detected Quantity:1.5 pgC/s* FID-2010 Plus gives you the world’s highest FID sensitivity with clean detector gas flows and the latest noise reduction technology. High-sensitivity has been achieved by thorough cleaning of detector gas lines and the latest noise-reduction technology. Automatic...

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GCMS QP2010 Ultra-9

Flame Photometric Detector A new FPD design featuring improved flame stability and double focusing optics has produced an FPD with the world's highest sensitivity. This has all been achieved in a compact design that fits within the detector bay. The dual-focus system adds a lens to the interference filter for efficient light collection at the photomultiplier light Minimum Detected Quantity: 55 fgP/s (phosphorus compounds) 3 pgS/s (sulfur compounds) l_ens Photomultiplier P mode: Analysis of 5 ppb Organo-Phosphorus Pesticides S Mode: Analysis of 20 ppb Thiophene in Benzene

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GCMS QP2010 Ultra-10

Industry Leading Detector Sensitivity El e c tro n C a p tu re D ete cto r* Thermal Conduc tivity Detec tor A highly sensitive and selective detector for the analysis of electrophilic compounds. Top class sensitivity results from upgraded cell insulation and a cell/flow line design to reduce contamination. Compact design achieves shorter stabilization times. ECD cell is common with that for GC-2010 (ECD-2010). *In some countries, registration with the appropriate authority for regulation of radioisotopes is required before purchasing or using this detector. (Contact your Shimadzu representative...

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GCMS QP2010 Ultra-11

Highly Evolved Design Delivers Analytical Productivity H i g h - S p e e d A n aly sis High-speed analysis with narrow bore capillary columns reduces analysis time and improves sample throughput. The new-generation digital flow rate controller (AFC) provides 970 kPa maximum operating pressure and 1200 mL/min total flow to support high-speed analysis. High-Speed Analysis of Coffee Flavoring Analysis time with conventional conditions DB-WAX 0.25mm×60m, 0.25µm ( He 25cm/s ) Analysis time reduced by GC-2010 Plus B a c k fl u s h R ed u ces A n aly sis T ime The Backflush technique is effective in...

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GCMS QP2010 Ultra-12

Ra p i d O v e n H ea tin g * / C o o lin g The GC-2010 Plus incorporates a double-jet cooling system, consisting of an exhaust fan to discharge hot air and an intake fan to draw in cooling air. The system enables the reduction of cooling time from 450°C to 50°C in 3.4 min. Double-jet cooling system Large fan rapidly discharges hot air. Small fan added to enhance efficiency of cooling air intake Column oven temperature (°C) Hydrocarbon analysis in conventional mode Total analysis time: 28.7 min. Hydrocarbon analysis with GC-2010 Plus high power oven model (230V) Total analysis time: 15.2 min....

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GCMS QP2010 Ultra-13

R e p e a ta b i l ity R esettin g th e Limits All units including the column oven, flow controller, and sample injection unit are comprehensively optimized at the design stage to achieve world-class precision. Gas Saver Func tion Reduc es Car r ier Gas Us age The GC-2010 Plus features a gas saving function that considerably reduces carrier gas consumption. In the split/ splitless sample injection mode, the split ratio can be reduced after injection and during stand-by. Simultaneous ly ins tall up to th ree injec tion units and up to four detec tors Select from three injection units and five...

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