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| | | Measurement up to 1600°C • SETSYS Evolution DSC: two models from ambient to 1600°C Two temperature versions of SETSYS Evolution DSC are available. The nature of the DSC plate rod constituents changes according to the desired temperature range. | | |
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| | | | | | | | | | | | SETSYS Evolution Instrument | | Type of | Maximum use range of the rods (°C) | | | | DSC 15 | 20 to 1600 | S | 20 to 1500 | | | | | | | | | | | |
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| | | DSC 16 20 to 1750 B 20 to 1600 | | |
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| | | A DSC-type plate transducer for quantitative measurements The DSC plate transducer offers an alternative to the use of DTA rods when a quantitative measurement is desired. The DSC plate transducer consists of a machined metallic plate with two housings for the measurement and the reference crucibles. Flat-bottomed crucibles are used to optimize the thermal contact. Small pins ensure correct positioning of the crucible on the transducer. | | |
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| | | SETSYS Evolution DTA/DSC : crucibles adapted to each model of transducer Up to 1750°C, platinum, industrial alumina and zirconia crucibles are proposed for tricouple and protected transducers. Three volumes of crucible (20, 100 and 300 mm3) are available according to the mass of sample to be analyzed or the thermal effect to be measured. For limited-temperature use (up to 500°C), aluminum crucibles fitted with lids are appropriate for studying controlled dehydration. The DSC plate rod requires the use of flat-bottomed alumina or platinum crucibles. For high temperature or special measurements, tungsten or industrial graphite crucibles with covers are available. | | |
| | | f. Heat Flow (mW) | | |
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| | | T2 Onset: 469J8°C Topofpeak2:472.76°C Enthalpy: 13/24J/g Transition 2 Transition 1 ßCuBrcäaCuBr YCuBrc±ßCuBr | | |
| | | Tl Onset:384.ll°C Top of peak 1:390. Enthalpy: 28.22 J/g | | |
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| | | Melting aCuBrç±CuBr liquid T3 Onset 487.54°C Topofpeak3:492.42°C Enthalpy: 3351J/g Temperature °C | | |
| | | Procedure: 300nC to 500"C at 2 K-min"1 Crucible: Platinium Mass:! 42.98 mg Atm: Argon | | |
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| | | 360 380 400 420 440 460 480 500 | | |
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| | | Phase transitions and melting of CuBr | | |
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| | | The SETSYS Evolution DTA or DSC models have numerous applications: change of state (fusion, solidification), phase transitions, dehydration, decomposition, oxidation and reduction, and can be used equally well for organic and inorganic products, metals and alloys, ceramics, glass, etc... | | |
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| | | Cp measurement of iron | | |
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