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Additional LIBS Components
LIBS Sample Chamber
The LIBS-SC Sample Chamber is a key component of a LIBS system and is designed to perform various functions safely and in clear view of the sample. The LIBS-SC has an eyewear-safe enclosure. The chamber has a safety-interlock so the laser will not fire when the door is open. It houses a manually controlled x-y-z stage and provides illumination for the optional LIBS-IM-USB Imaging Module. The LIBS-SC has an inert gas induction port and a suction nozzle to remove particulates. In addition, you have the ability to
Stages: Manual x-y-z stage
Sample size: 6.5 cm x 6.5 cm x 4 cm max.
Laser safety shield: OD 6 for 1.064 mm laser energy (call for other
focus the laser to a 40 spot size. The sample chamber is designed for use with the Big Sky Industrial lasers we resell (see below for laser
The LIBS-SC includes an evacuation system that removes material from the sample area. You also can feed gases such as argon into the chamber. Flooding the chamber with an inert gas provides greater sensitivity for many elements.
details). If you wish to use the LIBS-SC with a different laser, please contact Ocean Optics. LIBS-SC: $9,800
wavelengths)
Internal optics:
25 mm diameter focusing lens,
75 mm focal length supplied Ablation spot size: approximately 40 urn
LIBS Imaging Module for Pinpoint Analysis
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The LIBS-IM-USB Imaging Module directly attaches to the LIBS-SC Sample Chamber to enable users to magnify a sample image and to establish a laser ablation target on the sample. The camera is also useful when you want to adjust the laser focus at the surface of the sample, or above or below the sample surface. When used with the LIBS-SC and laser, the LIBS-IM-USB and laser are in the same focal plane enabling precise, rapid and convenient laser focus. The USB-enabled color camera captures pre- and post-ablation images of the sample and provides up
Specifications
Interface: USB 2.0 (480 Mb/sec)_
Power:_USB 5 VDC, max. 180 mA_
Frame size: 1280 x 1024, 640 x 480, 320 x 240,
_160 x 120_
Data output: RGB 24 bit_
Requirements: -- Windows XP Professional SP1
-- Support of Direct X
-- Driver compatible Windows driver
model (WDM)
-- SDK iREZ WDM library -- 3.2 GHz or higher processor -- 1 GB recommended memory -- 10 GB free hard disk space -- Rocket-fast GeForce 4200Ti or better video card recommended
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LIBS-IM-USB: $8,000
LIBS Laser Options
We offer two LIBS25000 laser power options from industry leader Big Sky Laser Technologies. Laser ablation and plasma formation are very specific to the sample matrix, and therefore the power requirements will vary by sample type. For most applications we employ a Q-switched 1064 nm Nd:Yag laser, and for maximum versatility, we recommend a 200 mJ laser with attenuator to adjust the laser power according to the sample matrix. The choice of laser power and wavelength depend on the material being analyzed and the sample's tolerable damage threshold. The LIBS-LASER is a 50 mJ CFR Nd:YAG laser for metal and thin film samples. The LIBS-LAS200MJ is a 200 mJ CFR Nd:YAG laser for most all other materials.
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$14,500 $22,500
LIBS-LASER: LIBS-LAS200MJ:
LIBS Versus Other Technologies
Parameter
LIBS
SEM/EDS
XRF
LA-ICP-MS
EPMA
Sample depth:
~50-100 |jm
~5 jm
~100 jm
~80 jm
<1 urn
Sensitivity:
10-50 ppm
1000 ppm
100 ppm
<1 ppm
100 ppm
Precision:
Fair-good
Poor
Fair-good
Excellent
Fair
Accuracy:
Semi-quantitative
Qualitative
Semi-quantitative
Quantitative
Semi-quantitative
Analysis time:
Fast
Slow
Very slow
Slow
Slow
Sample consump:
almost non-destructive
non-destructive
non-destructive
almost non-destructive
non-destructive
Complexity:
Easy to use
Easy to use
Easy to use
Complicated
Complicated
Discrimination:
Good
Poor
Good
Excellent
Fair
Cost:
$60,000
$120,000
$120,000
$250,000
$600,000
Tel: 727.733.2447 • Email: Info@OceanOptics.com 49
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