Catalogue NETZSCH Thermal Analysis product catalogue
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DSC, TG - F3 Series High-Pressure DSC Thermomechanical Analysis (TMA) Dynamic-Mechanical Analysis (DMA)
DSC 200 F3 Maia»
The DSC 200 F3 Maia® is the ideal tool for day to day work in your laboratory. As a member of our new value line this instrument is a reliable entry-level heat flux DSC for:
• Product Development
• Quality Assurance
• Failure Analysis
E'/MPa 7000
□SC/(mW/mg) °-7° J I exo 0.60 0.50 0.40 0.30 0.20 0.10
2423 °C
FTFE, Repeatability Test
Peak: 39.6 °C Peak: 39.1 °C
Temperature range: -150 ... 600°C Automatic gas switching Cooling: air, liquid N2, intracooler Automatic sample changer (ASC) for up to 20 samples and references Easy-to-use
Wide range of accessories Low cost of ownership
-10K/min applied cooling rates -20 K/min before heating segment -30 K/min -40 K/min -50 K/min -60 K/min
146.5 °C
150 200
Temperature/°C
Polyethylene terephthalate (PET) is a semi-crystalline thermoplastic polymer with a relatively slow crystallization rate. In the DSC experiments, the various levels of amorphousness (Tg 75-85°C) and crystallinity (recrystallization 146°C, melting 242°C) are apparent. The samples were cooled from the melt in the DSC 204 F1 Phoenix® with the intracooler at different rates as shown prior to the heating.
A PTFE bar of 10.03 mm width by 2.13 mm height was tested in the 3-point bending mode with support distance 40 mm. In the temperature range -150 to + 150°C, three transitions are found. The DMA detects these transitions with much higher sensitivity and reproducibility compared to DSC or TMA.
DSC 200 F3 Maia®
TG 209 F3 Tarsus
The TG 209 F3 Tarsus simplifies thermo-gravimetry by featuring high perfor­mance at low operational and instru­mental outlay.
The combination of safe sample loading, flexibility in atmospheres, fast heating programs, direct temperature measure­ment at the sample and high resolution comprises a high performance TG for daily use.
TMA 202/402
TMA is the generic term for thermoana-lytical methods used for measuring mechanical characteristics of a sample with a constant or oscillating load while the sample is subjected to a controlled temperature program. The fields of application of the TMA 202/402 are diverse. Due to the high resolution of the inductive displacement transducer and the quality of the com­ponents used, measurements even on thin layers can be carried out without any problem.
DMA 242 C
The DMA 242 C is used in the determi­nation of storage and loss modulus and the damping factor of a sample as a function of temperature, time and the applied force, along with its oscillation frequency.
Vertical mounting with selectable
pushrod load of 0.1 to 200 cn
Exchangeable industrial furnaces for the temperature ranges of -150 to 500°C and from ambient temperature to 1000°C (TMA 402) Easily exchangeable sample carriers and probes
Mechanical adjustment of the measuring head so that the sample length can be set between 1 urn and 50 mm (TMA 402) Highest resolution 0.0625 nm (TMA 402)
Temperature range: RT ... 1000°C Weighing range: 2000 mg TG-resolution: 0.1 ug Atmospheres: inert, oxidizing Unique: c-DTA®
Same ASC as for DSC 200 F3 Maia®
TG 209 F3 Tarsus with ASC
TMA 402
DSC 204 HP Phoenix®
The DSC 204 HP Phoenix® features the highest working pressure (up to 15 MPa). The measurement can run under precisely controlled static or dynamic atmosphere. It is especially well-suited for application fields such as energy materials (e.g. hydrogen storage) and petrochemistry (e.g. oxidation of oils).
Temperature range: -150 ... 600°C Pressure range: vacuum up to 15 MPa
Atmosphere: static and dynamic inert, reducing, oxidizing Pressure precision: 0.02 bar Precise flow control under high pressure
Temperature range: -170 ... 600°C Frequency range: 0.01 ... 100 Hz Modulus range: 10-3 ... 106 MPa Force up to 16 N Deformation modes: bending, tension, shearing, compression/ penetration
Special furnace: moisture, UV Special sample holders for liquids, stiff materials, industrial foams Immersion tests
Fast Fourier Transformation (FFT)
DSC 204 HP Phoenix® 6
DMA 242 C
7
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