Automated Mercury Porosimeters - Micromeritics - #5

/ 6


catalogue search
P. 01
P. 02
P. 03
P. 04
P. 05
P. 06
Pages:


See other catalogues for Micromeritics

Text version of the page
Penetrometer Characteristics
The penetrometer consists of a sample cup bonded to a metal-clad, precision-bore, glass capillary stem. The sample is placed in the sample cup; during analysis, mercury Ms the cup and capillary stem. As pressure
on the filled penetrometer increases, mercury
intrudes into the sample's pores, beginning with those pores of largest diameter. The mercury moves from the capillary stem
resulting in a capacitance change between the mercury column inside the stem and the metal cladding on the outer surface of the
stem. The AutoPore detects very slight changes in capacitance (equivalent to a dif­ference of less than 0.1 microliter of mercury) so extraordinary resolution is achieved.
The computer will not accept keyboard instructions to overpressurize the system.
The high-pressure system is mechanically unable to generate unsafe pressures.
A circuit stops the generation of pressure
in the event of a failure in the computer. The operating specifications of the
pressure systems (low = 50 psia, high = 60,000 psia) are well below the actual designed safety limits.
Micromeritics also offers a large selection
of penetrometer bulbs, volumes, stems, and closures designed to fit most sample forms, shapes, porosity, and quantity. The better the match between the sample, its porosity, and the measurement range of the sample cell, the more precise the results.
Safety Systems
The AutoPore features several levels of mechanical and electro-mechanical
safety devices:
m
Cavity to Tliroat Size Ratio
The extensive report system includes pore structure calculations including Cavity-to-Throat Size Ratio, Fractal Dimension, Material Compressibility, and Statistical Process Control reporting.
Material Compressibility
• Intrusion Volume, Predicted o Intrusion Volume Actual
Percent Paioslly Filled 1.%)
Intrusion Data Summary
Total Intrusion Volume =
1.2166 mug
Total Pore Area =
305 380 mVg
Median Pore Diameter (Volume)-
0.0171 um
Median Pore Diameter (Area) =
0.0084 um
Average Pore Diameter (4VM) =
0.0159 um
Bulk Density at 0-55 psia -
0.6872 SJfmL
Apparent (skeletal) Density =
4.1929 gmlL
Porosity =
32.6101 %
Stem Volume Used -
60 %
A convenient data summary is automatically generated with each sample reported.
20,000 40,000
Pressure (psia)
The material compressibility is easily calculated and may be reported both graphically and in tabular form using the AutoPore report system.
Pore Structure Summary
Threshold Pressure:
136.6Ê
psia (Calculated)
Characteristic length -
1.3213
pm
Conductivity formation factor =
0.232
Permeability constant -
D0D442
Permeability -
1.7956
mdarcy
BET Surface Area =
230.0000
Pore snaps exponent =
1.00
Tortuosity factor -
1907
Tortuosity -
3.3265
Additional pore structure calculations are included in the AutoPore software.
To request a quote or additional product information, visit Micromeritics' web site at www.micromeritics.com, contact your local Micromeritics sales representative, or our Customer Service Department at (770) 662-3636.

pageCatalog pdf di En 2012-02-07-16