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| | | Penetrometer Characteristics The penetrometer consists of a sample cup bonded to a metal-clad, precision-bore, glass capillary stem. The sample is placed in the sample cup; during analysis, mercury Ms the cup and capillary stem. As pressure on the filled penetrometer increases, mercury intrudes into the sample's pores, beginning with those pores of largest diameter. The mercury moves from the capillary stem resulting in a capacitance change between the mercury column inside the stem and the metal cladding on the outer surface of the stem. The AutoPore detects very slight changes in capacitance (equivalent to a difference of less than 0.1 microliter of mercury) so extraordinary resolution is achieved. | | |
| | | The computer will not accept keyboard instructions to overpressurize the system. The high-pressure system is mechanically unable to generate unsafe pressures. A circuit stops the generation of pressure in the event of a failure in the computer. The operating specifications of the pressure systems (low = 50 psia, high = 60,000 psia) are well below the actual designed safety limits. | | |
| | | Micromeritics also offers a large selection of penetrometer bulbs, volumes, stems, and closures designed to fit most sample forms, shapes, porosity, and quantity. The better the match between the sample, its porosity, and the measurement range of the sample cell, the more precise the results. Safety Systems The AutoPore features several levels of mechanical and electro-mechanical safety devices: | | |
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| | | Cavity to Tliroat Size Ratio | | |
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| | | The extensive report system includes pore structure calculations including Cavity-to-Throat Size Ratio, Fractal Dimension, Material Compressibility, and Statistical Process Control reporting. | | |
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| | | Material Compressibility • Intrusion Volume, Predicted o Intrusion Volume Actual | | |
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| | | Percent Paioslly Filled 1.%) | | |
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| | | | | | | | | | Intrusion Data Summary | | | | Total Intrusion Volume = | 1.2166 mug | | | | Total Pore Area = | 305 380 mVg | | | | Median Pore Diameter (Volume)- | 0.0171 um | | | | Median Pore Diameter (Area) = | 0.0084 um | | | | Average Pore Diameter (4VM) = | 0.0159 um | | | | Bulk Density at 0-55 psia - | 0.6872 SJfmL | | | | Apparent (skeletal) Density = | 4.1929 gmlL | | | | Porosity = | 32.6101 % | | | | Stem Volume Used - | 60 % | | | | | | | | | |
| | | A convenient data summary is automatically generated with each sample reported. | | |
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| | | 20,000 40,000 Pressure (psia) The material compressibility is easily calculated and may be reported both graphically and in tabular form using the AutoPore report system. | | |
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| | | | | | | | | | | Pore Structure Summary | | | | | Threshold Pressure: | 136.6Ê | psia (Calculated) | | | | Characteristic length - | 1.3213 | pm | | | | Conductivity formation factor = | 0.232 | | | | | Permeability constant - | D0D442 | | | | | Permeability - | 1.7956 | mdarcy | | | | BET Surface Area = | 230.0000 | | | | | Pore snaps exponent = | 1.00 | | | | | Tortuosity factor - | 1907 | | | | | Tortuosity - | 3.3265 | | | | | | | | | | | |
| | | Additional pore structure calculations are included in the AutoPore software. | | |
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| | | To request a quote or additional product information, visit Micromeritics' web site at www.micromeritics.com, contact your local Micromeritics sales representative, or our Customer Service Department at (770) 662-3636. | | |
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