The marcsc "Cryogenic Sample Changer" - marresearch - #4

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Goniometer, X-ray detector, Sensor, Detector, CCD sensor


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Technical Description
General:
Dedicated and highly optimized hardware for sample exchange
All operations are optimized for highest possible throughput
Sample exchange in approx. 2 minutes
Perfect fit into desktop beamline®, compact design
Liquid sample transfer
Quick and precise tranfer of sample from storage system onto goniometer head Sample stays submerged in liquid nitrogen during entire transfer procedure Special transfer containers extend time beyond 60 sec. before nitrogen starts boiling
Usage of standard cryo vials
Screw-caps or (optional) magnetic vials
Large allowances for pin size and shape
Length and style of the pin holding the sample may vary
Long term operation
Up to 7 days autonomous operation without user intervention Low icing rates achieved by special anti-icing mechanisms
Automatic liquid nitrogen refill
Two-chambered dewar allows for smooth refill from supplying dewar during operation
Storage carousel for up to 19 samples
Carousel can easily be loaded or unloaded by hand Automatic positioning of samples
High speed tp-axis for quick centering
Integrated automatic centering gear (x,y,z)
Automatic crystal finding and centering routines
Automatic interpretation of crystal pictures captured by video camera of desktop beamline"
Semi-automatic centering option - manual intervention possible
Seamless integration of sample changer control into data collection software
Sample changing is just one more parameter for data collection Support of mar345 image plate and mar©©D detector
Interface to AWT©mar data processing for fully automatic selection of suitable crystals
Motors:
Carousel rotation
Stepper motor to rotate carousel and present a vial to the vial picker
Vial picker
Stepper motor to pick a vial out ot the carousel Stepper motor to lift the vial out of the carousel
Vial server
Stepper motor to swing the vial from the vial picker to the goniometer head Stepper motor to translate the vial onto the goniometer head
Sample mounting
Stepper motor for tp-axis: opens and closes vials
Stepper motor for tp-swing: moves goniometer head into a suitable mounting position (x=60o) Sample centering
Stepper motor to translate the sample on the goniometer head in x-direction Stepper motor to translate the sample on the goniometer head in y-direction Stepper motor to translate the sample on the goniometer head in z-direction
Intelligent motor control
All motors are driven by real-time electronics of the desktop beamline® and operated in the same way as all other motors of the desktop beamline®
marifWSis&iiTCBüQ
X-RAY Research GmbH Phone: +49 40 529 884- 0
Hans-Boeckler-Ring 17 Fax: +49 40 529 884-20
D-22851 Norderstedt info@marresearch.com
Germany www.marresearch.com
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marUSA, Inc. 1880 Oak Avenue Evanston, IL 60201
USA
Phone: +1-847-869-1548 Toll free: 877-MAR-XRAY Fax: +1-847-869-1587 info@mar-usa.com www.mar-usa.com

pageCatalog pdf di En 2012-05-22-30