1,000 ml Bolted ClosureStirred Reactor

At a Glance ° F(Design Pressure)(379 Bar @ 343 Volume:1,000 ml Vessel MAWP:5,500 psi @ 650 ° C)Material of Construction:316 Stainless Steel orHASTELLOY
® C-276

Principle of Operation

The Autoclave Engineers’ Bolted Closure Reactor has been designed for reliable high pressure operation. The industrial seal is a metal gasket machined from the same material as the vessel. Many combinations of standard components are available. The cover of the unit remains fixed in the stand to permit opening of the vessel without disassembling any process connections. The body is easily removed and drops away from the cover.

General Specifications

Maximum Allowable Working Pressure (MAWP)

5,500 psi @ 650 ° F*(379 Bar @ 343 ° C)*

Minimum Design Metal Temperature (MDMT)

-20 ° F @ 5,500 psi(-29 ° C @ 379 Bar)

Maximum Recommended Operating Pressure (MROP)

varies based on gauge, transducer, and rupture disk selection.Refer to Ordering Guide for Details.Critical Dimensions:1,000 mlInside Diameter:3.0” (76 mm)Straight Wall:8.71” (221 mm)ApproximateDimensions:Tall Bench TopFloor StandOverall Height**39.4” (1002 mm)61.8” (1570 mm)Width:20.5” (522 mm)25.0” (635 mm)Depth:26.2” (665 mm)26.5” (665 mm)
*650 ° F (343 ° C) rating is vessel mean wall temperature. Actual Process temperature will be lower.** Overall height based on belt driven units. For actuals see standard drawings.

1,000 ml Bolted Closure Reactor Internals

Connection Schedule

All of the connections shown will be provided. For any accessories not ordered, the corresponding connection will be plugged.All connections at cover are AE high temperature F437 Flat Bottom adapted to the “Topside Of Cover” connection listed below.

OpeningLabelPurposeOpening or featuredescription onunderside of coverOpening or featuredescription on topsideof cover Entry PointSmallest diameterorfice (nominal)in flow path

“A” Charging Port0.375” port3/8” O.D. tubeCover top0.25”“B” Gas Inlet3/16” O.D. tube1/8” O.D. tubeCover side0.062”“C” Sparge Tube†3/16” O.D. tube1/8” O.D. tubeCover side0.031”†“D” & “H” Cooling Coil3/16” O.D. tube1/4” O.D. tubeCover side0.125”“E”Vent and Pressure IndicationBranched into “F”1/8” O.D. tubeCover side0.062”“F” Safety Head0.187” port1/8” FNPTCover top0.187”“G” Thermowell‡1/8” O.D. tube3/32” Port‡Cover topN/A“J” Blow Pipe3/16” O.D. tube1/8” O.D. tubeCover side0.062”“K” Liquid Sample3/16” O.D. tube1/8” O.D. tubeCover side0.062”“L” MagneDrive
® Agitator
1/2 ” O.D. Mixing ShaftMagneDrive
® Cover topN/A †
The tube that forms the sparge tube is 3/16” O.D. and 1/8” I.D. with a plug in the end. Nine .031” diameter holes are drilled in the sparge ring to bubble gas into the reactor. ‡
The tube that forms the thermowell is 1/8” O.D. and 1/16” I.D. with a plug in the end. A 3/32” port is drilled in the cover to guide the thermocouple to the opening in the thermowell.