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Agilent GC-MSD 5977

Agilent GC-MSD 5977
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NEW 7890B Gas Chromatograph + 5977 Single Quadrupole January 2013 1 Agilent Confidential March 8, 2013

Today’s Challenges Economic - Routine - Economic - Method Development Sensitivity 2 • • • • Productivity Cost of Ownership Investment Protection Ease-of-Use • Time = Money • Skilled Resources … Harder to Find • Trend – Lower LOD’s • “Imperfect” Samples Confidentiality Label March 8, 2013

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Agilent’s Response - 7890B GC & 5977A MSD - OpenLAB & MassHunter • Productivity Economic - Routine - Economic - Method Development • Investment Protection • Cost of Ownership • Ease-of-Use Integrated GC/MSD Communications OpenLAB, MassHunter Integrated GC/MSD Communications Gas/Power Resource Management OpenLAB, MassHunter • Time = Money • Skilled Resources … Harder to Find Integrated Intelligence • Trend – Lower LOD’s 5977A MSD GC FPD “Plus” Inert Flow Path Sensitivity • “Imperfect” Samples 3 Confidentiality Label March 8, 2013

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7890B 5977A Direct, 2-Way (LAN) Communication … Enhances and Protects Your GC/MSD Investment 5977A 7890B If the MSD vents Increases GC gas flows Cools MSD faster 40% Faster Vent Times If a Pump Event/Failure Stops GC Flows Don’t waste expensive He Don’t build-up H2 5977A 7890B GC monitors GC/MSD connection If communication is lost… GC shuts down various (GC) thermal zones

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7890B – Better GC Selective Detector MDL Specs … uECD, NPD No Changes in Designs Improved Manufacturing Processes/Controls Less Variability Lower MDL Specifications Guaranteed uECD 5.5 NPD 5 fg/sec 4.5 pg N/sec pg P/sec 0.1 0.08 0.03 0.01 Confidentiality Label March 8, 2013

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New FPD “Plus” • Advanced Photomultipliers • Deactivation Treatments • Design Improvements 7890A FPD Max Temp: 7890B FPD+ 250C 400C Sulfur MDL (pg S/sec)) : Phosphorus MDL (fg P/sec): 3.6 60 Higher Sulfur Response 2.5 45 [Agilent SCD = 0.5 pg S/sec] Lower Noise

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Analysis of Substituted Dibenzothiophenes in Light Cycle Oil (LCO) 4MDBT 4, 6 -DMDBT 2,3 DMDBT C3-DBT’s • The detector must be operated at temperatures above 300 C • Agilent FPD Plus’ higher temperature /improved sensitivity expands S-applications addressable by the easy-to-use FPD

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Improving Performance: Focus on sample flowpath Inert system Active system Active or contaminated components in the flow path, before the detector, can reduce the overall sensitivity of the system Consider the following: Inlet liner Gold seal SSL inlet (weldment) Column Capillary Flow Device Detector 8 Confidentiality Label March 8, 2013

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Technologies that matter: Only from Agilent Agilent has developed core competency in chemical vapor deposition surface deactivation resulting in proprietary processes to dramatically improve GC inertness. Deactivation processes for: •Glass •Steel •Gold •Glass wool

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Agilent Inert Flow Path … From Injection to Detection Ensures superior performance for trace level analysis Ultra Inert Inlet Liner New Ultimetal Plus Inlet Weldment Inert Flowpath S/SL Ultimetal Plus – TCD, FPD, NPD/FID Jets Ultra Inert Gold Seal Ultimetal Plus Capillary Flow Technology Devices, Ultimate Union Ultra Inert GC Column Page 10 Agilent Confidential November 2012

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Agilent’s Inert Flowpath..From Injection to Detection Clearly less breakdown of a ppb level standard after 100 injections! 50 ppb Endrin Consider the following: Inlet liner Gold seal Inlet weldment Column Capillary Flow Device Detector 100 ppb DDT With Inert Flowpath Without Inert Flowpath Splitless Injection, 280C, ECD, 280C 11 Confidentiality Label March 8, 2013

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Integrated Intelligence … A Smarter GC System Integrated Intelligence Benefit Integrated GC calculators Develop methods easier Barcode Scanning with Auto-Input Easier configuration Integrated early-maintenance-feedback Manage assets more efficiently GC:MSD communication Faster MSD vent Protect system better 3D Interactive Consumable and Parts Finder Find parts faster & order easier Sleep-Wake Modes … Also coordinated with 5977A MSD Lower cost of ownership 12 Agilent Confidential March 8, 2013

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Cormectioo | Qmfigutalion C ResouiceConservation Reciuce gas and power consumptlon by settng gas saver and Instrument- scheduie options Instrument Scheduie Select a scheduie Ihat best matches how jw use this Instrument WakeMethod | EditWake Method Sleep Metrod: Edil Sleep Method _Wake to last acbve method befwe tteep [r] Rerfam a condilioning i ur> on Wake | Ed* Condftcninc Method |

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Earty Martenance FeeAack Carter» Martenance Log [ Mart |tj FwntMet Backttet M ^ Ddedor [ ^ Back Detector [ <J Trri Detector J Frort frcctor' J Courn 1 j J Cok/m 2 Collectof asjernWy mjecöons Bead basdine voltage Eead integral of cur rent

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Criterion: C Translate Only H Best Efficiency f* Fast Änajysjs (*" None | Speed qain: 2.50000 Original Method Internal Diameter, Phase Ratio Outlet Velocity, Average Velocity, Hold-up Time, Outlet Pressure (absolute], psi Ambient Pressure (absolute), psi Sample Information |None ^1 Translated Method Very large Ramp Final Rate Temp. Agiient lechnoiogies

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Barcode Scanning Input Liners Columns Barcode in the columns, liners, and syringes right into the Agilent data system method *Also syringes 16 Confidentiality Label March 8, 2013

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PARTS FINDER FIND PARTS

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rt > Agilent 7890B > Top > Select an Inlet > Multimode Inlet Parts > Liners PARTS FINDER FIND PARTS PARTS LIST Ultra Inert Split Liners Add To Parts List Add To Favorites Part Number Part Description

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7890A Enhancements Kit 7890A Logic Board Enhancement Kit - Makes a 7890A GC ready for most (but not all*) 7890B GC features • “Integrated Intelligence” features: - Early Maintenance Feedback (EMF), Sleep/Wake modes - Method Translation Calculator - Enable 2-way GC/5977A MSD communication • Agilent Serial Port: - 2nd communication port for Remote Advisor - Optional Bar Code Reader connects directly to GC [also a version for USB/PC] • FPD Plus * 7890B Only - 2nd MMI on GC, 3rd Detector as uECD 19 Confidentiality Label March 8, 2013

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